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31.发明授权Hydroconversion processes employing multi-metallic catalysts and method for making thereof 有权采用多金属催化剂的加氢转化方法及其制备方法公开(公告)号：US07803735B2
公开(公告)日：2010-09-28
申请号：US12259507
申请日：2008-10-28
IPC分类号： B01J27/045 , B01J27/047 , B01J27/14 , B01J27/24 , B01J31/00
CPC分类号： C10G45/08 , B01J23/002 , B01J23/8885 , B01J31/2239 , B01J37/0018 , B01J37/036 , B01J37/20 , B01J2523/00 , B01J2531/26 , B01J2531/66 , B01J2531/847 , C10G45/06 , C10G45/10 , C10G45/12 , C10G45/48 , C10G45/50 , C10G45/52 , C10G45/54 , C10G47/06 , C10G47/18 , C10G47/20 , C10G49/04 , B01J2523/68 , B01J2523/69 , B01J2523/847 , B01J2523/27 , B01J2523/22 , B01J2523/31 , B01J2523/41 , B01J2523/43 , B01J2523/845
摘要： A catalyst precursor composition and methods for making such catalyst precursor are disclosed. The catalyst precursor comprises at least a metal compound selected from Group VIII, Group IIB, Group IIA, Group IVA and combinations thereof, at least one Group VIB metal, at least one organic, oxygen-containing ligand, and a cellulose-containing material. Catalysts prepared from the sulfidation of such catalyst precursors are used in the hydroprocessing of hydrocarbon feeds. In one embodiment, the sulfidation is carried out by contacting the catalyst precursor with hydrogen and a sulfur containing compound in a “slow” process with the sulfidation taking place over a few days up to two weeks, e.g., for at least over 96 hours. In another embodiment, the sulfidation is in a “quick” process with the sulfidation taking place in less than 72 hours. The catalyst prepared from the slow sulfidation process gives a 700° F.+ conversion rate of at least 25% higher than the 700° F.+ conversion rate of a catalyst prepared from a quick sulfidation process.
摘要翻译： 公开了催化剂前体组合物和制备这种催化剂前体的方法。 催化剂前体至少包含选自VIII族，IIB族，IIA族，IVA族及其组合的金属化合物，至少一种VIB族金属，至少一种有机，含氧配位体和含纤维素材料。 由这些催化剂前体的硫化制备的催化剂用于烃进料的加氢处理。 在一个实施方案中，硫化是通过使催化剂前体与“慢”方法中的含硫化合物接触进行的，其中硫化在几天至多两周内进行，例如至少超过96小时。 在另一个实施方案中，硫化是在“快速”过程中，硫化在少于72小时内发生。 从缓慢硫化过程制备的催化剂的转化率比从快速硫化工艺制备的催化剂的700°F +转化率高至少高出25％。
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公开(公告)号：US5954946A
公开(公告)日：1999-09-21
申请号：US959917
申请日：1997-10-29
申请人： Aan Hendrik Klazinga , Theodorus Ludovicus Michael Maesen , Johannes Anthonius Robert Van Veen , Ingrid Maria Van Vegchel
发明人： Aan Hendrik Klazinga , Theodorus Ludovicus Michael Maesen , Johannes Anthonius Robert Van Veen , Ingrid Maria Van Vegchel
IPC分类号： B01J29/08 , B01J29/06 , B01J29/10 , B01J29/12 , B01J29/14 , B01J29/16 , B02C17/16 , B02C17/18 , B22D11/12 , C01B39/24 , C07B61/00 , C08L83/06 , C10G11/05 , C10G47/16 , C10G47/18 , C10G47/20
CPC分类号： B01J29/084 , C10G11/05 , C10G47/16 , B01J2229/16
摘要： The present invention provides a catalyst comprising a very ultrastable zeolite Y (VUSY) in which less than 15% of the total amount of aluminum (Al) present is octahedrally coordinated; a process for preparing the zeolite; and a hydrocarbon conversion process using the catalyst.
