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公开(公告)号：US5104515A
公开(公告)日：1992-04-14
申请号：US720107
申请日：1991-06-24
IPC分类号： B01D53/86 , B01J20/02 , B01J29/03 , B01J29/04 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16
CPC分类号： C10G47/16 , B01D53/8628 , B01J20/06 , B01J20/28057 , B01J20/28083 , B01J29/0308 , B01J29/041 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , B01J2229/26 , B01J2229/32 , B01J2229/34 , B01J2229/36 , B01J2229/40 , B01J2229/42 , Y10S423/30
摘要： A method is described for purifying an ultra-large pore crystalline material by contact with an aqueous solution having a hydroxyl concentration sufficient to solubilize an impurity phase but not the crystalline material. The purified crystalline material is also described, as is a hydrocarbon conversion process over the purified crystalline material.
摘要翻译： 描述了通过与具有足以溶解杂质相而不是结晶材料的羟基浓度的水溶液接触来纯化超大孔结晶材料的方法。 还描述了纯化的结晶材料，以及在纯化的结晶材料上的烃转化方法。
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公开(公告)号：US5292698A
公开(公告)日：1994-03-08
申请号：US929061
申请日：1992-08-12
申请人： Cynthia T-W. Chu , Charles T. Kresge , Wieslaw J. Roth , Kenneth G. Simmons, deceased , James C. Vartuli
发明人： Cynthia T-W. Chu , Charles T. Kresge , Wieslaw J. Roth , Kenneth G. Simmons, deceased , James C. Vartuli
CPC分类号： B01J29/049 , B01J29/70 , C01B39/026 , B01J2229/42
摘要： There is provided a catalyst comprising MCM-36 and a binder material.
摘要翻译： 提供了包含MCM-36和粘合剂材料的催化剂。
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公开(公告)号：US06310265B1
公开(公告)日：2001-10-30
申请号：US09432006
申请日：1999-11-01
申请人： Arthur W. Chester , David C. Calabro , Sandeep S. Dhingra , Jean W. Beeckman , Timothy J. Fiebig , Glenn R. Sweeten , Terry E. Helton , Charles T. Kresge , Richard F. Socha , Simon C. Weston
发明人： Arthur W. Chester , David C. Calabro , Sandeep S. Dhingra , Jean W. Beeckman , Timothy J. Fiebig , Glenn R. Sweeten , Terry E. Helton , Charles T. Kresge , Richard F. Socha , Simon C. Weston
IPC分类号： C07C522
CPC分类号： C07C5/2702 , C07C5/2724 , C07C9/00
摘要： This invention relates to a process for isomerizing paraffins comprising the step of contacting a feed containing paraffins with a catalyst comprising a synthetic porous crystalline material, designated MCM-68, which exhibits a distinctive X-ray diffraction pattern and has a unique crystal structure which contains at least one channel system, in which each channel is defined by a 12-membered ring of tetrahedrally coordinated atoms, and at least two further, independent channel systems, in each of which each channel is defined by a 10-membered ring of tetrahedrally coordinated atoms, wherein the number of unique 10-membered ring channels is twice the number of 12-membered ring channels.
摘要翻译： 本发明涉及异构烷烃的方法，其包括使含有链烷烃的进料与包含合成多孔结晶材料的催化剂（称为MCM-68）的催化剂接触，该催化剂表现出独特的X射线衍射图并具有独特的晶体结构，其含有 至少一个通道系统，其中每个通道由四面体配位的原子的12元环定义，以及至少两个独立的通道系统，每个通道系统的每个通道由四面体配位的10元环 原子，其中唯一的10元环通道的数目是12元环通道数目的两倍。
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4.发明授权Isoparaffin/olefin alkylation over vacancy-containing titanometallate molecular sieves 失效在含空白金属酸盐分子筛上的异链烷烃/烯烃烷基化
公开(公告)号：US5498817A
公开(公告)日：1996-03-12
申请号：US308898
申请日：1994-09-20
申请人： Tracy J. Huang , Charles T. Kresge
发明人： Tracy J. Huang , Charles T. Kresge
IPC分类号： C07C2/58
CPC分类号： C07C2/58
摘要： The invention provides a process for alkylating an olefin with an isoparaffin comprising contacting an olefin-containing feed in the presence of a thermally stable composition comprising a non-swellable layered chalcogenide of an element having an atomic number of 4, 5, 12 to 15, 20 to 33, 38 to 51, 56 to 83 and greater than 90, inclusive, said layered metal chalcogenide comprising an interspathic polymeric chalcogenide of an element selected from Groups IB, IIB, IIIA, IIIB, IVA, IVB, VA, VB, VIA, VIIA, and VIIIA of the Periodic Table.
