Method for producing powder for magnet
    126.
    发明授权
    Method for producing powder for magnet 有权
    磁铁粉末制造方法

    公开(公告)号:US09435012B2

    公开(公告)日:2016-09-06

    申请号:US14979111

    申请日:2015-12-22

    Inventor: Toru Maeda

    Abstract: Provided are a method for producing powder for a magnet, and methods for producing a powder compact, a rare-earth-iron-based alloy material, and a rare-earth-iron-nitrogen-based alloy material. Magnetic particles constituting the powder each have a texture in which grains of a phase of a hydride of a rare-earth element are dispersed in a phase of an iron-containing material. The uniform presence of the phase of the iron-containing material in each magnetic particle results in powder having excellent formability, thereby providing a powder compact having high relative density. The powder is produced by heat-treating rare-earth-iron-based alloy powder in a hydrogen atmosphere to separate the rare-earth element and the iron-containing material and then forming a hydride of the rare-earth element. The powder is compacted. The powder compact is heat-treated in vacuum to form a rare-earth-iron-based alloy material. The rare-earth-iron-based alloy material is heat-treated in a nitrogen atmosphere to form a rare-earth-iron-nitrogen-based alloy material.

    Abstract translation: 提供一种用于制造用于磁体的粉末的方法,以及制造粉末压块,稀土 - 铁基合金材料和稀土 - 铁 - 氮基合金材料的方法。 构成粉末的磁性颗粒各自具有将稀土元素的氢化物的相的粒子分散在含铁材料的相中的结构。 每个磁性颗粒中含铁材料相的均匀存在导致具有优异成形性的粉末,从而提供具有高相对密度的粉末压块。 通过在氢气氛中热处理稀土 - 铁基合金粉末来分离稀土元素和含铁材料,然后形成稀土元素的氢化物来制造粉末。 粉末被压实。 粉末压片在真空中热处理以形成稀土 - 铁基合金材料。 稀土 - 铁基合金材料在氮气气氛中进行热处理,形成稀土 - 铁 - 氮基合金材料。

    METHOD FOR PREPARING ULTRA-LONG-TUBE TYPE FINE-GRAIN MOLYBDENUM TUBE TARGET
    130.
    发明申请
    METHOD FOR PREPARING ULTRA-LONG-TUBE TYPE FINE-GRAIN MOLYBDENUM TUBE TARGET 审中-公开
    制备超长管型精细粒度多晶管目标的方法

    公开(公告)号:US20160177437A1

    公开(公告)日:2016-06-23

    申请号:US14759547

    申请日:2014-06-19

    Inventor: Lingjie ZHANG

    Abstract: A method for preparing an ultra-long-tube type fine-grain molybdenum tube target uses molybdenum powder with the purity being greater than 3N to prepare a target tube with a uniform wall thickness, where the length is 1700-2700 mm; the diameter is greater than 150 mm; and the wall thickness is 15-40 mm. The method includes: taking molybdenum powder, feeding the molybdenum powder into a film, molding by static pressing, placing in a medium frequency furnace, performing hydrogen sintering to form a tube blank, placing into a mold, forging the mold of a tube target, placing into tempering furnace, annealing, forming fine-grain structures, fine processing, washing, and drying to prepare a molybdenum tube target. The method overcomes defects of a sintering process and a forging process, and relates to simple processes, easy industrial production and control, reduced pollution, reduced cost, improved quality, and remarkably improved production efficiency.

    Abstract translation: 制造超长管状细粒钼管靶的方法使用纯度大于3N的钼粉末制备壁厚均匀的靶管,长度为1700〜2700mm; 直径大于150毫米; 壁厚为15-40mm。 该方法包括:将钼粉末,钼粉进料成膜,静压成型,放入中频炉中,进行氢烧结,形成管坯,放入模具中,锻造管靶的模具, 放入回火炉中,退火,形成细晶粒结构,精加工,洗涤和干燥以制备钼管靶。 该方法克服了烧结过程和锻造过程的缺陷,涉及工艺简单,工业生产控制简单,污染减少,成本降低,质量提高,生产效率显着提高。

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