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    4-jod-2[N-(N-alkyl-aminocarbonyl)-aminosulfonyl]-benzoic acid methyl ester and derivatived thereof and method for their production
    2.
    发明授权
    4-jod-2[N-(N-alkyl-aminocarbonyl)-aminosulfonyl]-benzoic acid methyl ester and derivatived thereof and method for their production 有权
    4-氨基-2- [N-（N-烷基 - 氨基羰基） - 氨基磺酰基] - 苯甲酸甲酯并衍生并制备

    公开(公告)号：US6147248A

    公开(公告)日：2000-11-14

    申请号：US214041

    申请日：1998-12-23

    申请人： Lothar Willms ,  Harald Knorr

    发明人： Lothar Willms ,  Harald Knorr

    IPC分类号： C07C303/40 ,  C07C311/16 ,  C07C311/37 ,  C07C311/39 ,  C07C311/53 ,  C07C311/58 ,  C07C311/59 ,  C07C311/18

    CPC分类号： C07C311/58 ,  C07C311/37

    摘要： The invention relates to compounds of the formula (I) ##STR1## in which R=(subst.) alkyl or (subst.) cycloalkyl, which are suitable as intermediates for preparing herbicidal sulfonylureas. According to the invention, the compounds (I) are prepared by(a) diazotizing a compound of the formula (II) ##STR2## in the presence of an acid H.sup.+ X.sup.-, where X.sup.- is an equivalent of an anion, to give the novel compounds (diazonium salts) of the formula (III) ##STR3## (b) reacting the compound of the formula (III) in the presence of iodide ions to give the compound (IV) and ##STR4## (c) reacting the compound of the formula (IV) with an isocyanate of the formula (V)R--N.dbd.C.dbd.O (V)in which R is as defined in formula (I), to give the compound of the formula (I).

    摘要翻译： PCT No.PCT / EP97 / 03170 Sec。 371日期1998年12月23日第 102（e）1998年12月23日日期PCT 1997年6月18日PCT公布。 公开号WO98 / 00396 日本1998年1月8日本发明涉及式（I）化合物，其中R =（低级）烷基或（低级）环烷基，其适用作制备除草磺酰脲类的中间体。 根据本发明，化合物（I）通过（a）在酸H + X-存在下重氮化式（II）的化合物来制备，其中X-是阴离子当量，得到新颖的 式（III）化合物（重氮盐）（b）在碘离子存在下使式（Ⅲ）化合物反应，得到化合物（Ⅳ）和（ⅲ）使式（Ⅳ）化合物与式 式（Ⅴ）的异氰酸酯RN = C = O（Ⅴ）其中R如式（Ⅰ）所定义，得到式（Ⅰ）化合物。

    N-phenylsulfonyl-N'-pyrimidinylureas
    7.
    发明授权
    N-phenylsulfonyl-N'-pyrimidinylureas 失效
    N-苯基磺酰基-N'-吡啶二酮

    公开(公告)号：US5104440A

    公开(公告)日：1992-04-14

    申请号：US697178

    申请日：1991-05-08

    申请人： Willy Meyer ,  Dieter Reinehr ,  Konrad Oertle ,  Rolf Schurter

    发明人： Willy Meyer ,  Dieter Reinehr ,  Konrad Oertle ,  Rolf Schurter

    IPC分类号： B01J31/24 ,  A01N47/36 ,  A01P13/00 ,  C07B61/00 ,  C07C303/22 ,  C07C309/29 ,  C07C309/30 ,  C07C309/44 ,  C07C309/86 ,  C07C309/87 ,  C07C311/15 ,  C07C311/16 ,  C07C311/29 ,  C07C311/53 ,  C07C311/54 ,  C07C311/58 ,  C07C311/65 ,  C07C317/10 ,  C07D239/42 ,  C07D239/46 ,  C07D239/47 ,  C07D239/52 ,  C07D239/69 ,  C07D251/16 ,  C07D251/42 ,  C07D251/46 ,  C07D251/52 ,  C07D521/00

