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    ASYMMETRIC AND/OR LOW-SYMMETRIC FLUORINE-CONTAINING PHOSPHATE FOR NON-AQUEOUS ELECTROLYTE SOLUTION
    1.
    发明申请
    ASYMMETRIC AND/OR LOW-SYMMETRIC FLUORINE-CONTAINING PHOSPHATE FOR NON-AQUEOUS ELECTROLYTE SOLUTION 审中-公开
    不对称和/或低对称含氟磷酸盐用于非水溶性电解质溶液

    公开(公告)号：US20120094190A1

    公开(公告)日：2012-04-19

    申请号：US13380658

    申请日：2010-07-30

    申请人： Hideyuki Mimura ,  Kentaro Kono ,  Hisao Eguchi ,  Kotaro Sakoda ,  Masahiro Aoki

    发明人： Hideyuki Mimura ,  Kentaro Kono ,  Hisao Eguchi ,  Kotaro Sakoda ,  Masahiro Aoki

    IPC分类号： H01M10/056 ,  C07F9/141

    CPC分类号： H01M10/0569 ,  H01M10/052 ,  H01M10/0525 ,  H01M10/4235 ,  Y02T10/7011

    摘要： As to a fluorine-containing phosphate used to impart flame retardancy to an electrolyte solution for a non-aqueous secondary battery, a fluorine-containing phosphate having high flame retardancy and providing high battery performance such as high-rate charge-discharge characteristics, and a method for manufacturing the same are provided. Also provided are a non-aqueous electrolyte solution and a non-aqueous secondary battery each containing the fluorine-containing phosphate.Further a fluorine-containing phosphate having a high ability to dissolve an electrolyte and capable of providing the composition of a safer electrolyte solution is provided.The fluorine-containing phosphate for a non-aqueous electrolyte solution is represented by the general formula (1) (wherein R represents an alkyl group having 1 to 10 carbon atoms or a fluorine-containing alkyl group having 1 to 10 carbon atoms, A and B are different from each other and each represent a hydrogen atom or a fluorine atom, and n and m each independently represent an integer from 1 to 8) and contains fluorine atoms in a weight ratio of 30% or higher.

    摘要翻译： 对于用于赋予非水二次电池用电解液阻燃性的含氟磷酸盐，具有高阻燃性且具有高电压特性的含氟磷酸盐，例如高倍率充放电特性，以及 提供了制造该方法的方法。 还提供了含有含氟磷酸盐的非水电解液和非水二次电池。 此外，还提供了一种具有高溶解电解质并且能够提供更安全的电解质溶液组成的能力的含氟磷酸盐。 用于非水电解质溶液的含氟磷酸酯由通式（1）表示（其中R表示碳原子数为1〜10的烷基或碳原子数1〜10的含氟烷基，A和 B彼此不同，各自表示氢原子或氟原子，n和m各自独立地表示1〜8的整数），并且含有30重量％以上的氟原子。

    Method of purifying and separating 2-fluoro-3-oxoalkylcarboxylic acid ester
    3.
    发明授权
    Method of purifying and separating 2-fluoro-3-oxoalkylcarboxylic acid ester 失效
    纯化和分离2-氟-3-氧代烷基羧酸酯的方法

    公开(公告)号：US07220878B2

    公开(公告)日：2007-05-22

    申请号：US10490432

    申请日：2001-09-27

    申请人： Norihisa Kondo ,  Hideyuki Mimura ,  Kosuke Kawada ,  Shoji Arai

    发明人： Norihisa Kondo ,  Hideyuki Mimura ,  Kosuke Kawada ,  Shoji Arai

    IPC分类号： C07C69/66

    CPC分类号： C07C67/54 ,  C07C69/716

    摘要： The present invention concerns a method for purifying/separating a 2-fluoro-3-oxoalkylcarboxylic acid ester from a reaction mixture resulting from the fluorination of a 3-oxoalkylcarboxylic acid ester. The method involves depleting the reaction mixture of a hydrogen fluoride byproduct; and subsequently, separating the 2-fluoro-3-oxoalkylcarboxylic acid ester by distillation. The 2-fluoro-3-oxoalkylcarboxylic acid ester obtained by the method of the invention is highly pure and is thus suitable for use as an intermediate for the production of pharmacological products or agricultural chemicals.

    摘要翻译： 本发明涉及从3-氧代烷基羧酸酯氟化得到的反应混合物中纯化/分离2-氟-3-氧代烷基羧酸酯的方法。 该方法涉及耗尽氟化氢副产物的反应混合物; 随后通过蒸馏分离2-氟-3-氧代烷基羧酸酯。 通过本发明方法获得的2-氟-3-氧代烷基羧酸酯是高纯度的，因此适合用作生产药物产品或农药的中间体。

    Flame-retardant electrolytic capacitor
    5.
    发明授权
    Flame-retardant electrolytic capacitor 有权
    阻燃电解电容器

    公开(公告)号：US09496092B2

    公开(公告)日：2016-11-15

    申请号：US14411414

    申请日：2013-07-01

    申请人： NIPPON CHEMI-CON CORPORATION ,  TOSOH F-TECH, INC.

