公开(公告)号：US09296622B2

公开(公告)日：2016-03-29

申请号：US13671150

申请日：2012-11-07

申请人： HY-POWER NANO INC.

发明人： Hadi K Mahabadi ,  Juan-Pablo Bravo-Vasquez ,  Sinoj Abraham ,  Guibun Ma ,  Nathan Gerein

IPC分类号： F21V9/04 ,  F21V9/06 ,  G02B5/22 ,  G02B5/26 ,  C01G19/02 ,  G02B1/00 ,  H01B1/08 ,  C01G19/00 ,  G02B5/20 ,  B82Y20/00 ,  B82Y30/00 ,  C03C17/00 ,  C01G17/02 ,  C01G21/02

CPC分类号： C01G19/02 ,  B82Y20/00 ,  B82Y30/00 ,  C01G19/00 ,  C01P2002/72 ,  C01P2002/76 ,  C01P2004/03 ,  C01P2004/20 ,  C01P2004/32 ,  C01P2004/51 ,  C01P2004/62 ,  C01P2004/64 ,  C01P2006/80 ,  C03C17/007 ,  C03C2217/231 ,  C03C2218/114 ,  G02B1/002 ,  G02B5/206 ,  G02B5/208 ,  G02B2207/101 ,  H01B1/08

摘要： Disclosed herein are indium-tin-oxide nanoparticles and a method for continuously producing precipitated indium-tin nanoparticles having a particle size range of substantially from about 10 nm to about 200 nm and a substantially consistent ratio of indium to tin in the resultant nanoparticles across the duration of the continuous process, based on the ratio of indium to tin in a seeding solution. The method comprises preparing intermediate indium and tin compounds of the general formula [M(OH)xCy], where M represents the indium or tin ionic component of indium or tin salts, C represents the cationic component of indium or tin salt(s), x is a number greater than 0 and y=[M*valance−x]/C* valance in the seeding solution. The intermediate compounds are continuously precipitated with a base solution in a reaction vessel initially having a solvent contained therein. The method also provides a means for controlling the shape of the resultant nanoparticles. The resultant indium-tin nanoparticles may be further processed into dispersions.

摘要翻译： 本文公开了铟锡氧化物纳米颗粒和用于连续生产具有基本上约10nm至约200nm的粒度范围的沉淀的铟锡纳米颗粒的方法，并且在所得纳米颗粒中的铟与锡的比例基本上一致 基于接种溶液中铟与锡的比例，连续过程的持续时间。 该方法包括制备通式[M（OH）xCy]的中间体铟和锡化合物，其中M表示铟或锡盐的铟或锡离子组分，C表示铟或锡盐的阳离子组分， x是接种溶液中大于0且y = [M * valance-x] / C *值的数。 中间体化合物在最初具有其中包含溶剂的反应容器中用碱溶液连续沉淀。 该方法还提供了用于控制所得纳米颗粒的形状的手段。 所得的铟锡纳米颗粒可进一步加工成分散体。

公开(公告)号：US09272915B2

公开(公告)日：2016-03-01

申请号：US13978818

申请日：2012-01-11

申请人： Kazuhiro Doshita ,  Toshitaka Furuichi ,  Kosei Shimokawa

发明人： Kazuhiro Doshita ,  Toshitaka Furuichi ,  Kosei Shimokawa

IPC分类号： C01B33/12 ,  B01J20/30 ,  B01J20/28 ,  C01B13/14 ,  C01G19/02 ,  C01G23/053 ,  C01F7/02 ,  C01F17/00 ,  C01G23/047

CPC分类号： C01B33/12 ,  B01J20/28083 ,  B01J20/3085 ,  C01B13/14 ,  C01F7/02 ,  C01F7/021 ,  C01F17/0043 ,  C01G19/02 ,  C01G23/047 ,  C01G23/053 ,  C01P2004/03 ,  C01P2004/20 ,  C01P2006/12 ,  C01P2006/14 ,  C01P2006/16 ,  Y10T428/2982

摘要： Provided is a mesoporous particle having a flaky shape, having a single-layer structure, having a thickness of 0.1 μm to 3 μm, and having an average pore diameter of 10 nm or more. The mesoporous particle can be obtained by a production method including: feeding a metal oxide sol having a pH of 7 or higher and containing metal oxide colloidal particles as dispersoids and water as a dispersion medium, into a liquid containing a water-miscible solvent having a relative permittivity of 30 or lower (protic solvent) or of 40 or lower (aprotic solvent) at 20° C., and thereby forming a flaky aggregate of the metal oxide colloidal particles in the liquid; and subjecting the aggregate to treatment such as drying and heating, and thereby converting the aggregate into a flaky particle that is insoluble in water.

