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公开(公告)号：US07968750B2
公开(公告)日：2011-06-28
申请号：US12676188
申请日：2008-08-27
IPC分类号： C07C209/50
CPC分类号： B01J25/00 , B01J37/009 , C07C209/50 , C07C211/07 , C07C211/08
摘要： The present invention relates to a process for producing a tertiary amine by reducing an amide compound in the presence of a catalyst containing a sponge copper catalyst obtained by leaching alloy particles containing copper and aluminum and drying the thus leached alloy particles. The present invention provides a process for producing high-purity aliphatic tertiary amines containing a less amount of by-products at a high yield by subjecting aliphatic acid amides to hydrogenation reduction under solvent-free moderate conditions.
摘要翻译： 本发明涉及在含有通过浸出含有铜和铝的合金颗粒并干燥所浸出的合金颗粒而获得的海绵铜催化剂的催化剂存在下还原酰胺化合物来制备叔胺的方法。 本发明提供了一种通过在无溶剂的中等条件下使脂族酸酰胺进行氢化还原来生产高产率的含有少量副产物的高纯度脂族叔胺的方法。
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公开(公告)号：US07935846B2
公开(公告)日：2011-05-03
申请号：US12520739
申请日：2007-10-17
IPC分类号： C07C209/78 , C07C291/04
CPC分类号： C07C209/50 , B01J21/10 , B01J23/002 , B01J23/78 , B01J23/80 , B01J23/8926 , B01J23/8946 , B01J29/06 , B01J29/072 , B01J29/143 , B01J37/03 , B01J2523/00 , C07C211/08 , B01J2523/17 , B01J2523/22 , B01J2523/23 , B01J2523/25 , B01J2523/824 , B01J2523/27
摘要： The present invention provides a process for producing high-purity aliphatic tertiary amines containing a less amount of by-products by using a chromium-free catalyst with a good productivity in an economically advantageous manner. The present invention relates to a process for producing a tertiary amine by reducing an amide compound in the presence of a catalyst containing copper and magnesium at a molar ratio of magnesium to copper (magnesium/copper) of from 0.01 to 20.
摘要翻译： 本发明提供一种以经济上有利的方式通过使用无铬催化剂以高生产率生产含少量副产物的高纯度脂族叔胺的方法。 本发明涉及一种通过在含有铜与镁（镁/铜）摩尔比为0.01〜20的铜和镁的催化剂存在下还原酰胺化合物来制备叔胺的方法。
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公开(公告)号：US20090054677A1
公开(公告)日：2009-02-26
申请号：US12281152
申请日：2007-02-27
IPC分类号： C07C253/00
CPC分类号： C07C253/22 , C07C211/07 , C07C211/21 , C07C255/03 , C07C255/07
摘要： The present invention relates to a process for producing an aliphatic nitrile, including the step of reacting at least one compound selected from the group consisting of an aliphatic monocarboxylic acid, an aliphatic dicarboxylic acid and alkyl esters of these acids containing an alkyl group having 1 to 5 carbon atoms, with ammonia in the presence of a compound of at least one metal selected from the group consisting of zinc, cobalt, titanium and aluminum, and a sulfonic acid compound! and a process for producing an aliphatic amine, including the step of subjecting the aliphatic nitrile produced by the above process to hydrogenation reaction in the presence of a hydrogenation catalyst. There are provided an industrially advantageous process for producing an aliphatic nitrile with a high reactivity; and a process for producing an aliphatic amine using the aliphatic nitrile as a raw material.
