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公开(公告)号：US5677921A
公开(公告)日：1997-10-14
申请号：US409236
申请日：1995-03-24
CPC分类号： H01S3/16 , H01S3/1095 , H01S3/1618 , H01S3/1666
摘要： A new class of solid state laser crystals and lasers are formed from Yb-doped borate fluoride host crystals. The general formula for the host crystals is MM'(BO.sub.3)F, where M, M' are monovalent, divalent aria trivalent metal cations. A particular embodiment of the invention is Yb-doped BaCaBO.sub.3 F (Yb:BCBF). BCBF and some of the related derivative crystals are capable of nonlinear frequency conversion, whereby the fundamental of the laser is converted to a longer or shorter wavelength. In this way, these new crystals can simultaneously serve as self-frequency doubling crystals and laser materials within the laser resonator.
摘要翻译： 由掺杂硼酸的硼酸盐主体晶体形成新的固态激光晶体和激光器。 主体晶体的通式为MM'（BO3）F，其中M，M'为单价，二价咏叹调三价金属阳离子。 本发明的一个具体实施方案是Yb掺杂的BaCaBO3F（Yb：BCBF）。 BCBF和一些相关的衍生晶体能够进行非线性频率转换，从而将激光的基极转换为更长或更短的波长。 这样，这些新晶体可以同时用作激光谐振器内的自激倍频晶体和激光材料。
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公开(公告)号：US09228273B2
公开(公告)日：2016-01-05
申请号：US13301538
申请日：2011-11-21
申请人： Douglas A. Keszler , Ning Ye
发明人： Douglas A. Keszler , Ning Ye
CPC分类号： C30B9/00 , C09K11/7712 , C30B9/12 , C30B17/00 , C30B29/10 , C30B29/22 , G02F1/3551
摘要： Described are nonlinear optical (NLO) crystals, including aluminum-borate NLO crystals, that have low concentrations of contaminants that adversely affect the NLO crystal's optical properties, such as compounds that contain transition-metal elements and/or lanthanides, other than yttrium, lanthanum, and lutetium. Some NLO crystals with low concentrations of these contaminants are capable of second harmonic generation at very short wavelengths. Also described are embodiments of a method for making these NLO crystals. Some embodiments involve growing a single NLO crystal, such as an aluminum-borate NLO crystal, from a mixture containing a solvent that is substantially free of harmful contaminants. The described NLO crystals can be used, for example, in laser devices.
摘要翻译： 描述了非线性光学（NLO）晶体，包括铝 - 硼酸盐NLO晶体，其具有低浓度的污染物，其不利地影响NLO晶体的光学性质，例如包含过渡金属元素和/或镧系元素的化合物，除了钇，镧 和镥。 一些具有低浓度这些污染物的NLO晶体能够在非常短的波长下产生二次谐波。 还描述了制造这些NLO晶体的方法的实施方案。 一些实施方案涉及从含有基本上不含有害污染物的溶剂的混合物中生长单个NLO晶体，例如铝 - 硼酸盐NLO晶体。 所描述的NLO晶体可以用于例如激光器件中。
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3.发明授权Metal chalcogenide aqueous precursors and processes to form metal chalcogenide films 有权金属硫族化物含水前体和形成金属硫族化物膜的方法公开(公告)号：US08366967B2
公开(公告)日：2013-02-05
申请号：US12709834
申请日：2010-02-22
IPC分类号： H01B1/00
CPC分类号： C09D1/00 , C23C18/1204 , C23C18/1225
摘要： Metal chalcogenide precursor solutions are described that comprise an aqueous solvent, dissolved metal formate salts and a chalcogenide source composition. The chalcogenide source compositions can be organic compounds lacking a carbon-carbon bond. The precursors are designed to form a desired metal chalcogenide upon thermal processing into films with very low levels of contamination. Potentially contaminating elements in the precursors form gaseous or vapor by-products that escape from the vicinity of the product metal chalcogenide films.