摘要翻译： 本发明提供了一种用异链烷烃烷基化烯烃的方法，包括使含烯烃的进料在热稳定组合物存在下接触，所述组合物包含原子序数为4,5,12至15的元素的不溶胀的层状硫族化物， 20至33,38至51,56至83且大于90，所述层状金属硫族化物包含选自组IB，IIB，IIIA，IIIB，IVA，IVB，VA，VB，VIA中的元素的间质聚合硫属化物 ，VIIA和VIIIA。
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公开(公告)号：US5475178A
公开(公告)日：1995-12-12
申请号：US292653
申请日：1994-08-18
申请人： Kenneth J. Del Rossi , Gregory A. Jablonski , Charles T. Kresge , Guenter H. Kuehl , David O. Marler , Gayatri S. Rav , Brenda H. Rose
发明人： Kenneth J. Del Rossi , Gregory A. Jablonski , Charles T. Kresge , Guenter H. Kuehl , David O. Marler , Gayatri S. Rav , Brenda H. Rose
IPC分类号： B01J27/188 , B01J29/03 , B01J29/04 , C07C2/62 , C07C2/64 , C07C2/68 , C07C5/22 , C07C15/107
CPC分类号： B01J29/0341 , B01J27/188 , B01J29/041 , B01J29/043 , C07C2/62 , B01J29/0308 , C07C2527/188 , Y02P20/588
摘要： There is provided a catalyst comprising a heteropoly acid, such as phosphotungstic acid, supported on a mesoporous crystalline material, such as M41S. A particular form of this M41S support is designated as MCM-41. There is also provided a method for preparing this catalyst by impregnating the heteropoly acid on the support. There is also provided a process for using this catalyst to catalyze acid catalyzed reactions, such as the isomerization of paraffins and the alkylation of aromatics.
摘要翻译： 提供了一种催化剂，其包含负载在介孔结晶材料如M41S上的杂多酸如磷钨酸。 该M41S支持的特定形式被指定为MCM-41。 还提供了通过将杂多酸浸渍在载体上来制备该催化剂的方法。 还提供了一种使用该催化剂催化酸催化反应的方法，例如链烷烃的异构化和芳族化合物的烷基化。
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公开(公告)号：US5370785A
公开(公告)日：1994-12-06
申请号：US189773
申请日：1994-02-01
IPC分类号： B01D53/86 , B01J20/02 , B01J29/03 , B01J29/04 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16
CPC分类号： C10G47/16 , B01D53/8628 , B01J20/06 , B01J20/08 , B01J20/103 , B01J20/12 , B01J20/18 , B01J29/0308 , B01J29/041 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , B01J2229/26 , B01J2229/32 , B01J2229/34 , B01J2229/36 , B01J2229/40 , B01J2229/42
摘要： There is provided a hydrocarbon conversion process and a process for sorbing a sorbate wherein said conversion and sorption process each comprises the use of a porous material. A process for preparing this material involves adding an amphiphilic compound to the reaction mixture for preparing a crystalline oxide. The amphiphilic compound may be a quaternary ammonium cationic surfactant. These surfactants may be in the form of lamellar liquid crystals, and may function as templates for the formation of the present mesoporous oxide materials.
摘要翻译： 提供烃转化方法和用于吸附山梨酸盐的方法，其中所述转化和吸附方法各自包括使用多孔材料。 制备该材料的方法包括向反应混合物中加入两亲性化合物以制备结晶氧化物。 两亲性化合物可以是季铵阳离子表面活性剂。 这些表面活性剂可以是层状液晶的形式，并且可以用作形成本中介氧化物材料的模板。
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公开(公告)号：US5310715A
公开(公告)日：1994-05-10
申请号：US880409
申请日：1992-05-08
申请人： Charles T. Kresge , Wieslaw J. Roth
发明人： Charles T. Kresge , Wieslaw J. Roth
CPC分类号： B01J29/049 , C01B39/026
摘要： There is provided a method for preparing a pillared layered material, designated MCM-36, with a characteristic X-ray diffraction pattern. Upon calcination of the swollen, non-pillared form of this material, the layers collapse and condense upon one another in a somewhat disordered fashion to form a non-swellable material. However, when the swollen layered material is intercalated with polymeric oxide pillars, the layer separation is maintained, even after calcination. A quaternary ammonium silicate, such as tetramethylammonium silicate, is used as a pillaring agent for treating the swollen material.