    发明人： Masashi Ozawa ,  Junichi Kawakami ,  Hideyuki Mimura ,  Hisao Eguchi

    IPC分类号： H01G11/54 ,  H01G9/145 ,  H01G11/58 ,  H01G9/035

    CPC分类号： H01G9/145 ,  H01G9/035 ,  H01G11/54 ,  H01G11/58

    摘要： Provided is a flame-retardant electrolytic capacitor which is capable of maintaining flame-retardant effect even after a prolonged period of time. This is an electrolytic capacitor comprising an anode foil that is provided with an oxide film on the surface, a cathode foil, a separator, and an electrolytic solution that contains a solute in a solvent, wherein a phosphoric acid ester amide represented by the following general formula (1) is contained in the electrolytic solution: in which n is 1 or 2, and R1 and R2 each independently represent a linear or branched alkyl group having 1 to 10 carbon atoms, and Rf represents a linear or branched fluoroalkyl group having 1 to 10 carbon atoms or a linear or branched alkyl group having 1 to 10 carbon atoms).

    METHOD FOR STABILIZING LIPF6, ELECTROLYTE SOLUTION FOR NONAQUEOUS SECONDARY BATTERIES HAVING EXCELLENT THERMAL STABILITY, AND NONAQUEOUS SECONDARY BATTERY HAVING EXCELLENT THERMAL STABILITY
    6.
    发明申请
    METHOD FOR STABILIZING LIPF6, ELECTROLYTE SOLUTION FOR NONAQUEOUS SECONDARY BATTERIES HAVING EXCELLENT THERMAL STABILITY, AND NONAQUEOUS SECONDARY BATTERY HAVING EXCELLENT THERMAL STABILITY 有权
    用于稳定LIPF6的方法，具有极好的热稳定性的非水二次电池的电解液，以及具有极好的热稳定性的非水二次电池

    公开(公告)号：US20150140445A1

    公开(公告)日：2015-05-21

    申请号：US14406884

    申请日：2013-06-13

    申请人： TOSOH F-TECH, INC.

    发明人： Masahiro Aoki ,  Hideyuki Mimura ,  Hisao Eguchi

    IPC分类号： H01M10/0567 ,  H01G11/56 ,  H01M10/0568 ,  C07F9/24 ,  H01M10/052

    CPC分类号： H01M10/0567 ,  C07F9/091 ,  C07F9/11 ,  C07F9/1411 ,  C07F9/224 ,  C07F9/24 ,  C07F9/2458 ,  C07F9/2462 ,  C07F9/2466 ,  C07F9/247 ,  C07F9/650952 ,  C07F9/6533 ,  C07F9/6544 ,  H01G11/56 ,  H01G11/58 ,  H01M10/052 ,  H01M10/0568 ,  H01M10/0569 ,  H01M2300/0025 ,  H01M2300/0037 ,  Y02E60/122 ,  Y02E60/13 ,  Y02T10/7011 ,  Y02T10/7022

    摘要： [Problem] To provide: a method for stabilizing a solution that contains LiPF6 by increasing thermal stability of LiPF6 without changing the structure thereof; an electrolyte solution for nonaqueous secondary batteries, which has increased thermal stability; and a nonaqueous secondary battery which has increased thermal stability.[Solution] To have a solution containing LiPF6 contain a phosphoric acid ester amide represented by general formula (I) in such an amount that the molar ratio of the phosphoric acid ester amide relative to LiPF6 is 0.001-2. (In the formula, m represents an integer of 1 or 2; each of R1 and R2 represents a branched or linear alkyl group having 1 to 6 carbon atoms and/or a hydrocarbon group having an unsaturated bond, provided that R1 and R2 may have a substituent that is selected from the group consisting of an alkoxy group, an amino group, an alkylthio group, a saturated heterocyclic group, an unsaturated heterocyclic group, and a fluorine atom, and R1 and R2 may combine together to form a 5 to 8 membered cyclic structure; and R3 represents a branched or linear alkyl group having 1 to 6 carbon atoms or a branched or linear fluorine-containing alkyl group having 1 to 6 carbon atoms)

