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公开(公告)号：US10260156B2
公开(公告)日：2019-04-16
申请号：US15078784
申请日：2016-03-23
Applicant: BATTELLE MEMORIAL INSTITUTE , BATTELLE ENERGY ALLIANCE, LLC
Inventor： Michael A. Lilga , Asanga B. Padmaperuma , Tedd E. Lister , Eric J. Dufek , Lucia M. Petkovic , Luis A. Diaz-Aldana
IPC: C07C1/24 , C25B3/04 , C25B3/00 , C25B9/08 , C25B9/04 , C25B15/02 , C25B15/08 , C07B31/00 , C25B1/04
Abstract: A system and process are disclosed for electrochemically upgrading bio-oils and bio-crudes that enhance yields of selected reduction products for subsequent production of bio-based fuels.
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公开(公告)号：US20170369804A1
公开(公告)日：2017-12-28
申请号：US15681154
申请日：2017-08-18
Applicant: Battelle Memorial Institute
Inventor： Michael A. Lilga , Richard T. Hallen , Karl O. Albrecht , Alan R. Cooper , John G. Frye , Karthikeyan Kallupalayam Ramasamy
IPC: C10L1/04 , C07C2/12 , C07C2/24 , C10G69/12 , C07C5/03 , C10G29/20 , C10G45/00 , C10G50/00 , C10G3/00 , C07C2/66
CPC classification number: C10L1/04 , C07C2/12 , C07C2/24 , C07C2/66 , C07C5/03 , C07C2521/04 , C07C2521/12 , C07C2523/42 , C07C2523/755 , C07C2529/06 , C07C2529/40 , C07C2529/70 , C07C2529/76 , C10G3/00 , C10G29/205 , C10G45/00 , C10G50/00 , C10G69/123 , C10G69/126 , C10G2300/1081 , C10G2300/1092 , C10G2300/1096 , C10L2200/0469 , C10L2270/02 , C10L2270/04 , C10L2290/24 , C10L2290/543 , Y02P30/42
Abstract: Systems, processes, and catalysts are disclosed for obtaining fuels and fuel blends containing selected ratios of open-chain and closed-chain fuel-range hydrocarbons suitable for production of alternate fuels including gasolines, jet fuels, and diesel fuels. Fuel-range hydrocarbons may be derived from ethylene-containing feedstocks and ethanol-containing feedstocks.
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公开(公告)号：US09771533B2
公开(公告)日：2017-09-26
申请号：US14528185
申请日：2014-10-30
Applicant: BATTELLE MEMORIAL INSTITUTE
Inventor： Michael A. Lilga , Richard T. Hallen , Karl O. Albrecht , Alan R. Cooper , John G. Frye , Karthikeyan Kallupalayam Ramasamy
IPC: C07C2/12 , C10L1/04 , C10G29/20 , C10G45/00 , C10G50/00 , C10G69/12 , C10G3/00 , C07C2/24 , C07C2/66 , C07C5/03
CPC classification number: C10L1/04 , C07C2/12 , C07C2/24 , C07C2/66 , C07C5/03 , C07C2521/04 , C07C2521/12 , C07C2523/42 , C07C2523/755 , C07C2529/06 , C07C2529/40 , C07C2529/70 , C07C2529/76 , C10G3/00 , C10G29/205 , C10G45/00 , C10G50/00 , C10G69/123 , C10G69/126 , C10G2300/1081 , C10G2300/1092 , C10G2300/1096 , C10L2200/0469 , C10L2270/02 , C10L2270/04 , C10L2290/24 , C10L2290/543 , Y02P30/42
Abstract: Systems, processes, and catalysts are disclosed for obtaining fuels and fuel blends containing selected ratios of open-chain and closed-chain fuel-range hydrocarbons suitable for production of alternate fuels including gasolines, jet fuels, and diesel fuels. Fuel-range hydrocarbons may be derived from ethylene-containing feedstocks and ethanol-containing feedstocks.
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公开(公告)号：US09517984B2
公开(公告)日：2016-12-13
申请号：US14678729
申请日：2015-04-03
Applicant: Battelle Memorial Institute
Inventor： Michael A. Lilga , Guo-Shuh Lee , Suh-Jane Lee
CPC classification number: C07C29/145 , C07C29/172 , C07C29/60 , C07C45/29 , C07C45/52 , C10G3/44 , C10G45/00 , C10G2400/30 , C10L1/04 , Y02P30/20 , C07C31/12 , C07C49/10
Abstract: Embodiments of an integrated method for step-wise conversion of 2,3-butanediol to 2-butanol, and optionally to hydrocarbons, are disclosed. The method includes providing an acidic catalyst, exposing a composition comprising aqueous 2,3-butanediol to the acidic catalyst to produce an intermediate composition comprising methyl ethyl ketone, providing a hydrogenation catalyst that is spatially separated from the acidic catalyst, and subsequently exposing the intermediate composition to the hydrogenation catalyst to produce a composition comprising 2-butanol. The method may further include subsequently exposing the composition comprising 2-butanol to a deoxygenation catalyst, and deoxygenating the 2-butanol to form hydrocarbons. In some embodiments, the hydrocarbons comprise olefins, such as butenes, and the method may further include subsequently exposing the hydrocarbons to a hydrogenation catalyst to form saturated hydrocarbons.