摘要翻译： 提供具有厚度为0.1μm〜3μm，平均孔径为10nm以上的具有单层结构的片状形状的中孔粒子。 中孔粒子可以通过以下的制造方法获得：将含有作为分散质的金属氧化物胶体粒子作为分散相，含有作为分散介质的水分的pH为7以上的金属氧化物溶胶进料到含有水溶性溶剂的液体中， 相对介电常数为30以下（质子性溶剂）或40以下的非质子溶剂（非质子溶剂），由此在液体中形成金属氧化物胶体粒子的片状聚集体; 并对骨料进行干燥和加热处理，从而将骨料转变成不溶于水的片状颗粒。

公开(公告)号：US20150139894A1

公开(公告)日：2015-05-21

申请号：US14398903

申请日：2013-05-06

申请人： Faculdades Católicas, Associação sem fins lucrativos, Mantenedora da Pontificia Universidade

发明人： Diego Manuel Ferreira Lusquinos Fontanez ,  Francisco José Moura

IPC分类号： C01G19/02 ,  B01J19/00 ,  B01J19/24 ,  B01J12/02

CPC分类号： C01G19/02 ,  B01J4/002 ,  B01J4/005 ,  B01J12/02 ,  B01J19/006 ,  B01J19/2415 ,  B01J2219/00006 ,  B01J2219/00777 ,  B01J2219/24 ,  B82Y30/00 ,  B82Y40/00 ,  C01P2002/72 ,  C01P2002/85 ,  C01P2004/04 ,  C01P2004/64 ,  Y10S977/773 ,  Y10S977/896

摘要： The following invention relates to a novel and efficient nanoparticles synthesis reactor and process production. More particularly, the present invention is applied to the synthesis of nanostructured tin dioxide. The benefits provided by the invention can be seen in various gaseous reactions where occurs the formation of solid and gaseous phases.

摘要翻译： 以下发明涉及一种新颖有效的纳米粒子合成反应器和工艺生产。 更具体地，本发明应用于纳米结构二氧化锡的合成。 本发明提供的益处可以在发生固相和气相形成的各种气态反应中看出。

公开(公告)号：US20140127109A1

公开(公告)日：2014-05-08

申请号：US14115366

申请日：2012-05-08

申请人： MITSUBISHI MATERIALS CORPORATION

发明人： Takuma Katase ,  Akihiro Masuda ,  Kanji Kuba

IPC分类号： C01G19/02

CPC分类号： C01G19/02 ,  C01P2004/61 ,  C01P2006/11 ,  C01P2006/12 ,  C01P2006/80 ,  C25D3/30 ,  C25D21/18

摘要： An object and a problem of the present invention is to provide tin (II) oxide powder which has extremely high solubility in an acid or an acidic plating solution and excellent in storage stability in the air. The tin (II) oxide powder of the present invention is for replenishing a tin component of a tin-alloy plating solution, and comprises 100 to 5000 ppm of an antioxidant being contained in the powder with a mass ratio, and has such a dissolution rate that when 0.1 g of the tin (II) oxide powder is added to 100 ml of 100 g/L aqueous alkylsulfonic acid solution at a temperature of 25° C. and stirred, then the powder dissolves therein within 180 seconds.

