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公开(公告)号：US12017207B2
公开(公告)日：2024-06-25
申请号：US18059712
申请日：2022-11-29
发明人： Lianhui Ding , Khalid Otaibi , Faisal Alotaibi
IPC分类号： B01J29/70 , B01J35/23 , B01J35/61 , B01J35/63 , B01J35/64 , B01J37/00 , B01J37/02 , B01J37/03 , B01J37/04 , B01J37/06 , C01B39/48
CPC分类号： B01J29/7007 , B01J35/23 , B01J35/615 , B01J35/617 , B01J35/635 , B01J35/638 , B01J35/647 , B01J37/0018 , B01J37/0236 , B01J37/03 , B01J37/04 , B01J37/06 , C01B39/48 , C01P2004/03 , C01P2004/64 , C01P2006/12 , C01P2006/14 , C01P2006/16
摘要： Methods for synthesizing a mesoporous nano-sized zeolite beta are described. The method may include mixing an aqueous base solution with hexadecyltrimethylammonium bromide (CTAB) to form a first solution; adding nano-sized zeolite particles having a particle size of less than or equal to 100 nm to the first solution to form a second solution. The nano-sized zeolite particles include a microporous framework with a plurality of micropores having diameters of less than or equal to 2 nm and a BEA framework type. The method may further include transferring the second solution to an autoclave operated at 25° C. to 200° C. for 3 to 24 hours to form a colloid; drying the colloid at 100° C. to 200° C. for 8 to 36 hours without washing the colloid to form a zeolite precursor; and calcining the zeolite precursor at 250° C. to 600° C. for 1 to 8 hours to form the mesoporous nano-sized zeolite beta.
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公开(公告)号：US12006482B2
公开(公告)日：2024-06-11
申请号：US18144427
申请日：2023-05-08
CPC分类号： C10G67/06 , C10G25/003 , C10G25/12 , C10G45/00 , C10G47/00 , C10G2300/107 , C10G2300/206 , C10G2300/301 , C10G2300/4025 , C10G2300/44 , C10G2300/708 , C10G2400/18 , C10G2400/20
摘要： A system for upgrading heavy hydrocarbon feeds, such as crude oil, include a hydrotreating unit, a hydrotreated effluent separation system, a solvent-assisted adsorption system, and a hydrocracking unit. Processes for upgrading heavy hydrocarbon feeds include hydrotreating the hydrocarbon feed to produce a hydrotreated effluent that includes asphaltenes, separating the hydrotreated effluent into a lesser boiling hydrotreated effluent and a greater boiling hydrotreated effluent comprising the asphaltenes, combining the greater boiling hydrotreated effluent with a light paraffin solvent to produce a combined stream, adsorbing the asphaltenes from the combined stream to produce an adsorption effluent, and hydrocracking the lesser boiling hydrotreated effluent and at least a portion of the adsorption effluent to produce a hydrocracked effluent with hydrocarbons boiling less than 180° C. The systems and processes increase the hydrocarbon conversion and yield of hydrocarbons boiling less than 180° C.
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公开(公告)号：US20240173702A1
公开(公告)日：2024-05-30
申请号：US18059733
申请日：2022-11-29
发明人： Faisal Alotaibi , Lianhui Ding
IPC分类号： B01J29/08 , B01J35/00 , B01J35/10 , B01J37/00 , B01J37/04 , B01J37/08 , B01J37/30 , C01B39/08 , C01B39/24
CPC分类号： B01J29/084 , B01J35/0013 , B01J35/1023 , B01J35/1038 , B01J35/1061 , B01J37/009 , B01J37/04 , B01J37/08 , B01J37/30 , C01B39/08 , C01B39/24 , B01J2029/081 , B01J2229/16 , B01J2229/32 , C01P2004/64 , C01P2006/12 , C01P2006/14 , C01P2006/16
摘要： Methods for synthesizing a mesoporous nano-sized ultra-stable Y zeolite include combining a microporous Y zeolite having a SiO2/Al2O3 molar ratio of less than 5.2 with water to form a microporous Y zeolite slurry and heating the microporous Y zeolite slurry to 30° C. to 100° C. to form a heated microporous Y zeolite slurry. Further the method includes adding a 0.1M to 2.0M ammonium hexafluorosilicate solution and a 0.1M to 2.0M ammonium hydroxide solution in a drop-wise manner, either sequentially or simultaneously, to the heated microporous Y zeolite slurry to form a treated zeolite solution and holding the treated zeolite solution at 50° C. to 100° C. Finally the method includes filtering and washing the dealuminated solution with water to form an ultra-stable Y zeolite precursor, drying the ultra-stable Y zeolite precursor, and calcining the dried zeolite precursor to form the nano-sized ultra-stable Y zeolite.