摘要翻译： 本发明涉及一种生产脂族腈的方法，包括使选自脂肪族一元羧酸，脂族二羧酸和含有1个烷基的酸的烷基酯中的至少一种化合物与至少一种选自下列化合物的化合物反应的步骤： 在含有选自锌，钴，钛和铝的至少一种金属的化合物和磺酸化合物的存在下，使氨与5个碳原子一起使用。 以及脂肪族胺的制造方法，其特征在于，在氢化催化剂的存在下，使由上述方法制造的脂肪族腈进行氢化反应的工序。 提供了一种工业上有利的生产具有高反应性的脂族腈的方法; 以及使用脂肪族腈作为原料的脂族胺的制造方法。
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公开(公告)号：US06737050B2
公开(公告)日：2004-05-18
申请号：US10026641
申请日：2001-12-27
申请人： Yasuhiro Doi , Keiko Hasebe , Hiroyuki Masuda , Tetsuaki Fukushima , Uichiro Nishimoto , Hiroshi Abe
发明人： Yasuhiro Doi , Keiko Hasebe , Hiroyuki Masuda , Tetsuaki Fukushima , Uichiro Nishimoto , Hiroshi Abe
IPC分类号： A61K7075
CPC分类号： A61K8/898 , A61K8/416 , A61K8/44 , A61K8/463 , A61K8/60 , A61K8/73 , A61K8/891 , A61Q5/00 , A61Q5/02 , A61Q5/12
摘要： Provided are a hair cosmetic composition comprising an ether type cationic surfactant represented by the following formula (1): wherein, R1 represents a linear or branched C6-24 alkyl or alkenyl group, R2 and R4 each represents a C1-6 alkyl group or —(AO)nH (A: a C2-4 alkylene group, n: a number of from 1 to 6 with the proviso that n pieces of A may be the same or different and their sequence is optional), R3 represents a C1-6 alkyl group or —(A′O)mH (A′: a C2-4 alkylene group, m: a number of from 1 to 6 with the proviso that m pieces of A may be the same or different and their sequence is optional), and X− represents an anion; a hair cleansing composition containing the cationic surfactant(1); and a method of treating hair with these compositions. The hair cosmetic composition of the present invention can impart good flexibility and smoothness to hair not only when it is wetted but also after drying. When used as a hair cleansing composition, it provides excellent quality of foam and feeling upon use and exhibits good low-temperature stability.
摘要翻译： 提供一种包含由下式（1）表示的醚型阳离子表面活性剂的毛发化妆品组合物：其中，R 1表示直链或支链的C 6-24烷基或链烯基，R 2和R 4各自 表示C 1-6烷基或 - （AO）n H（A：C 2-4亚烷基，n：1至6的数，条件是n个A可以相同或不同，它们的顺序为 可选），R 3表示C 1-6烷基或 - （A'O）m H（A'：C 2-4亚烷基，m：1至6的数，条件是m个A 可以相同或不同，它们的顺序是任选的），而X“表示阴离子; 含有阳离子表面活性剂（1）的毛发清洁组合物; 以及使用这些组合物处理毛发的方法。本发明的毛发化妆品组合物可以赋予头发良好的柔韧性和光滑性，不仅当其被润湿时，而且在干燥之后。 当用作头发清洁组合物时，它提供优异的泡沫质量和使用感，并表现出良好的低温稳定性。
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公开(公告)号：US06667382B1
公开(公告)日：2003-12-23
申请号：US09674410
申请日：2000-11-01
申请人： Kazuo Isobe , Ryoichi Tamaki , Keiichiro Tomioka , Wataru Yoshida , Tetsuaki Fukushima , Uichiro Nishimoto
发明人： Kazuo Isobe , Ryoichi Tamaki , Keiichiro Tomioka , Wataru Yoshida , Tetsuaki Fukushima , Uichiro Nishimoto
IPC分类号： C08G802
CPC分类号： C08L95/005 , C07C211/14 , C08K5/17
摘要： The present invention provides an amine or polyamine, which has a surface activity not inferior to a solid tallow-based amine and an excellent workability. A salt of the amine is suited for emulsifying asphalt and the like, and also provides an asphalt emulsion composition which is obtained by using the salt and which has a quick setting property. Namely, the prevent invention provides a polyamine represented by the formula (1), a process for producing the amine, and an asphalt emulsion composition containing a water-soluble salt of the amine. wherein R is a straight or branched hydrocarbon group having 8 to 22 carbon atoms; x is a number of 1 to 5; and each of y and z is a number of 0 to 5 with the proviso that both of y and z are not 0 at the same time.