摘要翻译： 提供了一种具有特征X射线衍射图谱的制备称为MCM-36的柱状分层材料的方法。 在煅烧该材料的膨胀的非柱形形式时，这些层以有点无序的方式彼此崩溃并冷凝，形成不溶胀的材料。 然而，当膨胀的层状材料插入聚合物氧化物柱时，即使在煅烧之后也保持层分离。 使用硅酸四季铵盐作为处理溶胀材料的支柱剂。
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公开(公告)号：US5215737A
公开(公告)日：1993-06-01
申请号：US842684
申请日：1992-02-27
IPC分类号： B01D53/86 , B01J20/02 , B01J29/03 , B01J29/04 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16
CPC分类号： C10G47/16 , B01D53/8628 , B01J20/16 , B01J29/041 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , B01J2229/26 , B01J2229/32 , B01J2229/34 , B01J2229/36 , B01J2229/40 , B01J2229/42
摘要： There is provided a method for synthesizing a new synthetic composition of ultra-large pore crystalline material which can be used as a sorbent or catalyst component for conversion of organic and inorganic compounds. The crystalline material product of this method exhibits unusually large sorption capacity demonstrated by its benzene adsorption capacity of greater than about 15 grams benzene/100 grams at 50 torr and 25.degree. C. This material may have a hexagonal electron diffraction pattern that can be indexed with a d.sub.100 value greater than about 18 Angstrom Units and a hexagonal arrangement of uniformly sized pores with a maximum perpendicular cross section of a least about 13 Angstrom units. The reaction mixture for preparing this material contains silica-alumina hydrogel.
摘要翻译： 提供了一种用于合成可用作有机和无机化合物转化的吸附剂或催化剂组分的超大孔结晶材料的新合成组合物的方法。 该方法的结晶材料产品表现出异常大的吸附能力，其在50托和25℃下苯吸附能力大于约15克苯/ 100克。该材料可具有六角形电子衍射图，其可以用 大于约18埃单位的d100值和具有至少约13埃单位的最大垂直截面的均匀尺寸孔的六边形排列。 用于制备该材料的反应混合物含有二氧化硅 - 氧化铝水凝胶。
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9.发明授权Demetallation of hydrocarbon feedstocks with a synthetic mesoporous crystalline material 失效用合成介孔结晶材料对烃原料进行脱金属化
公开(公告)号：US5183561A
公开(公告)日：1993-02-02
申请号：US734992
申请日：1991-07-24
申请人： Charles T. Kresge , Michael E. Leonowicz , Wieslaw J. Roth , James C. Vartuli , Kathleen M. Keville , Stuart S. Shih , Thomas F. Degnan , Francis G. Dwyer , Michael E. Landis
发明人： Charles T. Kresge , Michael E. Leonowicz , Wieslaw J. Roth , James C. Vartuli , Kathleen M. Keville , Stuart S. Shih , Thomas F. Degnan , Francis G. Dwyer , Michael E. Landis
IPC分类号： B01J29/06 , B01D53/86 , B01J20/02 , B01J29/03 , B01J29/04 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , B01J37/00 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G45/08 , C10G45/12 , C10G47/16
CPC分类号： C10G45/12 , B01D53/8628 , B01J20/02 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/103 , B01J20/12 , B01J29/041 , B01J29/044 , B01J29/045 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16 , B01J2229/26 , B01J2229/32 , B01J2229/34 , B01J2229/36 , B01J2229/40 , B01J2229/42 , B01J37/0009
摘要： There is provided a process for demetallizing hydrocarbon feedstocks, such as resids or shale oil. The process uses a catalyst comprising at least one hydrogenation metal, such as nickel and molybdenum, and an ultra-large pore oxide material. This ultra-large pore oxide material may have uniformly large pores, e.g., having a size of about 40 Angstroms in diameter.
摘要翻译： 提供了一种使烃原料脱金属的方法，例如残油或页岩油。 该方法使用包含至少一种氢化金属如镍和钼的催化剂和超大孔隙氧化物材料。 这种超大孔隙氧化物材料可以具有均匀的大孔，例如具有约40埃直径的尺寸。
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公开(公告)号：US4547605A
公开(公告)日：1985-10-15
申请号：US536469
申请日：1983-09-28
CPC分类号： C07C2/66 , C07C2529/70
摘要： This specification discloses a process for the alkylation of aromatics utilizing ZSM-23 catalyst. A particularly preferred embodiment utilizes ZSM-23 made from a forming mixture containing amorphous precipitated silica, as a silica source, including trace amounts of alumina and sodium chloride.
摘要翻译： 本说明书公开了使用ZSM-23催化剂烷基化芳族化合物的方法。 特别优选的实施方案使用由包含无定形沉淀二氧化硅的成形混合物制成的ZSM-23作为二氧化硅源，包括痕量的氧化铝和氯化钠。
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