摘要翻译： 描述了含有水性溶剂，溶解的金属甲酸盐和硫族化物源组合物的金属硫族化物前体溶液。 硫族化物源组合物可以是缺少碳 - 碳键的有机化合物。 这些前体被设计成在热处理时形成期望的金属硫属元素化成具有非常低的污染水平的膜。 前体中潜在的污染元素形成从产物金属硫族化物膜附近逃逸的气态或蒸气副产物。
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4.发明申请公开(公告)号：US20120070613A1
公开(公告)日：2012-03-22
申请号：US13284531
申请日：2011-10-28
CPC分类号： G03F7/0043 , G03F7/0042 , G03F7/20 , G03F7/327 , Y10T428/24355
摘要： Stabilized precursor solutions can be used to form radiation inorganic coating materials. The precursor solutions generally comprise metal suboxide cations, peroxide-based ligands and polyatomic anions. Design of the precursor solutions can be performed to achieve a high level of stability of the precursor solutions. The resulting coating materials can be designed for patterning with a selected radiation, such as ultraviolet light, x-ray radiation or electron beam radiation. The radiation patterned coating material can have a high contrast with respect to material properties, such that development of a latent image can be successful to form lines with very low line-width roughness and adjacent structures with a very small pitch.
摘要翻译： 稳定的前体溶液可用于形成辐射无机涂层材料。 前体溶液通常包含金属低氧化物阳离子，基于过氧化物的配体和多原子阴离子。 可以进行前体溶液的设计以实现前体溶液的高水平的稳定性。 可以将所得涂层材料设计成用所选择的辐射（例如紫外光，x射线辐射或电子束辐射）进行图案化。 辐射图案化涂层材料可以在材料性质方面具有高对比度，使得潜像的显影可以成功地形成具有非常低的线宽粗糙度的线和具有非常小间距的相邻结构。
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公开(公告)号：US06419855B1
公开(公告)日：2002-07-16
申请号：US09398604
申请日：1999-09-16
申请人： Douglas A. Keszler , Dong Li , John F. Wager , Benjamin L. Clark , Paul D. Keir
发明人： Douglas A. Keszler , Dong Li , John F. Wager , Benjamin L. Clark , Paul D. Keir
IPC分类号： C07K1156
CPC分类号： H05B33/145 , C09K11/623 , C09K11/642 , C09K11/883 , C09K11/885 , C09K11/886 , H05B33/10 , H05B33/14
摘要： Phosphor compositions of the formula Zn1-3x/2MxX:Mn, wherein M is selected from the group consisting of the trivalent cations of Al, In, Ga, and mixtures thereof, and X is selected from the group consisting of S, Se, Te, and mixtures thereof are disclosed. Also disclosed are phosphor compositions of the formula, MX:Cu,L,A wherein M is selected from the divalent ions of Sr, Mg, Ca, Ba, X is selected from the group consisting of S, Se, Te, and mixtures thereof, and mixtures thereof, L is selected from the group consisting of the trivalent cations of the lanthanides, Al, In, Ga, Sc, and mixtures thereof, and A is selected from the alkali metal ions or mixtures thereof. Emission chromaticity of the phosphors is controlled by varying codopant concentrations. Electroluminescent devices comprising the phosphors also are disclosed.
