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    Mass spectrometer ring-shaped electrode having high ion selection efficiency and mass spectrometry method thereby
    71.
    发明授权
    Mass spectrometer ring-shaped electrode having high ion selection efficiency and mass spectrometry method thereby 失效
    因此，具有高离子选择效率和质谱法的质谱仪环形电极

    公开(公告)号：US5623144A

    公开(公告)日：1997-04-22

    申请号：US598890

    申请日：1996-02-09

    申请人： Kiyomi Yoshinari ,  Yoichi Ose ,  Yoshiaki Kato

    发明人： Kiyomi Yoshinari ,  Yoichi Ose ,  Yoshiaki Kato

    IPC分类号： H01J49/42

    CPC分类号： H01J49/424 ,  H01J49/427

    摘要： A mass spectrometer and a mass spectrometry method having a high ion selection efficiency are provided. The mass spectrometer comprises an ion trap, a sample introducing device, an electron gun, a detector, a power supply for applying voltage to the ion trap, a control device for controlling the power supply and the electron gun, a mass analyzing device for performing mass spectrometry based on a detected signal of the detector. Using an auxiliary power supply, direction of an auxiliary electric field generated between end cap electrodes is made to point only toward the detector. In this occasion, by setting the cycle of the auxiliary voltage near the oscillation cycle of interest ion species in the axial direction, the interest ion species are synchronized with the auxiliary electric field to be certainly unstabilized in the detector side.

    摘要翻译： 提供了具有高离子选择效率的质谱仪和质谱法。 质谱仪包括离子阱，样品引入装置，电子枪，检测器，用于向离子阱施加电压的电源，用于控制电源和电子枪的控制装置，用于执行的质量分析装置 基于检测器的检测信号的质谱。 使用辅助电源，使端帽电极之间产生的辅助电场的方向仅指向检测器。 在这种情况下，通过将辅助电压的周期设定在轴向的兴趣离子种类的振荡周期附近，兴趣离子种类与辅助电场同步，在检测器侧肯定不稳定。

    4,6-Di-t-butyl-dihydrobenzofuran-5-ol and its derivatives
    72.
    发明授权
    4,6-Di-t-butyl-dihydrobenzofuran-5-ol and its derivatives 失效
    4,6-二叔丁基 - 二氢苯并呋喃-5-醇及其衍生物

    公开(公告)号：US5574178A

    公开(公告)日：1996-11-12

    申请号：US416862

    申请日：1995-04-17

    申请人： Kunio Tamura ,  Yoshiaki Kato ,  Mitsutaka Yoshida ,  Osamu Cynshi ,  Yasuhiro Ohba

    发明人： Kunio Tamura ,  Yoshiaki Kato ,  Mitsutaka Yoshida ,  Osamu Cynshi ,  Yasuhiro Ohba

    IPC分类号： C07C43/23 ,  C07C47/277 ,  C07C69/017 ,  C07C69/157 ,  C07D307/79 ,  C07D307/94

    CPC分类号： C07D307/79 ,  C07C43/23 ,  C07C47/277 ,  C07C69/017 ,  C07D307/94

    摘要： Compounds represented by the general formula as well as intermediates for the synthesis of thereof: ##STR1## where R.sup.1 is a hydrogen atom or an acyl group; R.sup.2 is a lower alkyl group; R.sup.3 is a hydrogen atom or a lower alkyl group; R.sup.4, R.sup.5 and R.sup.6, which may be the same or different, are a hydrogen atom or an optionally substituted alkyl, alkenyl, alkynyl or aryl group; R.sup.2 and R.sup.4, when taken together, may form a 5-membered ring; R.sup.5 and R.sup.6, when taken together, may form a cycloalkyl group or a heterocyclic group in which at least one methylene on the ring of a cycloalkyl group is substituted by an oxygen atom, a sulfur atom or an alkyl-substituted nitrogen atom, provided that R.sup.6 is not present if the ring formed by R.sup.2 and R.sup.4 taken together is a benzofuran ring. The compounds represented by the general formula (I) have a highly selective anti-oxidative activity and are useful as therapeutics of ischemic diseases such as arteriosclerosis and myocardial infarction.

