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    FORMATION OF SUGAR COATINGS
    3.
    发明申请
    FORMATION OF SUGAR COATINGS 审中-公开
    糖涂料的形成

    公开(公告)号：US20090130269A1

    公开(公告)日：2009-05-21

    申请号：US11571718

    申请日：2005-07-06

    申请人： Linda Jane McCausland ,  Neil Maxted ,  Anthony James Brown ,  Ian Humphrey Smith

    发明人： Linda Jane McCausland ,  Neil Maxted ,  Anthony James Brown ,  Ian Humphrey Smith

    IPC分类号： A23P1/08 ,  A23L1/025 ,  A23G3/26 ,  B01D9/00

    CPC分类号： A23G3/343 ,  A23G3/26 ,  A23G2200/06 ,  A23G2220/20 ,  A23V2002/00 ,  A23V2200/22 ,  A23V2250/60

    摘要： A sugar coating is formed on a solution multiplicity of items (5) such as confectionery, using a suspension of crystal nuclei in a solution of sugar. This suspension is created by ultrasonic irradiation of a supersaturated solution. For example a saturated solution is cooled, and stored in a tank (16) connected to a recirculation (10) loop (18) containing a pump (24) and an ultrasonic irradiation module (26). Treated suspension (20) is withdrawn to coat items (11), and new supersaturated solution (14) is introduced. The sugar solution is sufficiently viscous to suppress crystal growth.

    摘要翻译： 在糖的溶液中使用结晶核的悬浮液，在诸如糖果的物品（5）的多种物质上形成糖衣。 该悬浮液通过超饱和溶液的超声波照射产生。 例如，将饱和溶液冷却并储存在连接到包含泵（24）和超声波照射模块（26）的再循环（10）回路（18）的罐（16）中。 撤回处理的悬浮液（20）以涂覆物品（11），并引入新的过饱和溶液（14）。 糖溶液足够粘稠以抑制晶体生长。

    Production of crystalline materials by using high intensity ultrasound
    4.
    发明授权
    Production of crystalline materials by using high intensity ultrasound 有权
    通过使用高强度超声波生产结晶材料

    公开(公告)号：US07244307B2

    公开(公告)日：2007-07-17

    申请号：US10513154

    申请日：2003-05-08

    申请人： Linda Jane McCausland

    发明人： Linda Jane McCausland

    IPC分类号： C30B15/01

    CPC分类号： B01D9/0013 ,  B01D9/005 ,  B01D9/0054 ,  B01D9/0081

    摘要： A crystalline material sufficiently pure for use in pharmaceuticals may be made by forming a saturated solution of the material changing the temperature of the solution so it becomes supersaturated, and briefly subjecting the solution to irradiation by high intensity ultrasound, before allowing the solution to cool gradually without further irradiation. The ultrasound may be applied using a vessel with an array of ultrasonic transducers attached to a wall, so each transducer radiates no more than 3 W/cm2 yet the power dissipation within the vessel is between 25 and 150 W/litre. This method can reduce the metastable zone width to less than 10 K. There is no erosion of the wall and consequently no formation of small particles of metal. It is applicable for example to aspartame, and to amino acids.

    摘要翻译： 用于药物的足够纯的结晶物质可以通过形成改变溶液温度的材料的饱和溶液使其变得过饱和，并且在使溶液逐渐冷却之前将溶液短暂地经过高强度超声波照射， 无需进一步照射。 可以使用具有附接到壁的超声波换能器阵列的血管来应用超声波，因此每个换能器辐射不超过3W / cm 2，而容器内的功率耗散在25和150之间 W /升。 这种方法可以将亚稳区宽度减小到小于10K。没有壁的侵蚀，因此没有形成小的金属颗粒。 它适用于例如阿斯巴甜和氨基酸。

    Chemical process and plant
    5.
    发明授权
    Chemical process and plant 失效
    化学工艺和植物

    公开(公告)号：US06841095B2

    公开(公告)日：2005-01-11

    申请号：US10343786

    申请日：2001-09-05

    申请人： Glyn Jeffrey Buckley ,  Michael Joseph Bowe ,  John William Stairmand

    发明人： Glyn Jeffrey Buckley ,  Michael Joseph Bowe ,  John William Stairmand

    IPC分类号： B01J8/02 ,  B01J8/00 ,  B01J8/20 ,  B01J19/10 ,  B01J19/18 ,  C07F1/02

    CPC分类号： B01J19/10 ,  B01J8/006 ,  B01J8/009 ,  B01J8/20 ,  B01J19/1862 ,  B01J2208/00061 ,  B01J2208/00212 ,  B01J2208/00867 ,  C07F1/02

    摘要： A chemical plant for performing a chemical reaction between particles of a material such as lithium metal, and a reagent such as butyl chloride in solution in hexane, in which one reaction product is a solid material, includes a reaction vessel (12). Several ultrasonic transducers (16) are attached to a wall of the vessel (12) so as to irradiate ultrasonic waves into the vessel, the vessel being large enough that each transducer irradiates into fluid at least 0.1 m thick, each transducer irradiating no more than 3 W/cm2, and the transducers being sufficiently close to each other and the number of transducers being sufficiently high that the power dissipation within the vessel is at least 10 W/liter but no more than 200 W/liter. The high intensity of ultrasound ensures that lithium chloride is cleaned off the surface of lithium metal particles throughout the vessel (12).

