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    Nanoparticle-textured surfaces and related methods for selective adhesion, sensing and separation
    2.
    发明授权
    Nanoparticle-textured surfaces and related methods for selective adhesion, sensing and separation 有权
    纳米颗粒纹理表面和相关方法用于选择性粘附，感测和分离

    公开(公告)号：US08652640B2

    公开(公告)日：2014-02-18

    申请号：US13749381

    申请日：2013-01-24

    申请人： The University of Massachusetts

    发明人： Maria M. Santore ,  Jun Zhang ,  Vincent Rotello

    IPC分类号： C12M1/00 ,  B82Y5/00 ,  B82Y15/00 ,  C12M1/12 ,  G01N33/543

    CPC分类号： C12M25/16 ,  B82Y5/00 ,  B82Y15/00 ,  G01N33/54333 ,  G01N33/54346 ,  Y10S977/796 ,  Y10S977/81 ,  Y10S977/832 ,  Y10T428/31504 ,  Y10T436/25375

    摘要： The present invention includes an article of manufacture or device, or related system, comprising a heterogeneous surface for selective analyte sensing or separation. Such an article can comprise a surface member and a plurality of spaced components extending therefrom and coupled thereto, such a surface member and spaced components providing a surface heterogeneity selected from different electrostatic interactions, different non-electrostatic interactions and a combination of such interactions, such that the interactions are at least partially sufficient for selective analyte interaction and/or separation. Each such component extension can be of a nanometer dimension about the Debye length of a medium comprising an analyte particle exposed to such a surface. An analyte particle, optionally of a mixture of particles, can be dimensioned from about 30 nm to 20 μm. In some embodiments, the extended components have a density at least partially sufficient for interaction of a single such component or multiple components with a single analyte particle, at a given Debye length. In other embodiments, such components have an average spatial density at least partially sufficient for selective particle interaction and/or separation.

    摘要翻译： 本发明包括制品或装置或相关系统，其包括用于选择性分析物感测或分离的非均匀表面。 这样的制品可以包括表面构件和从其延伸并与其连接的多个间隔的部件，这样的表面构件和间隔的部件提供选自不同的静电相互作用，不同的非静电相互作用和这种相互作用的组合的表面异质性，例如 相互作用至少部分足以用于选择性分析物相互作用和/或分离。 每个这样的部件延伸部可以是包括暴露于这种表面的分析物颗粒的介质的德拜长度的纳米尺寸。 可选的颗粒混合物的分析物颗粒的尺寸可以为约30nm至20μm。 在一些实施方案中，在给定的德拜长度下，延伸的组分具有至少部分足够的单一这样的组分或多个组分与单个分析物颗粒的相互作用的密度。 在其它实施方案中，这些组分具有至少部分足以用于选择性颗粒相互作用和/或分离的平均空间密度。

    Nanoparticle-textured surfaces and related methods for selective adhesion, sensing and separation
    4.
    发明授权
    Nanoparticle-textured surfaces and related methods for selective adhesion, sensing and separation 有权
    纳米颗粒纹理表面和相关方法用于选择性粘附，感测和分离

    公开(公告)号：US08382858B2

    公开(公告)日：2013-02-26

    申请号：US12491851

    申请日：2009-06-25

    申请人： Maria M. Santore ,  Jung Zhang ,  Vincent Rotello

    发明人： Maria M. Santore ,  Jung Zhang ,  Vincent Rotello

    IPC分类号： B01D57/00 ,  B82Y30/00 ,  B82Y5/00 ,  B82Y99/00 ,  B81C99/00

    CPC分类号： C12M25/16 ,  B82Y5/00 ,  B82Y15/00 ,  G01N33/54333 ,  G01N33/54346 ,  Y10S977/796 ,  Y10S977/81 ,  Y10S977/832 ,  Y10T428/31504 ,  Y10T436/25375

    摘要： Textured heterogeneous surfaces and related articles as can be used in conjunction with methods for selective sensing and/or separation. When used for selective particle separation such a system can comprise a heterogeneous surface comprising a surface member and a plurality of components extending therefrom, such components spaced about and having a surface density, with heterogeneity comprising different interactions of the surface member and of the extended components with a particle exposed thereto. Various surface heterogeneities and different interactions can be utilized. However, in certain embodiments, competing electrostatic interactions, or a combination of electrostatic and non-electrostatic interactions, with a particle can be utilized. Such a system can utilize a surface member having a charge difference with respect to the components extending therefrom.

