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    Surface Coated Tool
    74.
    发明申请
    Surface Coated Tool 审中-公开
    表面涂层工具

    公开(公告)号：US20090130434A1

    公开(公告)日：2009-05-21

    申请号：US12293930

    申请日：2007-03-26

    Applicant: Yaocan Zhu ,  Kenji Noda ,  Masahito Matsuzawa

    Inventor： Yaocan Zhu ,  Kenji Noda ,  Masahito Matsuzawa

    IPC: B32B5/16 ,  B23B27/14

    CPC classification number: C23C14/0664 ,  B23B2224/04 ,  B23B2224/24 ,  B23B2224/36 ,  B23B2228/105 ,  C04B35/58014 ,  C04B35/58021 ,  C04B35/581 ,  C04B2235/3852 ,  C04B2235/3856 ,  C04B2235/3865 ,  C04B2235/3873 ,  C04B2235/3886 ,  C23C14/0036 ,  Y10T407/27 ,  Y10T428/256

    Abstract: A surface coated tool including a substrate, and stacked layers composed of two coating layers represented by the following general formula (1) on the substrate is provided. A first coating layer to be coated on the surface of the substrate, which has a thickness of 0.1 to 1 μm, is composed of a granular crystal having a mean crystal diameter of 0.01 to 0.1 μm. A second coating layer to be coated on the surface of the first coating layer, which has a thickness of 0.5 to 5 μm, is composed of columnar crystal grown in a direction perpendicular to the substrate, and the columnar crystal has a mean crystal width of 0.05 to 0.3 μm in a direction parallel to the substrate while a mean crystal width thereof is larger than the mean crystal diameter of the first coating layer. [Formula 3] M1-aAla(CbN1-b)  (1) wherein, M represents at least one metal element selected from the group consisting of the elements of Groups 4, 5 and 6 of the periodic table, Si and rare earth elements, “a” satisfies the relation of 0.25≦a≦0.75, and “b” satisfies the relation of 0≦b≦1.

    Abstract translation: 提供一种包括基板的表面涂覆工具，以及由在基板上由以下通式（1）表示的两个涂层组成的堆叠层。 涂布在基板表面上的厚度为0.1〜1μm的第一涂层由平均结晶直径为0.01〜0.1μm的粒状晶体构成。 要涂覆在第一涂层的表面上的厚度为0.5至5μm的第二涂层由在垂直于衬底的方向上生长的柱状晶体构成，柱状晶体的平均晶体宽度为 其平均晶面宽度大于第一涂层的平均晶体直径，在与基板平行的方向上为0.05〜0.3μm。 [公式3] <？in-line-formula description =“In-line Formulas”end =“lead”？> M1-aAla（CbN1-b）（1）<？in-line-formula description =“In-line 式“end =”tail“？>其中，M表示选自周期表第4,5,6族元素中的至少一种金属元素，Si和稀土元素，”a“满足关系式 为0.25 <= a <= 0.75，“b”满足0 <= b <= 1的关系。

    Hard multilayer coating, and hard multilayer coated tool including the hard multilayer coating
    75.
    发明授权
    Hard multilayer coating, and hard multilayer coated tool including the hard multilayer coating 有权
    硬质多层涂层，硬质多层涂层工具，包括硬质多层涂层

    公开(公告)号：US07504149B2

    公开(公告)日：2009-03-17

    申请号：US11434832

    申请日：2006-05-17

    Applicant: Takaomi Toihara ,  Masatoshi Sakurai ,  Yasuo Fukui ,  Masuo Saitoh

    Inventor： Takaomi Toihara ,  Masatoshi Sakurai ,  Yasuo Fukui ,  Masuo Saitoh

    IPC: B32B9/00

    CPC classification number: C04B35/58007 ,  C04B35/58014 ,  C04B35/58021 ,  C04B35/581 ,  C04B2235/3826 ,  C04B2235/3895 ,  Y10T428/24975 ,  Y10T428/265

    Abstract: A hard multilayer coating that is to be disposed on a body, including: (a) a first coating layer disposed to be held in contact with the body, the first coating layer consisting of TiAlCrX1-aNa (wherein “X” represents carbon or oxygen, and “a” represents a mixed crystal ratio satisfying 0.5≦a≦1); (b) a second coating layer disposed on the first coating layer, the second coating layer being provided by a mixture layer consisting of TiAlCrX1-bNb (wherein “b” represents a mixed crystal ratio satisfying 0.5≦b≦1) and TiAl(SiC)X1-cNc (wherein “c” represents a mixed crystal ratio satisfying 0.5≦c≦1), or provided by a multilayer including a first sublayer consisting of the TiAlCrX1-bNb and a second sublayer consisting of the TiAl(SiC)X1-cNc, which are alternately superposed on each other; and (c) a third coating layer disposed on the second coating layer and constituting an outermost layer of the hard multilayer coating, the third coating layer consisting of TiAl(SiC)X1-dNd (wherein “d” represents a mixed crystal ratio satisfying 0.5≦d≦1).