    摘要翻译： PCT No.PCT / JP93 / 01489 371日期1995年04月17日 102（e）日期1995年04月17日PCT 1993年10月18日PCT公布。 出版物WO94 / 08930 日本1994年4月28日由通式表示的化合物及其合成中间体：其中R 1是氢原子或酰基; R2是低级烷基; R3是氢原子或低级烷基; R 4，R 5和R 6可以相同或不同，为氢原子或任选取代的烷基，烯基，炔基或芳基; 当R 2和R 4一起时可以形成5元环; R 5和R 6一起可以形成环烷基或杂环基，其中环烷基环上的至少一个亚甲基被氧原子，硫原子或烷基取代的氮原子取代，条件是 如果由R2和R4形成的环在一起是苯并呋喃环，则R6不存在。 由通式（I）表示的化合物具有高度选择性的抗氧化活性，并且可用作缺血性疾病如动脉硬化和心肌梗死的治疗剂。

    Mass spectrometer
    73.
    发明授权
    Mass spectrometer 失效
    质谱仪

    公开(公告)号：US5298744A

    公开(公告)日：1994-03-29

    申请号：US12469

    申请日：1993-02-02

    申请人： Tadao Mimura ,  Yoshiaki Kato ,  Kazumi Matsumura

    发明人： Tadao Mimura ,  Yoshiaki Kato ,  Kazumi Matsumura

    IPC分类号： G01N27/62 ,  G01N30/72 ,  H01J49/04 ,  H01J49/10

    CPC分类号： H01J49/0404 ,  G01N30/7266 ,  G01N30/7293 ,  H01J49/0468 ,  H01J49/165

    摘要： Ions generated by an ES ion supply are introduced into a mass spectrometer portion through a small hole in a second electrode after passing through a small hole in a heated first electrode, and are analyzed by a mass spectrometer. Corresponding to heating of the first electrode, a length of the small hole in the first electrode is determined to a predetermined adequate value.

    摘要翻译： 通过ES离子源产生的离子通过第一电极中的小孔后通过第二电极中的小孔引入质谱仪部分，并通过质谱仪进行分析。 对应于第一电极的加热，将第一电极中的小孔的长度确定为预定的适当值。

    Liquid chromatograph-direct coupled mass spectrometer
    74.
    发明授权
    Liquid chromatograph-direct coupled mass spectrometer 失效
    液相色谱 - 直接耦合质谱仪

    公开(公告)号：US5240616A

    公开(公告)日：1993-08-31

    申请号：US492321

    申请日：1990-03-12

    申请人： Yoshiaki Kato ,  Tadao Mimura

    发明人： Yoshiaki Kato ,  Tadao Mimura

    IPC分类号： G01N30/72 ,  H01J49/04

    CPC分类号： H01J49/049 ,  G01N30/7246 ,  H01J49/0445 ,  G01N30/7253

    摘要： A liquid chromatograph-direct coupled mass spectrometer, which comprises a liquid chromatograph section, a mass spectrometer section and an interface section coupling the liquid chromatograph section with the mass spectrometer section, the interface section being provided with a first nebulizing means for nebulizing an eluate of a hydrophobic solvent containing a sample in solution introduced from the liquid chromatograph section through a capillary continuously into a vacuum or atmospheric pressure region and the first nebulizing means being further provided with a second nebulizing means for nebulizing a hydrophilic solvent and with a heating means for heating the first and second nebulizing means has a high separability and has no limit to selection of a mobile phase solvent and an ionization solvent.

    摘要翻译： 一种液相色谱 - 直接耦合质谱仪，其包括液相色谱部分，质谱仪部分和将液相色谱部分与质谱仪部分结合的界面部分，界面部分设置有第一雾化装置，用于将洗脱液 含有从液相色谱部分通过毛细管连续引入真空或大气压区域的溶液中的样品的疏水溶剂，第一雾化装置还设置有用于使亲水溶剂雾化的第二雾化装置和用于加热的加热装置 第一和第二雾化装置具有高的分离性，并且对流动相溶剂和电离溶剂的选择没有限制。

    Method for diagnosing abnormality of sensor
    75.
    发明授权
    Method for diagnosing abnormality of sensor 失效
    诊断传感器异常的方法