    摘要翻译： 纹理异质表面和相关物品可与选择性感测和/或分离方法结合使用。 当用于选择性颗粒分离时，这种系统可以包括非均质表面，其包括表面部件和从其延伸的多个部件，这些部件间隔开并具有表面密度，其异质性包括表面部件和延伸部件的不同相互作用 其中暴露于其中的颗粒。 可以利用各种表面异质性和不同的相互作用。 然而，在某些实施例中，可以利用与颗粒的竞争静电相互作用或静电和非静电相互作用的组合。 这样的系统可以利用相对于从其延伸的部件具有电荷差的表面部件。

    SELF-DOPED POLYANILINE NANOPARTICLE DISPERSIONS BASED ON BORONIC ACID-PHOSPHATE COMPLEXATION
    6.
    发明申请
    SELF-DOPED POLYANILINE NANOPARTICLE DISPERSIONS BASED ON BORONIC ACID-PHOSPHATE COMPLEXATION 有权
    基于硼酸 - 磷酸盐复合的自聚苯胺纳米粒子分散体

    公开(公告)号：US20110315932A1

    公开(公告)日：2011-12-29

    申请号：US13131052

    申请日：2009-11-25

    申请人： Michael S. Freund ,  Bhavana A. Deore

    发明人： Michael S. Freund ,  Bhavana A. Deore

    IPC分类号： H01B1/12 ,  C08G73/06 ,  C08G75/06 ,  C09D179/04 ,  C09D181/02 ,  B32B5/16 ,  C08G73/02 ,  C09D179/02 ,  B82Y30/00

    CPC分类号： C09D5/08 ,  C08G73/0266 ,  C09D5/24 ,  C09D179/02 ,  Y10S977/773 ,  Y10S977/832 ,  Y10S977/902 ,  Y10T428/2982

    摘要： Poly(anilineboronic acid)/phosphate nanoparticle dispersions are produced in high yields using the reactivity of the boronic acid moiety with phosphate in the presence of fluoride. The poly(anilineboronic acid)/phosphate dispersions have been characterized using spectroscopic, microscopic and electrochemical techniques. According to 11B NMR studies, the formation of anionic tetrahedral boronate group in phosphoric acid in the presence of fluoride forms the basis of self-doped, stabilized PABA nanoparticle dispersion. Transmission electron microscope images show that 25-50 nm diameter PABA nanoparticles are formed under these conditions. UV-vis, FT-IR-ATR spectroscopic and cyclic voltammetric results confirm the formation of the conducting form of PABA. Films produced from these particles exhibit enhanced redox stability and potential dependant conductivity under neutral and basic pH conditions due to the formation of a boron-phosphate complex containing fluoride, which results in a self-doped form of the polymer.

    摘要翻译： 使用硼酸部分与磷酸酯在氟化物存在下的反应性，以高产率制备聚（苯胺硼酸）/磷酸盐纳米颗粒分散体。 聚（苯胺硼酸）/磷酸盐分散体已经使用光谱，显微镜和电化学技术进行表征。 根据11B NMR研究，在氟化物存在下，磷酸中阴离子四面体硼酸酯基团的形成形成了自掺杂稳定的PABA纳米粒子分散体的基础。 透射电子显微镜图像显示在这些条件下形成直径25-50nm的PABA纳米颗粒。 UV-vis，FT-IR-ATR光谱和循环伏安结果证实形成了导电形式的PABA。 由于形成含氟化物的磷酸硼配合物，这些颗粒在中性和碱性pH条件下表现出增强的氧化还原稳定性和电位依赖性电导率，这导致聚合物的自掺杂形式。