    摘要翻译： 在一种反应产物是固体材料的溶剂中，用于在诸如锂金属的材料的颗粒和诸如丁基氯的试剂之间进行化学反应的化学工厂包括反应容器（12）。 几个超声波换能器（16）附着在容器（12）的壁上，以便将超声波照射到容器中，容器足够大，使得每个传感器照射至少0.1μm厚的流体，每个传感器辐射不超过 3W / cm 2，并且换能器彼此充分接近，并且换能器的数量足够高，使得容器内的功率消耗为至少10W /升但不超过200W /升。 高强度的超声波确保氯化锂从整个容器（12）的锂金属颗粒表面清除。

    Production of crystalline materials by using high intensity ultrasound
    8.
    发明授权
    Production of crystalline materials by using high intensity ultrasound 有权
    通过使用高强度超声波生产结晶材料

    公开(公告)号：US07357835B2

    公开(公告)日：2008-04-15

    申请号：US10514883

    申请日：2003-05-13

    申请人： Linda Jane McCausland ,  John Patrick Perkins

    发明人： Linda Jane McCausland ,  John Patrick Perkins

    IPC分类号： B01D9/00 ,  C30B1/00

    CPC分类号： B01D9/0013 ,  B01D9/0036 ,  B01D9/0063 ,  B01D9/0081 ,  C07K5/0613 ,  Y10T117/1024 ,  Y10T117/1028

    摘要： A crystalline material sufficiently pure for use in pharmaceuticals may be made by forming a saturated solution of the material, changing the temperature of the solution so it becomes supersaturated, and subjecting the solution to irradiation by high intensity ultrasound, the frequency of the ultrasound being scanned over a range of frequencies. For example the ultrasound may be varied between 19.5 and 20.5 kHz, and this variation may be sinusoidal. Preferably the ultrasound is provided only briefly, say for less than 5 s, before allowing the solution to cool gradually without further irradiation. The ultrasound may be applied using a vessel with an array of ultrasonic transducers attached to a wall, so each transducer radiates no more than 3 W/cm2 yet the power dissipation within the vessel is between 25 and 150 W/litre. This method can reduce the metastable zone width to less than 10 K. It is applicable in particular to aspartame.

    摘要翻译： 可以通过形成饱和的材料溶液，改变溶液的温度，使其变得过饱和，并通过高强度超声波对该溶液进行照射，使超声频率被扫描，可以制备足够纯的用于药物的结晶物质 在一个频率范围内。 例如，超声可以在19.5和20.5kHz之间变化，并且该变化可以是正弦的。 优选地，在允许溶液逐渐冷却而不进一步照射之前，仅提供超声波，例如少于5秒。 可以使用具有附接到壁的超声波换能器阵列的血管来应用超声波，因此每个换能器辐射不超过3W / cm 2，而容器内的功率耗散在25和150之间 W /升。 该方法可将亚稳区宽度减小到10K以下。特别适用于阿斯巴甜。

    Process and apparatus for irradiating fluids
    9.
    发明授权
    Process and apparatus for irradiating fluids 有权
    用于照射流体的方法和装置

    公开(公告)号：US07354556B2

    公开(公告)日：2008-04-08

    申请号：US10722494

    申请日：2003-11-28

    申请人： John Patrick Perkins

    发明人： John Patrick Perkins

    IPC分类号： B06B1/00

    CPC分类号： B01J19/10 ,  B01J2219/0877

    摘要： Fluids in a vessel are subjected to a high ultrasonic intensity, by means of several ultrasonic transducers attached to a wall of the vessel, each transducer (14) radiating no more than 3 W/cm2, the transducers being sufficiently close to each other, and the number of transducers being sufficiently high, that the power dissipation within the vessel is at least 25 W/liter. The number of transducers, the power of the transducers, and the volume of the vessel may be such that the power density is between 40 and 80 W/liter. The vessel may be double walled, and the space between the two walls be filled by a low attenuation buffer liquid (36) whose cavitation threshold is above that of the liquid being treated.

    摘要翻译： 容器中的流体通过附着在容器壁上的几个超声波换能器受到高超声波强度，每个换能器（14）辐射不超过3W / cm 2，换能器 彼此足够接近，并且换能器的数量足够高，容器内的功率消耗至少为25W /升。 换能器的数量，换能器的功率和容器的体积可以是功率密度在40和80W /升之间。 容器可以是双壁的，并且两个壁之间的空间由其空化阈值高于被处理液体的低衰减缓冲液（36）填充。