摘要翻译： 本发明提供了一种催化剂，其包含非常超稳定的沸石Y（VUSY），其中存在的铝（Al）总量的少于15％是八面体配位的; 沸石的制备方法; 和使用该催化剂的烃转化方法。
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公开(公告)号：US10183282B2
公开(公告)日：2019-01-22
申请号：US14602394
申请日：2015-01-22
IPC分类号： B01J29/06 , B01J29/12 , C10G47/18 , B01J37/02 , B01J37/04 , B01J35/10 , B01J35/00 , B01J37/30 , B01J37/00 , C10G47/16
摘要： A second-stage hydrocracking catalyst is provided comprising: a. from 40 wt % to 70 wt % of a zeolite USY having an ASDI from 0.05 to 0.18; b. an amorphous silica alumina; c. a second alumina; and d. 0.1 to 10 wt % noble metal; wherein the second-stage hydrocracking catalyst has a BET surface area from 450 to 650 m2/g. A second-stage hydrocracking process is provided comprising using the second-stage hydrocracking catalyst to produce middle distillate. A method for making the second-stage hydrocracking catalyst is also provided.
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公开(公告)号：US10040058B2
公开(公告)日：2018-08-07
申请号：US14823807
申请日：2015-08-11
IPC分类号： B01J29/80 , B01J37/04 , B01J35/00 , B01J23/88 , B01J23/888 , B01J29/08 , B01J29/70 , B01J37/00 , B01J37/02 , B01J37/08 , C10G47/20 , B01J29/16 , B01J29/78
摘要： A hydrocracking catalyst is provided comprising: a zeolite beta having an OD acidity of 20 to 50 μmol/g and an average crystal size from 300 to 800 nanometers; a zeolite USY; wherein a wt % of the zeolite beta is less than the wt % of the zeolite USY; a support comprising an amorphous silica aluminate and a second support material; and at least one metal selected from the group consisting of elements from Group 6 and Groups 8 through 10 of the Periodic Table. A process for hydrocracking a hydrocarbonaceous feedstock is provided, comprising: contacting the hydrocarbonaceous feedstock with the hydrocracking catalyst under hydrocracking conditions to produce a hydrocracked effluent that comprises middle distillates. A method for making the hydrocracking catalyst is also provided.
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35.发明申请MIDDLE DISTILLATE HYDROCRACKING CATALYST CONTAINING ZEOLITE USY, AND ZEOLITE BETA WITH LOW ACIDITY AND LARGE DOMAIN SIZE 审中-公开含有沸石使用的中间蒸馏水解催化剂，酸度低，酸度大的ZEOLITE BETA公开(公告)号：US20170043329A1
公开(公告)日：2017-02-16
申请号：US14823807
申请日：2015-08-11
CPC分类号： B01J29/80 , B01J23/88 , B01J23/888 , B01J29/084 , B01J29/166 , B01J29/7007 , B01J29/7815 , B01J35/0006 , B01J35/002 , B01J37/0018 , B01J37/0201 , B01J37/0207 , B01J37/0236 , B01J37/04 , B01J37/08 , C10G47/20
摘要： A hydrocracking catalyst is provided comprising: a zeolite beta having an OD acidity of 20 to 50 μmol/g and an average crystal size from 300 to 800 nanometers; a zeolite USY; wherein a wt % of the zeolite beta is less than the wt % of the zeolite USY; a support comprising an amorphous silica aluminate and a second support material; and at least one metal selected from the group consisting of elements from Group 6 and Groups 8 through 10 of the Periodic Table. A process for hydrocracking a hydrocarbonaceous feedstock is provided, comprising: contacting the hydrocarbonaceous feedstock with the hydrocracking catalyst under hydrocracking conditions to produce a hydrocracked effluent that comprises middle distillates. A method for making the hydrocracking catalyst is also provided.
摘要翻译： 提供加氢裂化催化剂，其包括：OD酸度为20至50μmol/ g，平均晶体尺寸为300至800纳米的沸石β; 沸石USY; 其中β沸石的wt％小于沸石USY的wt％; 包含无定形硅铝酸盐和第二载体材料的载体; 和选自元素周期表第6族和第8至10族中的至少一种金属。 提供了一种用于加氢裂解烃原料的方法，包括：在加氢裂化条件下使烃原料与加氢裂化催化剂接触，以产生包含中间馏分的加氢裂化流出物。 还提供了制备加氢裂化催化剂的方法。
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公开(公告)号：US20160214094A1
公开(公告)日：2016-07-28
申请号：US14602394
申请日：2015-01-22
CPC分类号： B01J37/0201 , B01J21/04 , B01J21/12 , B01J29/126 , B01J35/0006 , B01J35/002 , B01J35/0026 , B01J35/1004 , B01J35/1023 , B01J37/0009 , B01J37/0207 , B01J37/30 , B01J2229/18 , B01J2229/186 , B01J2229/20 , B01J2229/40 , B01J2229/42 , C10G47/16 , C10G47/18
摘要： A second-stage hydrocracking catalyst is provided comprising: a. from 40 wt % to 70 wt % of a zeolite USY having an ASDI from 0.05 to 0.18; b. an amorphous silica alumina; c. a second alumina; and d. 0.1 to 10 wt % noble metal; wherein the second-stage hydrocracking catalyst has a BET surface area from 450 to 650 m2/g. A second-stage hydrocracking process is provided comprising using the second-stage hydrocracking catalyst to produce middle distillate. A method for making the second-stage hydrocracking catalyst is also provided.