    CPC分类号： C07C311/65 ,  A01N47/36 ,  C07C309/00 ,  C07D239/47 ,  C07D521/00

    摘要： The invention relates to N-phenylsulfonyl-N'-pyrimidinylureas and N-phenylsulfonyl-N-triazinylures of the general formula ##STR1## wherein R.sub.1 is hydrogen, halogen, nitro, amino, C.sub.1 -C.sub.5 alkyl, C.sub.1 -C.sub.4 haloalkyl or a --Q--R.sub.7, --CO--OR.sub.8 or --(CO).sub.n --NR.sub.9 R.sub.10 radical,R.sub.2 is hydrogen, C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy, C.sub.1 -C.sub.4 alkylthio, C.sub.1 -C.sub.4 haloalkyl, C.sub.1 -C.sub.4 haloalkoxy, halogen or alkoxyalkyl containing not more than 4 carbon atoms,R.sub.3 is C.sub.2 -C.sub.10 alkenyl which is substituted by one or more fluorine or bromine atoms or by one or more hydroxyl, cyano, nitro, --(Y).sub.m --CO--(Z).sub.n --R.sub.8, --SO.sub.2 --NR.sub.11 R.sub.12, --S(O).sub.P --C.sub.1 -C.sub.3 haloalkyl or --S(O).sub.n --C.sub.1 -C.sub.3 alkyl groups and which may additionally be substituted by one or more chlorine atoms,R.sub.4 is C.sub.1 -C.sub.3 alkyl, C.sub.1 -C.sub.3 haloalkyl, C.sub.1 -C.sub.3 haloalkyl, C.sub.1 -C.sub.3 alkoxy or C.sub.1 -C.sub.3 haloalkoxy,R.sub.5 is hydrogen, halogen, --NR.sub.13 R.sub.14, C.sub.1 -C.sub.3 alkyl, C.sub.1 -C.sub.3 haloalkyl, C.sub.1 -C.sub.3 alkoxy or C.sub.1 -C.sub.2 haloalkoxy,R.sub.6 is hydrogen, C.sub.1 -C.sub.3 alkyl or C.sub.1 -C.sub.3 alkoxy,X is oxygen or sulfur, andE is nitrogen or the methine group, and R.sub.7 is C.sub.1 -C.sub.4 alkyl which is substituted by halogen or C.sub.1 -C.sub.3 alkoxy or is C.sub.3 -C.sub.5 alkenyl,R.sub.8 is C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 haloalkyl or C.sub.2 -C.sub.6 alkoxyalkyl, R.sub.9, R.sub.10, R.sub.11, R.sub.12, R.sub.13 and R.sub.14, each independently of the other, are hydrogen or C.sub.1 -C.sub.3 alkyl,Q is oxygen, sulfur, the sulfinyl or sulfonyl bridge,Y is oxygen, sulfur or --NR.sub.16 --, wherein R.sub.16 is hydrogen or C.sub.1 -C.sub.3 alkyl,Z is oxygen, sulfur or --NR.sub.17 --, wherein R.sub.17 is hydrogen or C.sub.1 -C.sub.3 alkyl, m and n are each 0 or 1, andp is 0, 1 or 2, and to the salts of these compounds with amines, alkali metal bases or alkaline earth metal bases.These compounds have good pre- and postemergence selective herbicidal and growth regulating properties.

    N-phenylsulfonyl-N'-pyrimidinyl-ureas and N-phenyl-sulfonyl-N'-triazinyl ureas
    8.
    发明授权
    N-phenylsulfonyl-N'-pyrimidinyl-ureas and N-phenyl-sulfonyl-N'-triazinyl ureas 失效
    N-苯基磺酰基-N'-嘧啶基脲和N-苯基 - 磺酰基-N'-三嗪基脲