摘要翻译： 本发明的目的和问题是提供在酸性或酸性电镀溶液中具有极高溶解度的氧化锡（II）粉末，并且在空气中的储存稳定性优异。 本发明的锡（II）氧化物粉末用于补充锡合金电镀液的锡成分，其中含有质量比为100〜5000ppm的粉末中的抗氧化剂，并具有这样的溶解速度 当将0.1g氧化锡（II）粉末在25℃的温度下加入100ml 100g / L烷基磺酸水溶液中并搅拌时，粉末在180秒内溶解。

公开(公告)号：US20140079618A1

公开(公告)日：2014-03-20

申请号：US14115360

申请日：2012-05-08

申请人： MITSUBISHI MATERIALS CORPORATION

发明人： Takuma Katase ,  Akihiro Masuda ,  Kanji Kuba

IPC分类号： C01G19/02

CPC分类号： C01G19/02 ,  C01P2004/61 ,  C01P2006/11 ,  C01P2006/12 ,  C01P2006/80 ,  C25D3/30 ,  C25D21/14

摘要： An object of the present invention is to provide tin(II) oxide powder which has extremely high solubility in an acid or an acidic plating solution, excellent in storage stability in the air and can heighten oxidation-preventive effect of Sn2+ ion in the plating solution. The method for manufacturing tin(II) oxide powder of the present invention comprises Step (11) of preparing an aqueous acidic solution containing Sn2+ ions, Step (12) of neutralizing the aqueous acidic solution by adding an aqueous alkaline solution to prepare a slurry of tin(II) hydroxide, Step (13) of dehydrating the prepared slurry to obtain a slurry of tin(II) oxide, Step (14) of separating the slurry of tin(II) oxide into a solid and a liquid to obtain tin(II) oxide, Step (15) of treating the obtained tin(II) oxide with an aqueous antioxidant solution, and Step (16) of vacuum drying the tin(II) oxide treated with the aqueous antioxidant solution.

摘要翻译： 本发明的目的在于提供在酸性或酸性电镀液中溶解度极高的氧化锡（II）粉末，空气中的保存稳定性优异，能够提高镀液中Sn2 +离子的氧化效果 。 制备本发明的氧化锡（II）的方法包括制备含有Sn 2+离子的酸性水溶液的步骤（11），通过加入碱性水溶液中和酸性水溶液的步骤（12），制备 （II）氢氧化物，步骤（13）使制备的浆料脱水以获得氧化锡（II）的浆料，步骤（14）将氧化锡（II）的浆料分离成固体和液体以获得锡（ II）氧化物，用抗氧化剂水溶液处理得到的氧化锡（II）的步骤（15），以及用水性抗氧化剂溶液处理的氧化锡（II）的真空干燥步骤（16）。

公开(公告)号：US20130032798A1

公开(公告)日：2013-02-07

申请号：US13642314

申请日：2011-04-18

申请人： Aya Miki ,  Yumi Iwanari ,  Toshihiro Kugimiya ,  Shinya Morita ,  Yasuaki Terao ,  Satoshi Yasuno ,  Jae Woo Park ,  Je Hun Lee ,  Byung Du Ahn

发明人： Aya Miki ,  Yumi Iwanari ,  Toshihiro Kugimiya ,  Shinya Morita ,  Yasuaki Terao ,  Satoshi Yasuno ,  Jae Woo Park ,  Je Hun Lee ,  Byung Du Ahn

IPC分类号： C01G19/02 ,  C23C14/08 ,  C01G35/00 ,  H01L29/786 ,  C01F7/02

CPC分类号： H01L29/7869 ,  H01L21/02422 ,  H01L21/02554 ,  H01L21/02565 ,  H01L21/02631 ,  H01L29/66742 ,  H01L29/66969 ,  H01L29/78693

摘要： Disclosed is an oxide for a semiconductor layer of a thin-film transistor, said oxide being excellent in the switching characteristics of a thin-film transistor, specifically enabling favorable characteristics to be stably obtained even in a region of which the ZnO concentration is high and even after forming a passivation layer and after applying stress. The oxide is used in a semiconductor layer of a thin-film transistor, and the aforementioned oxide contains Zn and Sn, and further contains at least one element selected from group X consisting of Al, Hf, Ta, Ti, Nb, Mg, Ga, and the rare-earth elements.