摘要翻译： 本发明提供一种胺或多胺，其具有不劣于固体牛脂基胺的表面活性和优异的可加工性。 胺的盐适于乳化沥青等，并且还提供了通过使用盐获得并且具有快速固化性能的沥青乳液组合物。 即，本发明提供由式（1）表示的多胺，胺的制造方法和含有胺的水溶性盐的沥青乳液组合物。其中R为直链或支链的烃基，其具有8〜 22个碳原子; x是1到5的数字; 并且y和z中的每一个是0至5的数，条件是y和z两者同时不为0。
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公开(公告)号：US6117948A
公开(公告)日：2000-09-12
申请号：US192385
申请日：1998-11-16
申请人： Tetsuaki Fukushima , Wataru Yoshida , Hiroshi Abe
发明人： Tetsuaki Fukushima , Wataru Yoshida , Hiroshi Abe
IPC分类号： C07C213/04 , C07C217/08 , C07C217/50 , C08G65/32 , C08L71/02
CPC分类号： C07C213/04
摘要： The present invention provides a process for easily producing an alkylene oxide adduct to an aliphatic amine compound which has a fully excellent color, is not turbid, and does not deteriorate in color even through long-term storage. That is, the present invention provides a process for producing an alkylene oxide adduct to a primary or secondary amine compound having an aliphatic, saturated or unsaturated, hydrocarbon radical having 8 to 22 carbon atoms, having an excellent color, by reacting an alkyene oxide to the amine compound, characterized by comprising the step of adding a base or an aqueous solution thereof to the amine compound and then heating the mixture.
摘要翻译： 本发明提供一种容易地制备脂肪族胺化合物的烯化氧加合物的方法，其具有完全优异的颜色，不混浊，即使长期保存也不会劣化颜色。 也就是说，本发明提供了通过使氧化烯与氧化烯反应生成具有碳原子数为8〜22的脂肪族，饱和或不饱和的烃基的伯或仲胺化合物的烯化氧加合物，具有优异的颜色的方法 所述胺化合物的特征在于包括将碱或其水溶液加入到所述胺化合物中，然后加热所述混合物的步骤。
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27.发明授权Polyurethane, process for producing the same, and process for producing polyurethane foam 失效聚氨酯，其制造方法和聚氨酯泡沫的制造方法
公开(公告)号：US5306735A
公开(公告)日：1994-04-26
申请号：US32107
申请日：1993-03-17
申请人： Shoichiro Harada , Yasutoshi Isayama , Tetsuaki Fukushima , Masayoshi Morii , Hiroshi Kitagawa , Hiroshi Abe
发明人： Shoichiro Harada , Yasutoshi Isayama , Tetsuaki Fukushima , Masayoshi Morii , Hiroshi Kitagawa , Hiroshi Abe
CPC分类号： C08G18/3271 , C08G18/1825 , C08G18/2875 , C08G18/3275 , C08G18/5021 , C08G18/6688 , C08G2101/0008 , C08G2101/0025 , C08G2101/005 , C08G2101/0083
摘要： Processes for producing a polyurethane, a rigid polyurethane foam, a flexible polyurethane foam and a spray type rigid polyurethane foam are disclosed. In these processes, a specified tertiary aminoalcohol is used as a polyol component and a catalyst.
摘要翻译： 公开了用于生产聚氨酯，硬质聚氨酯泡沫，柔性聚氨酯泡沫和喷雾型硬质聚氨酯泡沫的方法。 在这些方法中，使用特定的叔氨基醇作为多元醇成分和催化剂。
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公开(公告)号：US08581003B2
公开(公告)日：2013-11-12
申请号：US12741928
申请日：2008-10-31
IPC分类号： C07C231/02
CPC分类号： C07C231/02 , B01J21/063 , B01J21/066 , B01J23/002 , B01J23/14 , B01J23/20 , B01J35/023 , B01J35/1019 , B01J37/03 , B01J37/033 , B01J2523/00 , B01J2523/47 , B01J2523/56 , B01J2523/41 , B01J2523/42 , B01J2523/48 , C07C233/05
摘要： The present invention relates to a process for producing an aliphatic carboxylic acid amide, including the step of reacting an aliphatic carboxylic acid or an alkyl ester thereof containing an alkyl group having 1 to 4 carbon atoms with a mono- or dialkylamine containing an alkyl group or groups having 1 to 4 carbon atoms in the presence of a solid acid catalyst containing titanium oxide as a main component and an oxide or oxides of at least one element selected from elements (except titanium) belonging to Groups 4, 5 and 14 of the long form of the periodic table, wherein the catalyst has an average particle diameter of 2 μm or more. The process for producing an aliphatic carboxylic acid amide according to the present invention has a high reaction efficiency of the reaction of the aliphatic carboxylic acid or alkyl ester thereof with the mono- or dialkylamine, and shows an excellent filtration efficiency in separation of the catalyst.