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14.发明公开公开(公告)号：US20240139720A1
公开(公告)日：2024-05-02
申请号：US18051910
申请日：2022-11-02
发明人： Lianhui Ding , Faisal Alotaibi
IPC分类号： B01J29/78 , B01J21/04 , B01J29/08 , B01J29/80 , B01J35/10 , B01J37/00 , B01J37/03 , B01J37/04 , B01J37/08 , C10G47/20
CPC分类号： B01J29/7815 , B01J21/04 , B01J29/084 , B01J29/80 , B01J35/1019 , B01J35/1038 , B01J35/1042 , B01J35/1061 , B01J37/0018 , B01J37/031 , B01J37/04 , B01J37/08 , C10G47/20 , B01J2029/062
摘要： This disclosure generally relates to methods for producing catalyst compositions, which may include forming a precursor solution comprising a silicon-containing material, an aluminum-containing material, and a quaternary amine, hydrothermally treating the precursor solution at a first temperature to form an intermediate mixture, hydrothermally treating the intermediate mixture at a second temperature to form beta zeolite, wherein the first temperature is less than the second temperature by at least 200° C., forming an extrudable mixture comprising the beta zeolite, alumina, a metal precursor, and a binder, extruding the extrudable mixture to form extrudates, and calcining the extrudates to form the catalyst composition.
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公开(公告)号：US11866651B1
公开(公告)日：2024-01-09
申请号：US18053800
申请日：2022-11-09
发明人： Mansour Ali Al Herz , Aaron Akah , Qi Xu , Lianhui Ding , Bander A. Al Ghamdi
IPC分类号： C10G11/05 , C10G69/04 , B01J29/40 , B01J29/80 , B01J21/16 , B01J21/08 , C10G45/02 , B01J29/08 , B01J37/00 , B01J37/02 , B01J35/00 , B01J29/06
CPC分类号： C10G11/05 , B01J21/08 , B01J21/16 , B01J29/088 , B01J29/40 , B01J29/80 , B01J35/0006 , B01J37/0009 , B01J37/0201 , C10G45/02 , C10G69/04 , B01J2029/062 , B01J2229/18 , B01J2229/20 , B01J2229/42 , C10G2300/1033 , C10G2300/301 , C10G2300/308 , C10G2300/4006 , C10G2300/4018 , C10G2300/4025 , C10G2300/70 , C10G2400/20
摘要： A process for converting crude oil may comprise contacting a crude oil with one or more hydroprocessing catalysts to produce a hydroprocessed effluent and contacting the hydroprocessed effluent with a fluidized catalytic cracking (FCC) catalyst composition in an FCC system to produce cracked effluent comprising at least olefins. The crude oil may have an API gravity from 30 to 35. The FCC system may operate at a temperature of greater than or equal to 580° C., a weight ratio of the FCC catalyst composition to the crude oil of from 2:1 to 10:1, and a residence time of from 0.1 seconds to 60 seconds. The FCC catalyst composition may comprise ultrastable Y-type zeolite (USY zeolite) impregnated with lanthanum; ZSM-5 zeolite impregnated with phosphorous; an alumina binder; colloidal silica; and a matrix material comprising Kaolin clay.
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16.发明授权公开(公告)号：US11365358B2
公开(公告)日：2022-06-21
申请号：US16879948
申请日：2020-05-21
发明人： Emad Naji Al-Shafei , Mohammed Z. Al-Bahar , Manal Al-Eid , Lianhui Ding , Ali Nader Al-Jishi , Ki-Hyouk Choi
摘要： An integrated process for conversion of a hydrocarbon stream comprising light naphtha to enhanced value products. The process includes passing the hydrocarbon stream through a first reactor, the first reactor being a catalytic bed reactor with a dual-function catalyst to simultaneously reform light naphtha to BTEX and crack light naphtha to ethane, propane, and butanes. Further, the process includes passing an effluent of the first reactor to a gas-liquid separating unit to generate a liquid stream and a gas stream, and passing the gas stream to a gas separator unit to remove hydrogen gas and methane and generate an enhanced gas stream. The process further includes passing the enhanced gas stream through a second reactor, the second reactor being a pyrolysis unit operated at steam cracking conditions to convert ethane, propane, and butanes in the enhanced gas stream to light. An associated system for performing the process is also provided wherein the integrated process does not include passage of a process stream to a separate and independent hydrocracking unit to crack light alkanes in the hydrocarbon stream to smaller alkanes.