摘要翻译： 提供了第二级加氢裂化催化剂，其包括：a。 40重量％至70重量％的具有0.05至0.18的ASDI的沸石USY; b。 无定形二氧化硅氧化铝; C。 第二氧化铝; 和d。 贵金属0.1〜10重量％ 其中第二级加氢裂化催化剂的BET表面积为450〜650m2 / g。 提供第二阶段加氢裂化方法，包括使用第二级加氢裂化催化剂生产中间馏分。 还提供了制备第二级加氢裂化催化剂的方法。
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37.发明申请MIDDLE DISTILLATE HYDROCRACKING CATALYST CONTAINING HIGHLY NANOPOROUS STABILIZED Y ZEOLITE 审中-公开含有高度稳定的Y沸石的中间蒸馏水解催化剂公开(公告)号：US20160121312A1
公开(公告)日：2016-05-05
申请号：US14529768
申请日：2014-10-31
CPC分类号： B01J29/166 , B01J21/12 , B01J29/146 , B01J35/1033 , B01J35/1047 , B01J35/1061 , B01J35/1066 , B01J2229/14 , C10G47/16 , C10G47/20
摘要： Described herein is an improved hydrocracking catalyst containing a high nanopore volume (HNPV) stabilized Y (SY) zeolite. The HNPV SY zeolite is also characterized as having an enhanced acid site distribution as compared to conventional SY zeolites.
摘要翻译： 本文描述的是含有高纳米孔体积（HNPV）稳定的Y（SY）沸石的改进的加氢裂化催化剂。 与常规SY沸石相比，HNPV SY沸石的特征还在于具有增强的酸性位点分布。
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38.发明授权Hydroconversion processes employing multi-metallic catalysts and method for making thereof 有权采用多金属催化剂的加氢转化方法及其制备方法公开(公告)号：US08163169B2
公开(公告)日：2012-04-24
申请号：US12259495
申请日：2008-10-28
CPC分类号： C10G45/08 , B01J23/002 , B01J23/8885 , B01J31/2239 , B01J37/0018 , B01J37/036 , B01J37/20 , B01J2523/00 , B01J2531/26 , B01J2531/66 , B01J2531/847 , C10G45/06 , C10G45/10 , C10G45/12 , C10G45/48 , C10G45/50 , C10G45/52 , C10G45/54 , C10G47/06 , C10G47/18 , C10G47/20 , C10G49/04 , B01J2523/68 , B01J2523/69 , B01J2523/847 , B01J2523/27 , B01J2523/22 , B01J2523/31 , B01J2523/41 , B01J2523/43 , B01J2523/845
摘要： A catalyst precursor composition and methods for making such a catalyst precursor are disclosed. The catalyst precursor comprises at least a promoter metal selected from Group VIII, Group IIB, Group IIA, Group IVA and combinations thereof, having an oxidation state of +2 or +4, at least one Group VIB metal, at least one organic, oxygen-containing ligand, and a cellulose-containing material. In one embodiment, the catalyst precursor is of the formula Av[(MP) (OH)x (L)ny]z (MVIBO4), wherein A is one or more monovalent cationic species, MP is selected from Group VIII, Group IIB, Group IIA, Group IVA and combinations thereof, L is one or more oxygen-containing ligands, MVIB is at least a Group VIB metal, MP:MVIB has an atomic ratio between 100:1 and 1:100. In one embodiment, catalysts prepared from the sulfidation of such catalyst precursors are used in the hydroprocessing of hydrocarbon feeds. In a hydroconversion process at a hydrogen partial pressure of ˜450 psig, the catalyst a 700° F.+ conversion rate of at least 50% of the 700° F.+ conversion results gives obtained under comparable conditions and with a hydrogen partial pressure of 600 psig.
