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    Crosslinked polymer
    71.
    发明授权
    Crosslinked polymer 有权
    交联聚合物

    公开(公告)号：US07112614B2

    公开(公告)日：2006-09-26

    申请号：US10730238

    申请日：2003-12-08

    Applicant: Naiyong Jing ,  Steven J. Hamrock

    Inventor： Naiyong Jing ,  Steven J. Hamrock

    IPC: C08J5/22 ,  C08J5/20 ,  C08F2/46

    CPC classification number: C08J5/225 ,  C08J3/24 ,  C08J2327/12

    Abstract: A method is provided for obtaining crosslinked polymers, particularly fluorinated polymers having pendent sulfonic acid groups, by crosslinking through pendent groups which include a sulfonyl chloride group (—SO2Cl). The sulfonyl chloride group may be removed by application of electromagnetic radiation, typically in the ultraviolet band, or a radical initiator, leaving behind a radical which readily binds covalently to other polymer strands or to crosslinking agents to form crosslinks. Typically, the polymer is made by providing a polymer comprising pendent groups which include a group according to the formula —SO2F and converting at least a portion of the —SO2F groups to —SO2Cl. After crosslinking, the remaining —SO2F groups may be converted to sulfonic acid groups, yielding a crosslinked polymer electrolyte. Such crosslinked polymer electrolytes may be used to make polymer electrolyte membranes (PEM's) that may be used in electrolytic cells such as fuel cells.

    Abstract translation: 提供一种用于获得交联聚合物，特别是具有侧链磺酸基的氟化聚合物的方法，通过通过包括磺酰氯基团（-SO 2 Cl）的侧基进行交联。 可以通过施加通常在紫外线带中的电磁辐射或自由基引发剂来除去磺酰氯基团，留下易于与其它聚合物链或交联剂共价结合以形成交联的基团。 通常，通过提供包含侧基的聚合物制备聚合物，所述侧基包括根据式-SO 2 F的基团，并将至少一部分-SO 2 F基团取代-SO 2 Cl。 交联后，剩余的-SO 2 F基团可以转化为磺酸基团，得到交联聚合物电解质。 这种交联聚合物电解质可用于制备可用于电解池如燃料电池的聚合物电解质膜（PEM）。

    Method for modifying the surface of a substrate
    73.
    发明授权
    Method for modifying the surface of a substrate 有权
    改性基材表面的方法

    公开(公告)号：US06969166B2

    公开(公告)日：2005-11-29

    申请号：US10447774

    申请日：2003-05-29

    Applicant: John C. Clark ,  Peter T. Elliott ,  Caroline M. Ylitalo ,  Naiyong Jing ,  Gary A. Korba

    Inventor： John C. Clark ,  Peter T. Elliott ,  Caroline M. Ylitalo ,  Naiyong Jing ,  Gary A. Korba

    IPC: B41M3/00 ,  B41J2/01

    CPC classification number: B41M3/006 ,  Y10T428/3154

    Abstract: At least two fixable fluid materials are digitally applied adjacent to each other on a surface of a substrate and fixed to provide fixed coatings having different surface energies The first fixed coating has a first average receding contact angle with water, and the second fixed coating has a second average receding contact angle with water, wherein the magnitude of the difference between the first and second average receding contact angle is at least 30 degree. The coated substrates are useful for controlling the flow of fluid.

    Abstract translation: 至少两个可固定流体材料在基板的表面上彼此相邻地数字地施加并且被固定以提供具有不同表面能的固定涂层。第一固定涂层具有与水的第一平均后退接触角，并且第二固定涂层具有 第二平均与水的后退接触角，其中第一和第二平均后退接触角之间的差值的大小至少为30度。 涂覆的基材可用于控制流体的流动。

    Stain repellent optical hard coating
    74.
    发明申请
    Stain repellent optical hard coating 有权
    防污光学硬涂层

    公开(公告)号：US20050249957A1

    公开(公告)日：2005-11-10

    申请号：US11121456

    申请日：2005-05-04

    Applicant: Naiyong Jing ,  Zai-Ming Qiu ,  Thomas Klun ,  Richard Pokorny ,  George Moore ,  Mark Pellerite

    Inventor： Naiyong Jing ,  Zai-Ming Qiu ,  Thomas Klun ,  Richard Pokorny ,  George Moore ,  Mark Pellerite

    IPC: C08J7/04 ,  C09D4/00 ,  G02B1/10 ,  B32B5/16

    CPC classification number: C08J7/047 ,  C08J2433/00 ,  C09D4/00 ,  G02B1/105 ,  G02B1/14 ,  Y10T428/265 ,  Y10T428/3154 ,  Y10T428/31935

    Abstract: A hard coating composition for use as a stain repellent single layer on an optical display. The coating composition adds a monomer of a mono or multi(methyl)acrylate bearing at least one monovalent hexafluoropolypropylene oxide derivative and a free radically reactive compatibilizer consisting of either a fluoroalkyl-group containing acrylate compatibilizer or a fluoroalkylene-group containing acrylate compatibilizer to a conventional hydrocarbon-based hard coat formulation. The resultant coating is substantially smooth and forms a durable surface layer that has low surface energy that is stain and ink repellent.

