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    EPOXIDATION CATALYSTS
    1.
    发明申请
    EPOXIDATION CATALYSTS 审中-公开
    环氧化催化剂

    公开(公告)号：WO2011109276A8

    公开(公告)日：2011-10-13

    申请号：PCT/US2011026439

    申请日：2011-02-28

    Applicant: MASSACHUSETTS INST TECHNOLOGY ,  JAMISON TIMOTHY F ,  IKEUCHI YUTAKA

    Inventor： JAMISON TIMOTHY F ,  IKEUCHI YUTAKA

    IPC: C07D317/26 ,  C07D493/20

    CPC classification number: C07F7/1844 ,  C07D317/20 ,  C07D317/26 ,  C07D493/20

    Abstract: The present invention generally relates to methods for the synthesis of catalysts, including epoxidation catalysts, and related compounds and catalyst compositions. Embodiments described herein may provide efficient processes for providing catalysts (e.g., epoxidation catalysts) in large quantities and using simplified methods.

    Abstract translation: 本发明一般涉及合成催化剂的方法，包括环氧化催化剂以及相关化合物和催化剂组合物。 本文描述的实施方案可以提供大量提供催化剂（例如环氧化催化剂）和使用简化方法的有效方法。

    METHOD OF USING ORGANIC COMPOUNDS
    3.
    发明申请
    METHOD OF USING ORGANIC COMPOUNDS 审中-公开
    使用有机化合物的方法

    公开(公告)号：WO2008011742A1

    公开(公告)日：2008-01-31

    申请号：PCT/CH2007/000365

    申请日：2007-07-24

    Applicant: GIVAUDAN SA ,  GRAB, Willi

    Inventor： GRAB, Willi

    IPC: A23L1/226 ,  C07D317/24 ,  C07D317/26 ,  C07D319/06 ,  C07D405/04

    CPC classification number: C11C3/06 ,  A21D13/80 ,  A23L27/2052 ,  C07D317/24 ,  C07D319/06 ,  C07D405/04

    Abstract: A method of using organic compounds and providing slow release flavoring in or for food products wherein flavor precursors are added to flavor compositions and/or food products and release flavor compounds upon consumption of the food products, and novel flavor precursor compounds. The flavor precursors can be prepared from monoglycerides and flavor compounds which comprise one or more carbonyl groups.

    Abstract translation: 一种使用有机化合物并在食品中提供缓释调味剂的方法，其中将风味前体加入到风味组合物和/或食品中，并在食用食物时释放风味化合物，以及新的风味前体化合物。 风味前体可以由包含一个或多个羰基的单酸甘油酯和风味化合物制备。

    PROCESS FOR THE PREPARATION OF 3-(3,4-METHYLENEDIOXYPHENYL)-2-METHYLPROPANAL
    4.
    发明申请
    PROCESS FOR THE PREPARATION OF 3-(3,4-METHYLENEDIOXYPHENYL)-2-METHYLPROPANAL 审中-公开
    制备3-（3,4-亚甲基二苯基）-2-甲基丙酸的方法

    公开(公告)号：WO2005105774A1

    公开(公告)日：2005-11-10

    申请号：PCT/EP2005/051953

    申请日：2005-04-29

    Applicant: ENDURA S.P.A. ,  BORZATTA, Valerio ,  CAPPARELLA, Elisa ,  POLUZZI, Elisa

    Inventor： BORZATTA, Valerio ,  CAPPARELLA, Elisa ,  POLUZZI, Elisa

    IPC: C07D317/26

    CPC classification number: C07D317/26

    Abstract: Process for the preparation of 3-(3,4-methylenedioxyphenyl)-2-methylpropanal (I) comprising the following steps: a) reacting 5-propanoyl-1,3- benzodioxol (III) with the Vilsmeier reagent at temperatures ranging between 0° and 40°C and subsequently treating of the reaction mixture with a base in aprotic apolar solvent to obtain the unsaturated chloroaldehyde of formula (IV); b) reacting the unsaturated chloroaldehyde of formula (IV), obtained in the previous step, with hydrogen in the presence of a supported heterogeneous catalyst containing a metal chosen amongst Pd, Pt, Rh, Ru in the presence of an organic base or of a mixture of an organic and inorganic base.

