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    Processes for producing phosphorus pentafluoride and phosphate hexafluoride
    5.
    发明授权
    Processes for producing phosphorus pentafluoride and phosphate hexafluoride 有权
    生产五氟化磷和六氟化磷的方法

    公开(公告)号：US09034290B2

    公开(公告)日：2015-05-19

    申请号：US12673058

    申请日：2008-08-11

    申请人： Masahide Waki ,  Shinji Hashiguchi ,  Kazutaka Hirano

    发明人： Masahide Waki ,  Shinji Hashiguchi ,  Kazutaka Hirano

    IPC分类号： C01B25/10 ,  H01M10/04 ,  H01M4/58 ,  C01B25/455 ,  H01M10/0568 ,  H01M6/04 ,  H01M6/14 ,  H01M10/44

    CPC分类号： H01M10/0427 ,  C01B25/10 ,  C01B25/455 ,  C01D15/005 ,  H01M4/582 ,  H01M10/0413 ,  H01M10/0468 ,  H01M10/0568 ,  H01M10/44

    摘要： An object the invention is to provide a phosphorus pentafluoride producing process wherein phosphorus pentafluoride is separated/extracted from a pentavalent phosphorus compound or a solution thereof, or a composition obtained by allowing the pentavalent phosphorus compound or the solution thereof to react with hydrogen fluoride, thereby producing phosphorus pentafluoride; and a phosphate hexafluoride producing process wherein the resultant phosphorus pentafluoride is used as raw material to produce a phosphate hexafluoride high in purity. The present invention relates to a process for producing phosphorus pentafluoride, wherein a carrier gas is brought into contact with either of the following one: a pentavalent phosphorus compound, a solution thereof, or a solution in which a composition obtained by allowing the pentavalent phosphorus compound or the solution thereof to react with hydrogen fluoride is dissolved, thereby a phosphorus pentafluoride is extracted into the career gas.

    摘要翻译： 本发明的目的是提供一种五氟化磷制备方法，其中五氟化磷从五价磷化合物或其溶液中分离/萃取，或通过使五价磷化合物或其溶液与氟化氢反应获得的组合物，由此 生产五氟化磷; 和六氟磷酸盐生产方法，其中所得的五氟化磷作为原料生产高纯度的六氟磷酸盐。 本发明涉及一种生产五氟化磷的方法，其中使载气与以下任何一种接触：五价磷化合物，其溶液或其中通过使五价磷化合物获得的组合物 或其与氟化氢反应的溶液溶解，从而将五氟化磷萃取到活性气体中。

    PROCESSES FOR PRODUCING PHOSPHORUS TETRAFLUORIDE AND PHOSPHATE HEXAFLUORIDE
    7.
    发明申请
    PROCESSES FOR PRODUCING PHOSPHORUS TETRAFLUORIDE AND PHOSPHATE HEXAFLUORIDE 有权
    生产磷酸四氢四磷酸盐和磷酸氢铵的方法

    公开(公告)号：US20110286905A1

    公开(公告)日：2011-11-24

    申请号：US12673058

    申请日：2008-08-11

    申请人： Masahide Waki ,  Shinji Hashiguchi ,  Kazutaka Hirano

    发明人： Masahide Waki ,  Shinji Hashiguchi ,  Kazutaka Hirano

    IPC分类号： C01B25/10

    CPC分类号： H01M10/0427 ,  C01B25/10 ,  C01B25/455 ,  C01D15/005 ,  H01M4/582 ,  H01M10/0413 ,  H01M10/0468 ,  H01M10/0568 ,  H01M10/44

    摘要： An object the invention is to provide a phosphorus pentafluoride producing process wherein phosphorus pentafluoride is separated/extracted from a pentavalent phosphorus compound or a solution thereof, or a composition obtained by allowing the pentavalent phosphorus compound or the solution thereof to react with hydrogen fluoride, thereby producing phosphorus pentafluoride; and a phosphate hexafluoride producing process wherein the resultant phosphorus pentafluoride is used as raw material to produce a phosphate hexafluoride high in purity. The present invention relates to a process for producing phosphorus pentafluoride, wherein a carrier gas is brought into contact with either of the following one: a pentavalent phosphorus compound, a solution thereof, or a solution in which a composition obtained by allowing the pentavalent phosphorus compound or the solution thereof to react with hydrogen fluoride is dissolved, thereby a phosphorus pentafluoride is extracted into the career gas.

    摘要翻译： 本发明的目的是提供一种五氟化磷制备方法，其中五氟化磷从五价磷化合物或其溶液中分离/萃取，或通过使五价磷化合物或其溶液与氟化氢反应获得的组合物，由此 生产五氟化磷; 和六氟磷酸盐生产方法，其中所得的五氟化磷作为原料生产高纯度的六氟磷酸盐。 本发明涉及一种生产五氟化磷的方法，其中使载气与以下任何一种接触：五价磷化合物，其溶液或其中通过使五价磷化合物获得的组合物 或其与氟化氢反应的溶液溶解，从而将五氟化磷萃取到活性气体中。

    Processes for production of phosphorus pentafluoride and hexafluorophosphates
    10.
    发明授权
    Processes for production of phosphorus pentafluoride and hexafluorophosphates 有权
    生产五氟化磷和六氟磷酸盐的方法

    公开(公告)号：US08470278B2

    公开(公告)日：2013-06-25

    申请号：US12990914

    申请日：2009-08-04

    申请人： Masahide Waki ,  Tatsuhiro Yabune ,  Kazuhiro Miyamoto ,  Kazutaka Hirano

    发明人： Masahide Waki ,  Tatsuhiro Yabune ,  Kazuhiro Miyamoto ,  Kazutaka Hirano

    IPC分类号： C01B25/10

    CPC分类号： H01M10/0568 ,  C01B25/10 ,  C01B25/455 ,  H01M10/052 ,  H01M2300/0025 ,  Y02T10/7011

    摘要： A method of manufacturing phosphorus pentafluoride and hexafluorophosphate can suppress the manufacturing cost and also can manufacture high-quality phosphorus pentafluoride from an inexpensive and low-quality raw material. The raw material for the method can include at least a phosphorus atom and a fluorine atom. These are brought into contact with a carrier gas, and a phosphorus pentafluoride is extracted and separated into the carrier gas. A method of manufacturing hexafluorophosphate includes reacting fluoride with the resulting phosphorus pentafluoride according to the following chemical reaction scheme: sPF5+AFs→A(PF6)s, in which s is in the range of 1≦s≦3, and A is at least one of the following: Li, Na, K, Rb, Cs, NH4, Ag, Mg, Ca, Ba, Zn, Cu, Pb, Al and Fe.

    摘要翻译： 制造五氟化磷和六氟磷酸盐的方法可以抑制制造成本，并且还可以从廉价且低质量的原料制造高品质的五氟化磷。 该方法的原料可以至少包含磷原子和氟原子。 使其与载气接触，并且将五氟化磷萃取并分离成载气。 制造六氟磷酸盐的方法包括：根据以下化学反应方案使氟化物与得到的五氟化磷反应：sPF5 + AFs-> A（PF6）s，其中s在1 @ s @ 3的范围内，A在 Li，Na，K，Rb，Cs，NH4，Ag，Mg，Ca，Ba，Zn，Cu，Pb，Al和Fe中的至少一种。