Method of fabricating scanning tunneling microscope tips
    254.
    发明授权
    Method of fabricating scanning tunneling microscope tips 失效
    扫描隧道显微镜尖端的制造方法

    公开(公告)号:US5085746A

    公开(公告)日:1992-02-04

    申请号:US579892

    申请日:1990-09-10

    Abstract: A method of fabricating a double-tapered scanning tunneling microscope comprises (a) immersing one end of the tip in a bath of an acidic aqueous etchant solution containing an alkaline earth salt, with the wire positioned substantially perpendicularly to the surface of the solution; and (b) etching the wire at about 25 volts root mean squared (rms) alternating current (ac) until a double-tapered tip is formed thereon. The etching step is preferably followed by a polishing step which comprises (c) providing a thin film of a second acidic aqueous etchant solution containing an alkaline earth salt; then (d) contacting said electrode tip to the thin film: and then (e) etching the tip at about 2 volts rms ac to thereby polish the tip.Also disclosed is a method inhibiting the formation of carbon on a scanning tunneling microscope tip which comprises (a) positioning a wire in an etchant solution and then (b) etching the wire while excluding carbon dioxide therefrom.Double-tapered scanning tunneling microscope tip comprised of an elongate wire and methods of using the same are also disclosed.

    Abstract translation: 制造双锥形扫描隧道显微镜的方法包括(a)将尖端的一端浸入含有碱土盐的酸性含水蚀刻剂溶液的浴中,其中丝线基本上垂直于溶液的表面定位; 并且(b)以约25伏的均方根(rms)交流电(ac)蚀刻线,直到其上形成双锥形尖端。 优选的蚀刻步骤之后是抛光步骤,其包括(c)提供含有碱土金属盐的第二酸性水性蚀刻剂溶液的薄膜; 然后(d)使所述电极尖端接触所述薄膜:然后(e)以约2伏rms ac蚀刻所述尖端,从而抛光所述尖端。 还公开了一种抑制扫描隧道显微镜尖端上形成碳的方法,其包括(a)将线定位在蚀刻剂溶液中,然后(b)在不排除二氧化碳的情况下蚀刻线。 还公开了由细长线组成的双锥形扫描隧道显微镜尖端及其使用方法。

    Electron impact ion source with field emission cathode
    255.
    发明授权
    Electron impact ion source with field emission cathode 失效
    具有场致发射阴极的电子冲击离子源

    公开(公告)号:US4272699A

    公开(公告)日:1981-06-09

    申请号:US18646

    申请日:1979-03-08

    CPC classification number: H01J9/025 H01J1/304 H01J2201/30457

    Abstract: A field emission cathode affording multiple emitting points, formed by a tiplicity of carbon fibers mounted on a conductive base, preferably in spaced clusters of about one thousand or more fibers, and projecting from the base to afford a multiplicity of emission points at the fiber tips. The fibers are in a range of diameters of about two to ten microns. As applied to an electron impact ion source for an instrument such as a mass spectrometer or molecular beam detector, the cathode is of annular configuration, incorporated in an electrode assembly comprising, radially inwardly of the assembly, the cathode, an extraction grid, a retardation grid and an ionization cage.

    Abstract translation: 提供多个发射点的场发射阴极,其由安装在导电基底上的多个碳纤维形成,优选地具有约一千个或更多个纤维的间隔开的簇,并且从基底突出以在纤维尖端处提供多个发射点 。 纤维的直径范围约为2至10微米。 当应用于诸如质谱仪或分子束检测器的仪器的电子冲击离子源时,阴极是环形结构,并入电极组件中,包括在组件的径向内部,阴极,提取栅格,延迟 栅格和电离笼。

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