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公开(公告)号：US11247196B2
公开(公告)日：2022-02-15
申请号：US16703405
申请日：2019-12-04
发明人： Donya Alsewdan , Lianhui Ding , Manal Al-Eid
IPC分类号： B01J29/40 , B01J29/44 , B01J35/10 , B01J37/00 , B01J37/02 , B01J37/03 , B01J37/04 , B01J37/06 , B01J37/08 , B01J37/30 , B01J29/064 , B01J37/10 , B01J29/06 , B01J29/42 , B01J29/068 , C01B39/36 , C01B39/02 , C01B39/40 , C01B39/04
摘要： A method of making a zeolite with encapsulated platinum is provided. The method includes dissolving an aluminum source in water to form a first solution, dissolving a hydroxide in water to form a second solution, dissolving a templating agent in water to form a third solution, and adding a silica source to the first solution to form a fourth solution. The method further includes adding the second solution to the fourth solution to form a fifth solution, adding the third solution to the fifth solution to form a sixth solution, and adding a platinum source to the sixth solution. The sixth solution is crystallized to form a solid product, which is recovered. The solid product is calcined. An ammonium ion exchange is performed on the solid product to form a second solid product, and the second solid product is calcined.
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公开(公告)号：US20210156830A1
公开(公告)日：2021-05-27
申请号：US16696828
申请日：2019-11-26
发明人： Manal Al-Eid , Lianhui Ding
摘要： Examples described herein provide a method for characterizing a catalyst in a chemisorption unit. The method includes treating a catalyst sample with gas blend comprising ammonia in an inert gas and performing a first temperature programmed desorption (TPD) to desorb the ammonia from the catalyst sample. A temperature programmed reduction (TPR) of the catalyst sample is performed with hydrogen. The catalyst sample is treated after the TPR with a gas blend comprising ammonia in an inert gas. A second temperature programmed desorption is performed to desorb the ammonia from the catalyst sample.
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公开(公告)号：US10793792B2
公开(公告)日：2020-10-06
申请号：US15799338
申请日：2017-10-31
发明人： Lianhui Ding , Essam Al-Sayed , Sherif Mohamed , Ibrahim Al-Nutaifi , Alberto Lozano Ballesteros , Ibrahim Abba
摘要： According to one or more embodiments presently described, a feedstock oil may be processed by a method which may include hydrotreating the feedstock oil to reduce or remove one or more of sulfur content, metals content, nitrogen content, or aromatics content to produce a hydrotreated oil stream; separating at least a portion of the hydrotreated oil stream into a at least a lesser boiling point oil fraction stream and a greater boiling point oil fraction stream in a first separator; hydrocracking the greater boiling point oil fraction stream; and steam cracking the lesser boiling point oil fraction stream.
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公开(公告)号：US10696910B2
公开(公告)日：2020-06-30
申请号：US16036283
申请日：2018-07-16
IPC分类号： C10G67/02 , B01J35/10 , C10G47/20 , C10G45/08 , C10G69/04 , C10G53/02 , C10G57/00 , C10G65/10 , C10G69/02 , C10G69/06 , C10G65/12
摘要： According to one embodiment, a heavy oil may be processed by a method that may include upgrading at least a portion of the heavy oil to form an upgraded oil, where the upgrading comprises contacting the heavy oil with a hydrodemetalization catalyst, a transition catalyst, a hydrodenitrogenation catalyst, and a hydrocracking catalyst to remove at least a portion of metals, nitrogen, or aromatics content from the heavy oil and form the upgraded oil. The method may further include passing at least a portion of the upgraded oil to a separation device that separates the upgraded oil into one or more transportation fuels; and where the final boiling point of the upgraded oil is less than or equal to 540° C.
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