    Abstract translation: 在光学显示器上用作防污单层的硬涂层组合物。 涂料组合物将具有至少一种一价六氟聚环氧丙烷衍生物的单或多（甲基）丙烯酸酯的单体和由含氟代烷基的丙烯酸酯增容剂或含氟亚烷基基的丙烯酸酯增容剂组成的自由基反应性增容剂与常规 烃基硬涂层制剂。 所得到的涂层基本上是光滑的，并且形成具有低表面能的耐用表面层，其是防污染和防墨水的。

    Acid functional fluoropolymer membranes and method of manufacture
    76.
    发明申请
    Acid functional fluoropolymer membranes and method of manufacture 有权
    酸官能含氟聚合物膜及其制造方法

    公开(公告)号：US20050119417A1

    公开(公告)日：2005-06-02

    申请号：US10984031

    申请日：2004-11-09

    Applicant: Steven Hamrock ,  Naiyong Jing ,  Shane Mao ,  L. Hardy

    Inventor： Steven Hamrock ,  Naiyong Jing ,  Shane Mao ,  L. Hardy

    IPC: C08F8/26 ,  C08F8/36 ,  C08J5/22 ,  C08L27/16 ,  C08L27/22 ,  H01B1/06 ,  H01B13/00 ,  H01M8/02 ,  H01M8/10 ,  C08F14/18

    CPC classification number: C08L27/22 ,  C08F8/26 ,  C08J5/225 ,  C08L27/16 ,  C08L2205/02 ,  H01M8/1023 ,  H01M8/1039 ,  H01M8/1072 ,  Y02P70/56 ,  C08F14/18 ,  C08L2666/04

    Abstract: Methods are provided to make acid functional fluoropolymers by: a) dehydrofluorinating a starting fluoropolymer with a dehydrofluorinating agent to form an unsaturated fluoropolymer; b) adding an acidifiable nucleophilic functionalizing agent to a double bond of the unsaturated fluoropolymer; and c) acidifying the added acidifiable function. Acid functional fluoropolymers and ion conducting membranes thereof are also provided, including acid functional fluoropolymer having pendent groups according to the formula: —X—Ar-An, wherein X is selected from O, S or NR, where R is selected from H and C1-C30 alkyl or aryl, which are optionally substituted, wherein Ar is a C6-C30 aromatic group, which is optionally substituted, wherein A is an acidic function or salt thereof, wherein a can be independently chosen to be 1, 2 or 3.

    Abstract translation: 提供通过以下方式制备酸官能含氟聚合物的方法：a）用脱氟化氢剂使起始含氟聚合物脱氟化氢以形成不饱和含氟聚合物; b）将可酸化的亲核官能化剂加入到不饱和含氟聚合物的双键中; 和c）酸化所添加的酸化功能。 还提供了酸官能含氟聚合物及其离子传导膜，包括具有下式的侧基的酸官能含氟聚合物：-X-Ar-A N，其中X选自O，S或NR， 其中R选自H和任选取代的C 1 -C 30烷基或芳基，其中Ar是任选取代的C 6 -C 30芳族基团，其中A是酸性官能团或其盐，其中a可以独立地选自 为1,2或3。

    Polymer electrolyte membranes crosslinked by nitrile trimerization
    78.
    发明申请
    Polymer electrolyte membranes crosslinked by nitrile trimerization 失效
    通过腈三聚交联的聚合物电解质膜

    公开(公告)号：US20050107489A1

    公开(公告)日：2005-05-19

    申请号：US10712589

    申请日：2003-11-13

    Applicant: Michael Yandrasits ,  Steven Hamrock ,  Werner Grootaert ,  Miguel Guerra ,  Naiyong Jing

    Inventor： Michael Yandrasits ,  Steven Hamrock ,  Werner Grootaert ,  Miguel Guerra ,  Naiyong Jing

    IPC: C08J5/22 ,  C08G2/00

    CPC classification number: C08J5/225 ,  C08J2327/12

    Abstract: A method is provided for making a crosslinked polymer electrolyte, typically in the form of a membrane for use as a polymer electrolyte membrane in an electrolytic cell such as a fuel cell, by trimerization of nitrile groups contained on groups pendant from the polymer. The resulting polymer electrolyte membrane comprises a highly fluorinated polymer comprising: a perfluorinated backbone, first pendent groups which comprise sulfonic acid groups, and crosslinks comprising trivalent groups according to the formula: The first pendent groups are typically according to the formula: —R1—SO3H, where R1 is a branched or unbranched perfluoroalkyl or perfluoroether group comprising 1-15 carbon atoms and 0-4 oxygen atoms, most typically —O—CF2—CF2—CF2—CF2—SO3H or —O—CF2—CF(CF3)—O—CF2—CF2—SO3H.

    Abstract translation: 提供了一种制备交联聚合物电解质的方法，通常是通过聚合物悬浮在基团上的腈基的三聚作用，在电解池如燃料电池中用作聚合物电解质膜的膜形式。 所得聚合物电解质膜包括高度氟化的聚合物，其包含：全氟化骨架，包含磺酸基团的第一侧基和包含根据下式的三价基团的交联：第一侧基通常根据下式：-R

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