摘要翻译： 公开了一种用于薄膜晶体管的半导体层的氧化物，所述氧化物具有优异的薄膜晶体管的开关特性，特别是即使在ZnO浓度高的区域也能够稳定地获得良好的特性， 甚至在形成钝化层之后和施加应力之后。 氧化物用于薄膜晶体管的半导体层，上述氧化物含有Zn和Sn，还含有选自由Al，Hf，Ta，Ti，Nb，Mg，Ga组成的组X中的至少一种元素 ，和稀土元素。

公开(公告)号：US08003065B2

公开(公告)日：2011-08-23

申请号：US12445639

申请日：2007-06-27

申请人： Yuichiro Shindo ,  Kouichi Takemoto

发明人： Yuichiro Shindo ,  Kouichi Takemoto

IPC分类号： C25B1/00 ,  C25C1/14 ,  C25C1/22 ,  C01G19/00 ,  C01G19/02 ,  C01G15/00 ,  C22B25/00 ,  C22B25/06 ,  C22B58/00

CPC分类号： C25C1/00 ,  C22B3/045 ,  C22B3/44 ,  C22B7/006 ,  C22B25/06 ,  C22B58/00 ,  C25C1/14 ,  C25C1/22 ,  Y02P10/228 ,  Y02P10/234

摘要： Proposed is a method for collecting valuable metal from an ITO scrap including the steps of subjecting the ITO scrap to electrolysis in pH-adjusted electrolyte, and collecting indium or tin as oxides. Additionally proposed is a method for collecting valuable metal from an ITO scrap including the steps of subjecting the ITO scrap to electrolysis in an electrolytic bath partitioned with a diaphragm or an ion-exchange membrane to precipitate hydroxide of tin, thereafter extracting anolyte temporarily, and precipitating and collecting indium contained in the anolyte as hydroxide. With the methods for collecting valuable metal from an ITO scrap described above, indium or tin may be collected as oxides by roasting the precipitate containing indium or tin. Consequently, provided is a method for efficiently collecting indium from an ITO scrap of an indium-tin oxide (ITO) sputtering target or an ITO scrap such as ITO mill ends arisen during the manufacture of such ITO sputtering target.

摘要翻译： 提出了一种从ITO废料中收集有价金属的方法，包括以下步骤：将ITO废料在pH调节的电解液中电解，并收集铟或锡作为氧化物。 另外提出了一种从ITO废料中收集有价值的金属的方法，包括以下步骤：在用隔膜或离子交换膜分隔的电解槽中对ITO废料进行电解以沉淀锡的氢氧化物，然后暂时萃取阳极电解液，并沉淀 并收集阳极电解液中含有的铟作为氢氧化物。 利用从上述ITO废料中收集贵重金属的方法，通过焙烧含有铟或锡的沉淀物可以将铟或锡作为氧化物进行收集。 因此，在ITO溅射靶的制造过程中，提供了从铟锡氧化物（ITO）溅射靶的ITO废料或诸如ITO研磨端的ITO废料中高效收集铟的方法。

公开(公告)号：US20110136013A1

公开(公告)日：2011-06-09

申请号：US12591961

申请日：2009-12-07

申请人： Na Liu ,  Meng-Yao Wu ,  Lei-Min Xu ,  Lu Li ,  Rui Xu ,  Feng-Gang Zhao

发明人： Na Liu ,  Meng-Yao Wu ,  Lei-Min Xu ,  Lu Li ,  Rui Xu ,  Feng-Gang Zhao

IPC分类号： H01M4/58 ,  B05D5/12 ,  C01G25/02 ,  C01G19/02 ,  C01F7/02 ,  C01F5/02 ,  C01B33/12 ,  C01F17/00 ,  C01G9/02

CPC分类号： H01M10/0525 ,  H01M4/0471 ,  H01M4/131 ,  H01M4/1391 ,  H01M4/485 ,  H01M4/505 ,  H01M4/525

摘要： A method is disclosed for coating a positive active material of a lithium-ion battery. The method includes the step of dissolving at least one salt that contains a coating metal in a solvent to provide a solution, the step of dissolving a lithium-containing positive active material in the solution and adjusting the pH value of the solution to deposit M(OH)2n on the lithium-containing positive active material, the step of drying the M(OH)2n and the lithium-containing positive active material, and the step of sintering the M(OH)2n and the lithium-containing positive active material to coat the lithium-containing positive active material with MOn.