    公开(公告)号：US5041603A

    公开(公告)日：1991-08-20

    申请号：US464578

    申请日：1990-01-12

    申请人： Willy Meyer ,  Dieter Reinehr ,  Konrad Oertle ,  Rolf Schurter

    发明人： Willy Meyer ,  Dieter Reinehr ,  Konrad Oertle ,  Rolf Schurter

    IPC分类号： B01J31/24 ,  A01N47/36 ,  A01P13/00 ,  C07B61/00 ,  C07C303/22 ,  C07C309/29 ,  C07C309/30 ,  C07C309/44 ,  C07C309/86 ,  C07C309/87 ,  C07C311/15 ,  C07C311/16 ,  C07C311/29 ,  C07C311/53 ,  C07C311/54 ,  C07C311/58 ,  C07C311/65 ,  C07C317/10 ,  C07D239/42 ,  C07D239/46 ,  C07D239/47 ,  C07D239/52 ,  C07D239/69 ,  C07D251/16 ,  C07D251/42 ,  C07D251/46 ,  C07D251/52 ,  C07D521/00

    CPC分类号： C07C311/65 ,  A01N47/36 ,  C07C309/00 ,  C07D239/47 ,  C07D521/00

    摘要： The invention relates to N-phenylsulfonyl-N'-pyrimidinylureas and N-phenylsulfonyl-N-triazinylureas of the general formula ##STR1## wherein R.sub.1 is hydrogen, halogen, nitro, amino, C.sub.1 -C.sub.5 alkyl, C.sub.1 -C.sub.4 haloalkyl or a --Q--R.sub.7, --CO--OR.sub.8 or --(CO).sub.n --NR.sub.9 R.sub.10 radical,R.sub.2 is hydrogen, C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy, C.sub.1 -C.sub.4 alkylthio, C.sub.1 -C.sub.4 haloalkyl, C.sub.1 -C.sub.4 haloalkoxy, halogen or alkoxyalkyl containing not more than 4 carbon atoms,R.sub.3 is C.sub.2 -C.sub.10 alkenyl which is substituted by one or more fluorine or bromine atoms or by one or more hydroxyl, cyano, nitro, --(Y).sub.m --CO--(Z).sub.n --R.sub.8, --SO.sub.2 --NR.sub.11 R.sub.12, --S(O).sub.p --C.sub.1 -C.sub.3 haloalkyl or --S(O).sub.n --C.sub.1 -C.sub.3 alkyl groups and which may additionally be substituted by one or more chlorine atoms,R.sub.4 is C.sub.1 -C.sub.3 alkyl, C.sub.1 -C.sub.3 haloalkyl, C.sub.1 -C.sub.3 alkoxy or C.sub.1 -C.sub.3 haloalkoxy,R.sub.5 is hydrogen, halogen, --NR.sub.13 R.sub.14, C.sub.1 -C.sub.3 alkyl, C.sub.1 -C.sub.3 haloalkyl, C.sub.1 -C.sub.3 alkoxy or C.sub.1 -C.sub.2 haloalkoxy,R.sub.6 is hydrogen, C.sub.1 -C.sub.3 alkyl or C.sub.1 -C.sub.3 alkoxy,X is oxygen or sulfur, andE is nitrogen or the methine group, andR.sub.7 is C.sub.1 -C.sub.4 alkyl which is substituted by halogen or C.sub.1 -C.sub.3 alkoxy or is C.sub.3 -C.sub.5 alkenyl,R.sub.8 is C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 haloalkyl or C.sub.2 -C.sub.6 alkoxyalkyl,R.sub.9, R.sub.10, R.sub.11, R.sub.12, R.sub.13 and R.sub.14, each independently of the other, are hydrogen or C.sub.1 -C.sub.3 alkyl,Q is oxygen, sulfur, the sulfinyl or sulfonyl bridge,Y is oxygen, sulfur or --NR.sub.16 --, wherein R.sub.16 is hydrogen or C.sub.1 -C.sub.3 alkyl,Z is oxygen, sulfur or --NR.sub.17 --, wherein R.sub.17 is hydrogen or C.sub.1 -C.sub.3 alkyl,m and n are each 0 or 1, andp is 0, 1 or 2, and to the salts of these compounds with amines, alkali metal bases or alkaline earth metal bases.These compounds have good pre- and postemergence selective herbicidal and growth regulating properties.