摘要翻译： 公开了催化剂前体组合物和制备这种催化剂前体的方法。 催化剂前体至少包含选自氧化态为+2或+4的至少一种选自VIII族，IIB族，IIA族，IVA族及其组合的助催化剂金属，至少一种VIB族金属，至少一种有机氧 的含配体，和含纤维素的材料。 在一个实施方案中，催化剂前体具有式Av [（MP）（OH）x（L）ny] z（MVIBO4），其中A是一个或多个一价阳离子物质，MP选自VIII族，IIB族， IIA族，IVA族及其组合，L为一个或多个含氧配位体，MVIB为至少VIB族金属，MP：MVIB的原子比为100:1至1:100。 在一个实施方案中，由烃催化剂前体的硫化制备的催化剂用于烃进料的加氢处理。 在约450psig的氢分压下的加氢转化过程中，催化剂在700°F +转化结果的至少50％的转化率为700°F +，在相当的条件下得到，并且在氢分压 600 psig
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公开(公告)号：US07906698B2
公开(公告)日：2011-03-15
申请号：US12687698
申请日：2010-01-14
申请人： Stacey Zones , Allen Burton , Theodorus Ludovicus Michael Maesen , Berend Smit , Edith Beerdsen
发明人： Stacey Zones , Allen Burton , Theodorus Ludovicus Michael Maesen , Berend Smit , Edith Beerdsen
IPC分类号： C10G45/04
CPC分类号： C10G3/47 , B01J29/035 , B01J29/70 , C07C1/20 , C07C2529/70 , C10G3/45 , C10G3/46 , C10G3/49 , C10G29/205 , C10G2300/1088 , C10G2300/1092 , C10G2300/1096 , C10G2400/02 , C10G2400/30 , C07C11/02
摘要： The present invention relates to new crystalline molecular sieve SSZ-75 prepared using a tetramethylene-1,4-bis-(N-methylpyrrolidinium) dication as a structure-directing agent, and its use in catalysts for hydrocarbon conversion reactions.
摘要翻译： 本发明涉及使用四亚甲基-1,4-双 - （N-甲基吡咯烷鎓）双键作为结构导向剂制备的新型结晶分子筛SSZ-75及其在烃转化反应催化剂中的应用。
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公开(公告)号：US07651603B2
公开(公告)日：2010-01-26
申请号：US11756767
申请日：2007-06-01
申请人： Stacey I. Zones , Allen W. Burton, Jr. , Theodorus Ludovicus Michael Maesen , Berend Smit , Edith Beerdsen
发明人： Stacey I. Zones , Allen W. Burton, Jr. , Theodorus Ludovicus Michael Maesen , Berend Smit , Edith Beerdsen
IPC分类号： C10G45/04
CPC分类号： B01J29/70 , B01J29/035 , B01J29/74 , B01J2229/18 , B01J2229/34 , B01J2229/36 , C01B39/06 , C01B39/48 , C07C1/20 , C07C2/66 , C07C2/76 , C07C5/02 , C07C5/222 , C07C5/2708 , C07C5/2737 , C07C5/2775 , C07C6/126 , C07C2529/70 , C07C2529/74 , C08F10/00 , C08F10/02 , C10G3/45 , C10G3/46 , C10G3/47 , C10G3/49 , C10G11/05 , C10G29/205 , C10G45/64 , C10G45/68 , C10G47/16 , C10G50/02 , C10G2300/1092 , C10G2300/1096 , C10G2300/301 , C10G2300/305 , C10G2400/10 , C10G2400/20 , C10G2400/30 , Y02P20/52 , Y02P30/42 , C07C15/08 , C07C9/12 , C08F2/00
摘要： The present invention relates to new crystalline molecular sieve SSZ-75 prepared using a tetramethylene-1,4-bis-(N-methylpyrrolidinium) dication as a structure-directing agent, and its use in catalysts for hydrocarbon conversion reactions.
摘要翻译： 本发明涉及使用四亚甲基-1,4-双 - （N-甲基吡咯烷鎓）双键作为结构导向剂制备的新型结晶分子筛SSZ-75及其在烃转化反应催化剂中的应用。
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