    摘要翻译： [问题]提供：通过增加LiPF 6的热稳定性而不改变其结构来稳定含有LiPF 6的溶液的方法; 非水系二次电池用电解液，其热稳定性提高; 和具有增加的热稳定性的非水二次电池。 [溶液]为了使含有LiPF 6的溶液含有通式（I）所示的磷酸酯酰胺，其量使得磷酸酯酰胺相对于LiPF 6的摩尔比为0.001-2。 （式中，m表示1或2的整数，R1和R2各自表示碳原子数1〜6的支链或直链烷基，和/或具有不饱和键的烃基，只要R 1和R 2可具有 选自烷氧基，氨基，烷硫基，饱和杂环基，不饱和杂环基和氟原子的取代基，R1和R2可以组合在一起形成5至8个 R3表示碳原子数1〜6的支链或直链烷基或碳原子数1〜6的支链或直链状含氟烷基）

    FLUORINE-CONTAINING PHOSPHATE ESTER-AMIDE, AND FLAME RETARDANT RESIN, FLAME RETARDANT LIQUID AND FLAME RETARDANT SOLVENT FOR ORGANIC SYNTHESIS CONTAINING SAME
    7.
    发明申请
    FLUORINE-CONTAINING PHOSPHATE ESTER-AMIDE, AND FLAME RETARDANT RESIN, FLAME RETARDANT LIQUID AND FLAME RETARDANT SOLVENT FOR ORGANIC SYNTHESIS CONTAINING SAME 有权
    含氟磷酸酯酰胺和阻燃树脂，阻燃剂液体和阻燃剂用于有机合成

    公开(公告)号：US20150053901A1

    公开(公告)日：2015-02-26

    申请号：US14385862

    申请日：2013-03-22

    申请人： TOSOH F- TECH, INC.

    发明人： Hideyuki Mimura ,  Hiroaki Fujita ,  Hisao Eguchi

    IPC分类号： C07F9/59 ,  C09K21/12 ,  C08G18/24 ,  C08G18/72 ,  C08G18/32 ,  C07F9/24 ,  C08J9/00

    CPC分类号： C07F9/59 ,  C07F9/2408 ,  C07F9/2454 ,  C07F9/2458 ,  C08G18/24 ,  C08G18/32 ,  C08G18/72 ,  C08J9/0038 ,  C08J2375/04 ,  C09K21/12 ,  H01M10/0525 ,  H01M10/0567 ,  H01M10/4235

    摘要： [Problem] To provide a fluorine-containing phosphate ester-amide which has high flame retardancy such as exhibiting flame retardant effects at a small quantity of addition, and sufficient hydrolysis resistance.[Solution] A fluorine-containing phosphate ester-amide represented by general formula (1). (In the formula, R1 and R2 are the same or different and represent a branched or linear alkyl group having 1 to 20 carbon atoms in which at least one carbon bonded to a nitrogen atom is a secondary or tertiary carbon, wherein R1 and R2 may have a substituent group selected from the group consisting of an alkoxy group, a hydroxy group, an amino group, a methyl amino group, an ethyl amino group, a dimethyl amino group, diethyl amino group and a fluorine atom. In addition, R1 and R2 may be bonded together to form a five- to eight-membered cyclic structure. X and Y are the same or different and represent a hydrogen atom or a fluorine atom, and n and m represent an integer of 1 to 6.)

    摘要翻译： [问题]提供一种具有高阻燃性的含氟磷酸酯 - 酰胺，例如在少量添加下显示出阻燃效果，并且具有足够的耐水解性。 [溶液]由通式（1）表示的含氟磷酸酯 - 酰胺。 （式中，R 1和R 2相同或不同，表示碳原子数1〜20的支链或直链烷基，其中至少一个与氮原子键合的碳为仲或叔碳，其中R1和R2可以 具有选自烷氧基，羟基，氨基，甲基氨基，乙基氨基，二甲基氨基，二乙基氨基和氟原子的取代基，此外，R1和 R2可以结合在一起形成五元至八元环状结构，X和Y相同或不同，表示氢原子或氟原子，n和m表示1〜6的整数。）

    Trifluoromethylthiophenium derivative salt, method for producing the same, and method for producing trifluoromethyl-containing compounds using the same
    8.
    发明授权
    Trifluoromethylthiophenium derivative salt, method for producing the same, and method for producing trifluoromethyl-containing compounds using the same 有权
    三氟甲基噻吩衍生物盐，其制备方法，以及使用其制备含三氟甲基的化合物的方法

    公开(公告)号：US08703969B2

    公开(公告)日：2014-04-22

    申请号：US13378420

    申请日：2010-07-13

    申请人： Norio Shibata ,  Takumi Kagawa

    发明人： Norio Shibata ,  Takumi Kagawa

    IPC分类号： C07D333/54 ,  C07C321/28

    CPC分类号： C07D333/54 ,  C07C67/343 ,  C07C253/30 ,  C07C321/28 ,  C07C323/03 ,  C07C2601/02 ,  C07C2602/08 ,  C07C2602/10 ,  C07C69/738 ,  C07C69/757 ,  C07C69/716 ,  C07C255/35 ,  C07C255/37