摘要翻译： 式Zn1-3x / 2MxX：Mn的荧光体组合物，其中M选自Al，In，Ga的三价阳离子及其混合物，X选自S，Se，Te ，及其混合物。 还公开了下式的荧光体组合物MX：Cu，L，A，其中M选自Sr，Mg，Ca，Ba，X的二价离子，X选自S，Se，Te及其混合物 及其混合物，L选自镧系元素，Al，In，Ga，Sc及其混合物的三价阳离子，A选自碱金属离子或其混合物。 磷光体的发射色度是通过改变共掺杂浓度来控制的。 还公开了包含磷光体的电致发光器件。
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6.发明授权公开(公告)号：US06417954B1
公开(公告)日：2002-07-09
申请号：US09768906
申请日：2001-01-23
IPC分类号： G02F139
CPC分类号： C01B35/12 , G02F1/353 , G02F1/3551 , G02F1/39
摘要： Nonlinear optical materials, methods of crystal growth, and devices employing such materials satisfy the general formula (&Sgr;i=1-3M&agr;i1)(&Sgr;j=1-3M&bgr;j2)(&Sgr;k=1-6M&ggr;k3)B14O25 Formula 1 wherein M1, M2, and M3 are mono-, di, or tri-valent metal ions respectively; wherein (&Sgr;i=1-3&agr;i)=X and ranges from 0 to 2, (&Sgr;j=1-3&bgr;j)=Y and ranges from 0 to 4, and (&Sgr;k=1-6&ggr;k)=Z and ranges from 0 to 2, and wherein X+Y+Z=4.0. Other nonlinear optical compounds according to this invention also generally satisfy Formula 2 through 7 below: (&Sgr;j=1-3M&bgr;j2)B14O25, where (&Sgr;j=1-3&bgr;j)=4 Formula 2 M42B14O25 Formula 3 (&Sgr;i=1-3M&agr;i1)(&Sgr;k=1-6M&ggr;k3)B14O25 Formula 4 where (&Sgr;i=1-3&agr;i)=2, and (&Sgr;k=1-6&ggr;k)=2. M21M23B14O25 Formula 5 (&Sgr;i=1-3M&agr;i1)(&Sgr;j=1-3M&bgr;j2)(&Sgr;k=1-6M&ggr;k3)B14O25 Formula 6 where (&Sgr;i=1-3&agr;i)=1, (&Sgr;j=1-3&bgr;j)=2, and (&Sgr;k=1-6&ggr;k)=1. and M1M22M3B14O25 Formula 7.
摘要翻译： 非线性光学材料，晶体生长方法和使用这种材料的器件分别满足M1，M2和M3的一般，二价或三价金属离子的一般形式。 其中（SIGMAi = 1-3alphai）= X，范围为0-2，（SIGMAj = 1-3betaj）= Y，范围为0至4，（SIGMAk = 1-6gammak）= Z且为0至2， 并且其中X + Y + Z = 4.0。 根据本发明的其它非线性光学化合物还通常满足下面的式2至7：其中（SIGMAi = 1-3alphai）= 2，（SIGMAk = 1-6gammak）= 2.其中（SIGMAi = 1-3alphai）= 1， （SIGMAj = 1-3betaj）= 2，（SIGMAk = 1-6gammak）= 1。 和
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7.发明授权Patterned inorganic layers, radiation based patterning compositions and corresponding methods 有权图案化无机层，基于辐射的图案化组合物和相应的方法公开(公告)号：US09176377B2
公开(公告)日：2015-11-03
申请号：US12850867
申请日：2010-08-05
CPC分类号： G03F7/0043 , G03F7/0042 , G03F7/20 , G03F7/327 , Y10T428/24355
摘要： Stabilized precursor solutions can be used to form radiation inorganic coating materials. The precursor solutions generally comprise metal suboxide cations, peroxide-based ligands and polyatomic anions. Design of the precursor solutions can be performed to achieve a high level of stability of the precursor solutions. The resulting coating materials can be designed for patterning with a selected radiation, such as ultraviolet light, x-ray radiation or electron beam radiation. The radiation patterned coating material can have a high contrast with respect to material properties, such that development of a latent image can be successful to form lines with very low line-width roughness and adjacent structures with a very small pitch.