    Abstract translation: 要设置在主体上的硬质多层涂层，包括：（a）设置成与本体保持接触的第一涂层，由TiAlCrX1-aNa组成的第一涂层（其中“X”表示碳或氧 ，“a”表示满足0.5 <= a <= 1的混晶比; （b）设置在第一涂层上的第二涂层，第二涂层由由TiAlCrX1-bNb组成的混合层（其中“b”表示满足0.5≤b≤1的混晶比）和TiAl （SiC）X1-cNc（其中“c”表示满足0.5 <= c <1的混合晶体比），或由包括由TiAlCrX1-bNb组成的第一子层和由TiAl（ SiC）X1-cNc，它们彼此交替重叠; 和（c）设置在第二涂层上并构成硬多层涂层的最外层的第三涂层，由TiAl（SiC）X1-dNd组成的第三涂层（其中“d”表示满足0.5的混合晶体比 <= d <= 1）。

    Al2O3 dispersion-strengthened Ti2AlN composites and a method for producing the same
    77.
    发明授权
    Al2O3 dispersion-strengthened Ti2AlN composites and a method for producing the same 失效
    Al 2 O 3分散强化Ti 2 AlN复合材料及其制造方法

    公开(公告)号：US07459408B2

    公开(公告)日：2008-12-02

    申请号：US11629559

    申请日：2005-07-15

    Applicant: Juying Li ,  Yuyou Cui ,  Rui Yang

    Inventor： Juying Li ,  Yuyou Cui ,  Rui Yang

    IPC: C04B35/58 ,  C04B35/582

    CPC classification number: C04B35/58014 ,  B82Y30/00 ,  C04B35/117 ,  C04B35/6268 ,  C04B35/645 ,  C04B35/6455 ,  C04B2235/3217 ,  C04B2235/3886 ,  C04B2235/402 ,  C04B2235/404 ,  C04B2235/46 ,  C04B2235/465 ,  C04B2235/5436 ,  C04B2235/5445 ,  C04B2235/5454 ,  C04B2235/6581 ,  C04B2235/662 ,  C04B2235/78 ,  C04B2235/785 ,  C04B2235/80 ,  C04B2235/9684

    Abstract: The invention provides Al2O3 dispersion-strengthened Ti2AlN composites, wherein Ti2AlN matrix and Al2O3 strengthening phase both are reactively formed in situ. The volume fraction of Al2O3 is 5% to 50%; the particle size of Al2O3 ranges from 500 nm to 2 μm, with the mean size of Al2O3 particles about 0.8 μm to 1.2 μm; the shape of Ti2AlN grain is plate-like about 80 nm to 120 nm thick and 0.5 μm to 2 μm long. The composites exhibit excellent deformability at high temperature under compression and flexure stresses, and possess excellent oxidation resistance at 1100° C. to 1350° C. for long time (100 h). The composites show typical metallic conductor behavior and the electrical resistivity at room temperature is 0.3 to 0.8 μΩ·m. The invention also provides a method for preparing the same: First, nanoparticles in Ti—Al binary system were prepared in continuous way by hydrogen plasma-metal reaction (HPMR) using Ti—Al alloy rods with Al content 20% to 60% by atom, or pure Al rods and pure Ti rods. The atmosphere used in HPMR is the mixture atmosphere of nitrogen-containing gas, H2 and Ar, with total pressure of 0.8 to 1.2 atm, wherein volume ratio of H2 and Ar is 1:0.8-1.2, and volume fraction of nitrogen-containing gas is 0 to about 20%. Second, the nanoparticles were compacted by vacuum hot pressing at temperature of 800° C. to 1200° C., pressure of 40 MPa to 60 MPa, time of 4 h to 6 h, and vacuum of 2×10−2 Pa to 5×10−3 Pa.

    Abstract translation: 本发明提供了Al2O3分散强化的Ti2AlN复合材料，其中Ti2AlN基体和Al2O3强化相都在原位反应形成。 Al2O3的体积分数为5％〜50％; Al2O3的粒径为500nm〜2μm，Al2O3粒子的平均粒径为0.8〜1.2μm; Ti2AlN晶粒的形状为板状，约80nm〜120nm厚，0.5μm〜2μm长。 复合材料在压缩和挠曲应力下在高温下表现出优异的变形性，并且在1100℃至1350℃长时间（100小时）下具有优异的抗氧化性。 复合材料表现出典型的金属导体性能，室温下的电阻率为0.3〜0.8 muOmega.m。 本发明还提供了一种制备方法：首先，使用Al含量为20〜60原子％的Ti-Al合金棒，通过氢等离子体 - 金属反应（HPMR）连续制备Ti-Al二元体系中的纳米粒子 ，或纯Al棒和纯Ti棒。 HPMR中使用的气氛是含氮气体，H2和Ar的混合气氛，总压力为0.8〜1.2atm，其中H 2和Ar的体积比为1：0.8-1.2，含氮气体的体积分数 为0至约20％。 第二，通过真空热压在800℃至1200℃，40MPa至60MPa的压力，4小时至6小时的时间和2×10 -2 Pa至5×10 -3的真空压缩纳米颗粒 Pa。

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