摘要翻译： 本发明涉及脂肪族羧酸酰胺的制造方法，包括使含有碳原子数为1〜4的烷基的脂肪族羧酸或其烷基酯与含有烷基的一价二烷基胺或二烷基胺反应的工序 在含有氧化钛作为主要成分的固体酸催化剂存在下具有1至4个碳原子的基团和选自属于第4,5,5和14族的元素（除了钛之外）的至少一种元素的氧化物或氧化物 形式的周期表，其中催化剂的平均粒径为2μm以上。 本发明的脂肪族羧酸酰胺的制造方法的脂肪族羧酸或其烷基酯与单烷基胺或二烷基胺反应的反应效率高，催化剂的分离过滤效果优异。
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公开(公告)号：US07947853B2
公开(公告)日：2011-05-24
申请号：US12518888
申请日：2007-11-05
IPC分类号： C07C209/16
CPC分类号： C07C209/16 , B01J21/063 , B01J21/066 , B01J23/462 , B01J23/892 , B01J23/894 , B01J23/8946 , B01J27/053 , B01J35/1014 , B01J35/1019 , B01J37/03 , B01J37/031 , B01J37/035 , B01J37/16 , C07C209/14 , C07C211/07 , C07C211/08
摘要： The present invention relates to a process for producing an aliphatic primary amine or an aliphatic secondary amine from an aliphatic alcohol with a high catalytic activity and a high selectivity. In the process for producing an aliphatic amine according to the present invention, a linear, branched, or cyclic aliphatic alcohol having 6 to 22 carbon atoms is contacted with ammonia and hydrogen in the presence of a catalyst formed by supporting a ruthenium component on at least one material selected from the group consisting of (B) a zirconia-containing composite oxide and (C) zirconia surface-treated with a metal by hydrolysis of (A) a ruthenium compound.
摘要翻译： 本发明涉及从具有高催化活性和高选择性的脂族醇生产脂族伯胺或脂族仲胺的方法。 在本发明的脂肪族胺的制造方法中，将具有6〜22个碳原子的直链状，支链状或环状的脂肪族醇在氨和氢的存在下，通过至少支持钌组分而形成的催化剂 一种选自（B）含氧化锆复合氧化物的材料和（C）通过水解（A）钌化合物用金属进行表面处理的氧化锆。
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公开(公告)号：US20100298604A1
公开(公告)日：2010-11-25
申请号：US12741928
申请日：2008-10-31
IPC分类号： C07C231/02 , B01J21/06
CPC分类号： C07C231/02 , B01J21/063 , B01J21/066 , B01J23/002 , B01J23/14 , B01J23/20 , B01J35/023 , B01J35/1019 , B01J37/03 , B01J37/033 , B01J2523/00 , B01J2523/47 , B01J2523/56 , B01J2523/41 , B01J2523/42 , B01J2523/48 , C07C233/05
摘要： The present invention relates to a process for producing an aliphatic carboxylic acid amide, including the step of reacting an aliphatic carboxylic acid or an alkyl ester thereof containing an alkyl group having 1 to 4 carbon atoms with a mono- or dialkylamine containing an alkyl group or groups having 1 to 4 carbon atoms in the presence of a solid acid catalyst containing titanium oxide as a main component and an oxide or oxides of at least one element selected from elements (except titanium) belonging to Groups 4, 5 and 14 of the long form of the periodic table, wherein the catalyst has an average particle diameter of 2 μm or more. The process for producing an aliphatic carboxylic acid amide according to the present invention has a high reaction efficiency of the reaction of the aliphatic carboxylic acid or alkyl ester thereof with the mono- or dialkylamine, and shows an excellent filtration efficiency in separation of the catalyst.
摘要翻译： 本发明涉及脂肪族羧酸酰胺的制造方法，包括使含有碳原子数为1〜4的烷基的脂肪族羧酸或其烷基酯与含有烷基的一价二烷基胺或二烷基胺反应的工序 在含有氧化钛作为主要成分的固体酸催化剂存在下具有1至4个碳原子的基团和选自属于第4,5,5和14族的元素（除了钛之外）的至少一种元素的氧化物或氧化物 形式的周期表，其中催化剂的平均粒径为2μm以上。 本发明的脂肪族羧酸酰胺的制造方法的脂肪族羧酸或其烷基酯与单烷基胺或二烷基胺反应的反应效率高，催化剂的分离过滤效果优异。
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