    摘要： A trifluoromethylthiophenium derivative salt useful as synthetic intermediates for pharmaceuticals and agrochemicals, a method for producing the same, and a method for producing trifluoromethyl-containing compounds using the same are provided. An S-(trifluoromethyl)-benzo[b]thiophenium derivative salt is represented by the following general formula (1): wherein R1, R2, R3, and R4 are each independently a hydrogen atom, a methyl group, an ethyl group, a linear, branched, or cyclic alkyl group having 3 to 10 carbon atoms, a methoxy group, an ethoxy group, a linear, branched, or cyclic alkyloxy group having 3 to 10 carbon atoms, a fluorine atom, a chlorine atom, a bromine atom, a nitro group, or a cyano group, R5 is a methyl group, an ethyl group, a linear, branched, or cyclic alkyl group having 3 to 10 carbon atoms, a phenyl group, or a substituted phenyl group, and X− represents an anion. Various trifluoromethyl-containing compounds are produced using a method for producing the S-(trifluoromethyl)-benzo[b]thiophenium derivative salt, and using the S-(trifluoromethyl)-benzo[b]thiophenium derivative salt as a trifluoromethylating agent.

    摘要翻译： 可用作药物和农业化学品的合成中间体的三氟甲基噻吩衍生物盐，其制备方法和使用其的含三氟甲基的化合物的制备方法。 S-（三氟甲基） - 苯并[b]噻吩衍生物盐由以下通式（1）表示：其中R 1，R 2，R 3和R 4各自独立地为氢原子，甲基，乙基， 具有3至10个碳原子的直链，支链或环状烷基，甲氧基，乙氧基，具有3-10个碳原子的直链，支链或环状烷氧基，氟原子，氯原子，溴原子 硝基或氰基，R 5为甲基，乙基，碳原子数3〜10的直链状，支链状或环状的烷基，苯基或取代的苯基，X表示 一种阴离子。 使用S-（三氟甲基） - 苯并[b]噻吩衍生物盐的制备方法，使用S-（三氟甲基） - 苯并[b]噻吩衍生物盐作为三氟甲基化剂制备各种含三氟甲基的化合物。

    COATING LAYER FOR SOLAR BATTERIES, AND ITS PRODUCTION PROCESS
    10.
    发明申请
    COATING LAYER FOR SOLAR BATTERIES, AND ITS PRODUCTION PROCESS 审中-公开
    太阳能电池涂层及其生产工艺

    公开(公告)号：US20110256375A1

    公开(公告)日：2011-10-20

    申请号：US12830635

    申请日：2010-07-06

    申请人： Toru YOSHIDA ,  Yasukazu Kishimoto

    发明人： Toru YOSHIDA ,  Yasukazu Kishimoto

    IPC分类号： C08L33/06

    CPC分类号： C03C17/32 ,  C03C17/007 ,  C03C17/3678 ,  C03C17/38 ,  C03C2217/445 ,  C03C2217/478 ,  C03C2217/732 ,  G02B1/105 ,  G02B1/111 ,  G02B1/14 ,  H01L31/0481 ,  Y02E10/50

    摘要： The invention has for its object to coat a single layer form of low-refractive organic thin-film layer on a cover glass of a solar battery to enhance the light-collection efficiency of a solar battery module by a simple method, thereby enhancing the ability of collect sunlight.The invention provides a coating layer for solar batteries which can be formed directly on a protective layer of a solar battery module and used in direct contact with the air. The fluorine-containing coating layer for solar batteries is characterized by having a fluorine content of 5% by weight or greater. This coating layer or protective layer is formed by polymerizing and curing a composition comprising a methacrylate compound and/or an acrylate compound containing a fluoroalkyl group and/or a fluorine-containing polymer dissolved or dispersed in an organic solvent, a fluorine-free organic compound containing 1 to 5 acryloyl groups or methacryloyl groups, and a photo-polymerization initiator, optionally with the addition of fumed silica to it.

    摘要翻译： 本发明的目的是在太阳能电池的盖玻璃上涂覆单层低折射有机薄膜层，以通过简单的方法提高太阳能电池组件的集光效率，从而提高太阳能电池模块的光收集效率 收集阳光。 本发明提供一种能够直接形成在太阳能电池模块的保护层上并用于与空气直接接触的太阳能电池用涂层。 用于太阳能电池的含氟涂层的特征在于氟含量为5重量％以上。 该涂层或保护层通过聚合和固化包含甲基丙烯酸酯化合物和/或含有溶解或分散在有机溶剂中的氟代烷基和/或含氟聚合物的丙烯酸酯化合物，无氟有机化合物 含有1至5个丙烯酰基或甲基丙烯酰基，以及光聚合引发剂，任选地向其中加入热解法二氧化硅。