摘要翻译： 稳定的前体溶液可用于形成辐射无机涂层材料。 前体溶液通常包含金属低氧化物阳离子，基于过氧化物的配体和多原子阴离子。 可以进行前体溶液的设计以实现前体溶液的高水平的稳定性。 可以将所得涂层材料设计成用所选择的辐射（例如紫外光，x射线辐射或电子束辐射）进行图案化。 辐射图案化涂层材料可以在材料性质方面具有高对比度，使得潜像的显影可以成功地形成具有非常低的线宽粗糙度的线和具有非常小间距的相邻结构。
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公开(公告)号：US08436337B2
公开(公告)日：2013-05-07
申请号：US12777194
申请日：2010-05-10
CPC分类号： H01L29/7311 , C22C16/00 , C22C45/10 , H01L27/24 , H01L29/66265 , H01L29/66272 , H01L29/7317 , H01L29/732 , H01L45/00
摘要： An electronic structure comprising: (a) a first metal layer; (b) a second metal layer; (c) and at least one insulator layer located between the first metal layer and the second metal layer, wherein at least one of the metal layers comprises an amorphous multi-component metallic film. In certain embodiments, the construct is a metal-insulator-metal (MIM) diode.
摘要翻译： 一种电子结构，包括：（a）第一金属层; （b）第二金属层; （c）和位于第一金属层和第二金属层之间的至少一个绝缘体层，其中至少一个金属层包括非晶多组分金属膜。 在某些实施方案中，构建体是金属 - 绝缘体 - 金属（MIM）二极管。
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公开(公告)号：US20130084672A1
公开(公告)日：2013-04-04
申请号：US13703592
申请日：2011-06-14
申请人： Douglas A. Keszler , Wei Wang
发明人： Douglas A. Keszler , Wei Wang
CPC分类号： C09D1/00 , C23C18/1216 , C23C18/1245 , C23C18/1283 , H01L31/02168 , H01L31/18 , H01L31/1868 , Y02E10/50 , Y02P70/521
摘要： One disclosed embodiment concerns an aqueous inorganic coating precursor solution comprising a mixture of water, polynuclear aluminum hydroxide cations, and polyatomic ligands selected from nitrate (NO3−), nitrite (NO2−), or combinations thereof. In certain embodiments, the composition has a molar concentration ratio of polyatomic ligands to aluminum of less than 3; an aluminum cation concentration of from about 0.01 M to about 3.5 M; and/or a polyatomic anion concentration of from about 0.1 to about 2.5 times the aluminum cation concentration. Embodiments of a method for forming the precursor solution also are disclosed. For example, certain embodiments comprise adding a metal having a sufficient reduction potential to reduce nitric acid to an aqueous solution comprising aluminum nitrate (Al(NO3)3).
摘要翻译： 一个公开的实施方案涉及包含水，多核氢氧化铝阳离子和选自硝酸盐（NO 3 - ），亚硝酸盐（NO 2 - ）或其组合）的多原子配体的混合物的水性无机涂层前体溶液。 在某些实施方案中，组合物的多原子配体与铝的摩尔浓度比小于3; 铝阳离子浓度为约0.01M至约3.5M; 和/或多原子阴离子浓度为铝阳离子浓度的约0.1至约2.5倍。 还公开了用于形成前体溶液的方法的实施方案。 例如，某些实施方案包括加入具有足够还原电位的金属以将硝酸还原成包含硝酸铝（Al（NO 3）3）的水溶液）。
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公开(公告)号：US20120119202A1
公开(公告)日：2012-05-17
申请号：US12286606
申请日：2008-09-30
CPC分类号： G03F7/0002 , B01J21/02 , B01J21/066 , B01J23/002 , B32B9/005 , B32B2457/14 , B82Y10/00 , B82Y40/00 , G03F7/0042 , G03F7/11 , H01L27/1225 , H01L29/7869
摘要： Devices having a thin film or laminate structure comprising hafnium and/or zirconium oxy hydroxy compounds, and methods for making such devices, are disclosed. The hafnium and zirconium compounds can be doped, typically with other metals, such as lanthanum. Examples of electronic devices or components that can be made include, without limitation, insulators, transistors and capacitors. A method for patterning a device using the materials as positive or negative resists or as functional device components also is described. For example, a master plate for imprint lithography can be made. An embodiment of a method for making a device having a corrosion barrier also is described. Embodiments of an optical device comprising an optical substrate and coating also are described. Embodiments of a physical ruler also are disclosed, such as for accurately measuring dimensions using an electron microscope.
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