    Abstract translation: 制备3-（3,4-亚甲二氧基苯基）-2-甲基丙醛（I）的方法，包括以下步骤：a）将5-丙酰基-1,3-苯并间二氧杂环戊烯（III）与Vilsmeier试剂反应，温度范围为0 °和40℃，随后用非质子非极性溶剂中的碱处理反应混合物，得到式（IV）的不饱和氯醛; b）使在前一步骤中获得的式（IV）的不饱和氯醛与氢气在有机碱存在下，在含有选自Pd，Pt，Rh，Ru中的金属的负载型非均相催化剂存在下反应， 有机和无机碱的混合物。

    PROCESS FOR THE PREPARATION OF (S)-GLYCERALDEHYDE ACETONIDE
    5.
    发明申请
    PROCESS FOR THE PREPARATION OF (S)-GLYCERALDEHYDE ACETONIDE 审中-公开
    制备（S） - 甘油二乙酸酯的方法

    公开(公告)号：WO2005037819A1

    公开(公告)日：2005-04-28

    申请号：PCT/EP2004/011343

    申请日：2004-10-07

    Applicant: DSM IP ASSETS B.V. ,  QUAEDFLIEG, Peter, Jan, Leonard, Mario ,  LOMMEN, Franciscus, Alphons, Marie ,  VIJN, Robert, Jan ,  BOXTEL, VAN, Danniël, Adrianus, Franciscus, Jacobus

    Inventor： QUAEDFLIEG, Peter, Jan, Leonard, Mario ,  LOMMEN, Franciscus, Alphons, Marie ,  VIJN, Robert, Jan ,  BOXTEL, VAN, Danniël, Adrianus, Franciscus, Jacobus

    IPC: C07D317/26

    CPC classification number: C07D317/26

    Abstract: The invention relates to a process for the preparation of (S)-glyceraldehyde acetonide in aqueous solution from 3,4-O-­isopropylidene-L-threonic acid or a salt thereof in aqueous solution, and hypochlorite in aqueous solution wherein the aqueous hypochlorite solution has a pH > 7.5 and wherein during addition of at least 0.1 molar equivalents of hypochlorite based on the amount of 3,4-O-isopropylidene-­L-threonic acid, an acid solution is not simultaneously added. The invention also relates to a process according to the invention, wherein 3,4-O-isopropylidene-L-threonic acid or a salt thereof is prepared from 5,6-O-isopropylidene-L-ascorbic acid or a salt thereof in the presence of H 2 O 2 and a base in a manner known per se, wherein excess H 2 O 2 is optionally removed by catalase. The invention also relates to a process according to the invention, wherein 5,6-O-isopropylidene-L-ascorbic acid or a salt thereof is prepared by reacting L-ascorbic acid or a salt thereof with an acetonide forming agent, preferably in the presence of an acid catalyst.

    Abstract translation: 本发明涉及一种在水溶液中由3,4-O-异亚丙基-L-苏糖酸或其盐在水溶液中制备（S） - 甘油醛缩酮的方法，以及次氯酸盐水溶液中的次氯酸盐水溶液 pH> 7.5，其中基于3,4-O-异亚丙基-L-苏糖酸的量添加至少0.1摩尔当量的次氯酸盐，不能同时加入酸溶液。 本发明还涉及根据本发明的方法，其中3,4-O-异亚丙基-L-苏糖或其盐由5,6-O-异亚丙基-L-抗坏血酸或其盐在 以本身已知的方式存在H 2 O 2和碱，其中任选地通过过氧化氢酶除去过量的H 2 O 2。 本发明还涉及根据本发明的方法，其中5,6-O-异亚丙基-L-抗坏血酸或其盐通过L-抗坏血酸或其盐与丙酮化物形成剂反应制备，优选在 存在酸催化剂。

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