摘要翻译： 公开了一种涂覆锂离子电池的正极活性物质的方法。 该方法包括将含有涂层金属的至少一种盐溶解在溶剂中以提供溶液的步骤，将含锂正极活性物质溶解在溶液中并调节溶液的pH值以沉淀M（ OH）2 n，所述含有M（OH）2n和所述含锂正极活性物质的步骤，所述M（OH）2n和所述含锂正极活性物质的烧结工序 用MOn涂覆含锂正极活性物质。

公开(公告)号：US20110127162A1

公开(公告)日：2011-06-02

申请号：US12992067

申请日：2009-05-07

申请人： Charles Edmund King ,  Dosten Baluch

发明人： Charles Edmund King ,  Dosten Baluch

IPC分类号： C23C14/00 ,  C01G19/02 ,  B28B1/14

CPC分类号： C04B35/457 ,  B28B1/26 ,  C01G19/00 ,  C04B35/6261 ,  C04B35/62655 ,  C04B35/62675 ,  C04B35/64 ,  C04B2235/3286 ,  C04B2235/44 ,  C04B2235/444 ,  C04B2235/447 ,  C04B2235/5409 ,  C04B2235/5445 ,  C04B2235/6027 ,  C04B2235/6585 ,  C04B2235/72 ,  C04B2235/724 ,  C04B2235/77 ,  C23C14/3414

摘要： A process for manufacturing indium tin oxide (ITO) sputtering targets as described. The process includes the precipitation of indium and tin hydroxides, sintering in the absence of chloride ions, using the resultant oxide powders to prepare an aqueous slip with dispersing agent, binder, special high density promoting agents and compacting the slip in a specially surface coated porous mold using the method of slip casting followed by sintering the resultant compacted target body to yield high density ITO target.

摘要翻译： 制造如上所述的铟锡氧化物（ITO）溅射靶的方法。 该方法包括沉淀铟和锡氢氧化物，在不存在氯离子的情况下烧结，使用所得的氧化物粉末，制备含有分散剂，粘合剂，特殊高密度促进剂的水性滑爽剂，并将特殊表面涂布的多孔 模具使用滑移铸造方法，随后烧结所得到的压实靶体以产生高密度ITO靶。

公开(公告)号：US20100316544A1

公开(公告)日：2010-12-16

申请号：US12445639

申请日：2007-06-27

申请人： Yuichiro Shindo ,  Kouichi Takemoto

发明人： Yuichiro Shindo ,  Kouichi Takemoto

IPC分类号： C01G19/02 ,  C25B1/00

CPC分类号： C25C1/00 ,  C22B3/045 ,  C22B3/44 ,  C22B7/006 ,  C22B25/06 ,  C22B58/00 ,  C25C1/14 ,  C25C1/22 ,  Y02P10/228 ,  Y02P10/234

摘要： Proposed is a method for collecting valuable metal from an ITO scrap including the steps of subjecting the ITO scrap to electrolysis in pH-adjusted electrolyte, and collecting indium or tin as oxides. Additionally proposed is a method for collecting valuable metal from an ITO scrap including the steps of subjecting the ITO scrap to electrolysis in an electrolytic bath partitioned with a diaphragm or an ion-exchange membrane to precipitate hydroxide of tin, thereafter extracting anolyte temporarily, and precipitating and collecting indium contained in the anolyte as hydroxide. With the methods for collecting valuable metal from an ITO scrap described above, indium or tin may be collected as oxides by roasting the precipitate containing indium or tin. Consequently, provided is a method for efficiently collecting indium from an ITO scrap of an indium-tin oxide (ITO) sputtering target or an ITO scrap such as ITO mill ends arisen during the manufacture of such ITO sputtering target.

摘要翻译： 提出了一种从ITO废料中收集有价金属的方法，包括以下步骤：将ITO废料在pH调节的电解液中电解，并收集铟或锡作为氧化物。 另外提出了一种从ITO废料中收集有价金属的方法，包括以下步骤：在用隔膜或离子交换膜分隔的电解槽中对ITO废料进行电解以沉淀锡的氢氧化物，然后暂时萃取阳极电解液，并沉淀 并收集阳极电解液中含有的铟作为氢氧化物。 利用从上述ITO废料中收集贵重金属的方法，通过焙烧含有铟或锡的沉淀物可以将铟或锡作为氧化物进行收集。 因此，在ITO溅射靶的制造过程中，提供了从铟锡氧化物（ITO）溅射靶的ITO废料或诸如ITO研磨端的ITO废料中有效地收集铟的方法。