    公开(公告)号：US5235527A

    公开(公告)日：1993-08-10

    申请号：US974310

    申请日：1992-11-10

    申请人： Masaki Ogawa ,  Yoshiaki Kato

    发明人： Masaki Ogawa ,  Yoshiaki Kato

    IPC分类号： F02D41/22 ,  G01R31/28

    CPC分类号： G01K15/00 ,  F02D41/222 ,  G01K15/007 ,  G01K7/22 ,  G01R31/2829 ,  Y02T10/40

    摘要： There is provided a method for diagnosing an abnormal state of a sensor having a nonlinear output characteristic in which an output signal of a sensor changes nonlinearly. The method includes the steps of determining a first detection value which is indicated by the output signal of the sensor at a predetermined time, and determining a second detection value which is indicated by the output signal of the sensor obtained when a detection value indicated by the output signal has changed by a predetermined variation from the first detection value. The method also includes judging whether or not a deviation between the first detection value and the second detection value is out of a predetermined range, and determining that the sensor has an abnormal state when it is determined that the deviation is out of the predetermined range.

    摘要翻译： 提供了一种用于诊断具有非线性输出特性的传感器的异常状态的方法，其中传感器的输出信号非线性地变化。 该方法包括以下步骤：在预定时间确定由传感器的输出信号指示的第一检测值，以及确定在由所述传感器指示的检测值所获得的传感器的输出信号所指示的第二检测值 输出信号已经从第一检测值改变了预定的变化。 该方法还包括判断第一检测值和第二检测值之间的偏差是否超出预定范围，并且当确定偏差超出预定范围时，确定传感器具有异常状态。

    Image communication apparatus
    77.
    发明授权
    Image communication apparatus 失效
    图像通信设备

    公开(公告)号：US5099335A

    公开(公告)日：1992-03-24

    申请号：US410958

    申请日：1989-09-22

    申请人： Yoshiaki Kato

    发明人： Yoshiaki Kato

    IPC分类号： H04N1/32 ,  H04N1/393

    CPC分类号： H04N1/393 ,  H04N1/32496

    摘要： An image communication apparatus is provided which has various novel functions: a function of eliminating lacking portions in an image printed with a printer incorporating a so-called separation process; a function of shortening the time required for a multi-copy; a function of selecting a maximum resolution of the apparatus without using the same resolution as used during reading; a function of visualizing reading control data in a memory copy mode; and a function of compulsorily setting the manual reception mode when the apparatus at the automatic reception mode is not prepared for reception.

    摘要翻译： 提供一种图像通信装置，其具有各种新颖的功能：消除由包含所谓的分离过程的打印机打印的图像中的缺少部分的功能; 缩短复印所需时间的功能; 在不使用与读取期间相同的分辨率的情况下选择装置的最大分辨率的功能; 在存储器复制模式下可视化读取控制数据的功能; 以及在自动接收模式下的装置未准备接收时强制设定手动接收模式的功能。

    Atmospheric pressure ionization mass spectrometer
    80.
    发明授权
    Atmospheric pressure ionization mass spectrometer 失效
    大气压电离质谱仪

    公开(公告)号：US4996424A

    公开(公告)日：1991-02-26

    申请号：US531247

    申请日：1990-05-03

    申请人： Tadao Mimura ,  Yoshiaki Kato

    发明人： Tadao Mimura ,  Yoshiaki Kato

    IPC分类号： H01J49/04

    CPC分类号： H01J49/0431 ,  H01J49/0404 ,  H01J49/0472

    摘要： An atmospheric pressure ionization mass spectrometer has an interface by which the mass spectrometer is coupled on-line to a liquid chromatograph. This interface comprises an atomization unit which heats and atomizes a sample carried out by a mobile phase from the liquid chromatograph. The atomization unit includes a sample introducing pipe having therein a plurality of thin passages which extend along an axis of the pipe and into which the sample is introduced for atomization.

    摘要翻译： 大气压电离质谱仪具有界面，质谱仪通过该界面在线耦合到液相色谱仪。 该界面包括雾化单元，其从液相色谱仪加热和雾化由流动相进行的样品。 雾化单元包括：样品导入管，其中具有沿着管的轴线延伸的多个细通道，并且样品被引入其中用于雾化。