Abstract translation: 公开了用于将2,3-丁二醇逐步转化为2-丁醇和任选地转化成烃的综合方法的实施方案。 该方法包括提供酸性催化剂，将包含2,3-丁二醇水溶液的组合物暴露于酸性催化剂以产生包含甲基乙基酮的中间体组合物，提供与酸性催化剂在空间上分离的氢化催化剂，随后将中间体 组合物加氢催化剂以产生包含2-丁醇的组合物。 该方法可以进一步包括随后将包含2-丁醇的组合物暴露于脱氧催化剂，并将2-丁醇脱氧以形成烃。 在一些实施方案中，烃包括烯烃，例如丁烯，并且该方法还可以包括随后将烃暴露于氢化催化剂以形成饱和烃。
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公开(公告)号：US20150284307A1
公开(公告)日：2015-10-08
申请号：US14678729
申请日：2015-04-03
Applicant: Battelle Memorial Institute
Inventor： Michael A. Lilga , Guo-Shuh Lee , Suh-Jane Lee
CPC classification number: C07C29/145 , C07C29/172 , C07C29/60 , C07C45/29 , C07C45/52 , C10G3/44 , C10G45/00 , C10G2400/30 , C10L1/04 , Y02P30/20 , C07C31/12 , C07C49/10
Abstract: Embodiments of an integrated method for step-wise conversion of 2,3-butanediol to 2-butanol, and optionally to hydrocarbons, are disclosed. The method includes providing an acidic catalyst, exposing a composition comprising aqueous 2,3-butanediol to the acidic catalyst to produce an intermediate composition comprising methyl ethyl ketone, providing a hydrogenation catalyst that is spatially separated from the acidic catalyst, and subsequently exposing the intermediate composition to the hydrogenation catalyst to produce a composition comprising 2-butanol. The method may further include subsequently exposing the composition comprising 2-butanol to a deoxygenation catalyst, and deoxygenating the 2-butanol to form hydrocarbons. In some embodiments, the hydrocarbons comprise olefins, such as butenes, and the method may further include subsequently exposing the hydrocarbons to a hydrogenation catalyst to form saturated hydrocarbons.
Abstract translation: 公开了用于将2,3-丁二醇逐步转化为2-丁醇和任选地转化成烃的综合方法的实施方案。 该方法包括提供酸性催化剂，将包含2,3-丁二醇水溶液的组合物暴露于酸性催化剂以产生包含甲基乙基酮的中间体组合物，提供与酸性催化剂在空间上分离的氢化催化剂，随后将中间体 组合物加氢催化剂以产生包含2-丁醇的组合物。 该方法可以进一步包括随后将包含2-丁醇的组合物暴露于脱氧催化剂，并将2-丁醇脱氧以形成烃。 在一些实施方案中，烃包括烯烃，例如丁烯，并且该方法还可以包括随后将烃暴露于氢化催化剂以形成饱和烃。
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Patent Agency Ranking
公开(公告)号：US10005974B2
公开(公告)日：2018-06-26
申请号：US15681154
申请日：2017-08-18
Applicant: Battelle Memorial Institute
Inventor： Michael A. Lilga , Richard T. Hallen , Karl O. Albrecht , Alan R. Cooper , John G. Frye , Karthikeyan Kallupalayam Ramasamy
IPC: C10L1/04 , C07C2/12 , C10G3/00 , C10G69/12 , C10G50/00 , C10G45/00 , C10G29/20 , C07C2/24 , C07C2/66 , C07C5/03
CPC classification number: C10L1/04 , C07C2/12 , C07C2/24 , C07C2/66 , C07C5/03 , C07C2521/04 , C07C2521/12 , C07C2523/42 , C07C2523/755 , C07C2529/06 , C07C2529/40 , C07C2529/70 , C07C2529/76 , C10G3/00 , C10G29/205 , C10G45/00 , C10G50/00 , C10G69/123 , C10G69/126 , C10G2300/1081 , C10G2300/1092 , C10G2300/1096 , C10L2200/0469 , C10L2270/02 , C10L2270/04 , C10L2290/24 , C10L2290/543 , Y02P30/20 , Y02P30/42
Abstract: Systems, processes, and catalysts are disclosed for obtaining fuels and fuel blends containing selected ratios of open-chain and closed-chain fuel-range hydrocarbons suitable for production of alternate fuels including gasolines, jet fuels, and diesel fuels. Fuel-range hydrocarbons may be derived from ethylene-containing feedstocks and ethanol-containing feedstocks.
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公开(公告)号：US09932531B2
公开(公告)日：2018-04-03
申请号：US15494758
申请日：2017-04-24
Applicant: Battelle Memorial Institute
Inventor： Michael A. Lilga , Richard T. Hallen , Karl O. Albrecht , Alan R. Cooper , John G. Frye , Karthikeyan Kallupalayam Ramasamy
CPC classification number: C07C2/24 , B01J8/04 , B01J21/04 , B01J21/12 , B01J23/42 , B01J23/755 , B01J29/072 , B01J29/084 , B01J29/40 , B01J29/7007 , B01J29/7615 , B01J29/90 , B01J35/0006 , B01J37/0201 , B01J38/02 , B01J2208/02 , B01J2208/027 , C07C1/20 , C07C1/24 , C07C2/12 , C07C5/03 , C07C2521/12 , C07C2523/755 , C07C2529/06 , C07C2529/072 , C07C2529/14 , C07C2529/24 , C07C2529/46 , C07C2529/68 , C07C2529/70 , C07C2529/76 , C07C2529/85 , C10G3/00 , C10G45/00 , C10G50/00 , C10G69/126 , C10G2300/1092 , C10G2300/4081 , C10G2400/02 , C10G2400/04 , C10G2400/08 , Y02P20/52 , Y02P20/584 , Y02P30/42 , C07C11/04 , C07C11/02
Abstract: Systems, processes, and catalysts are disclosed for obtaining fuel and fuel blends containing selected ratios of open-chain and closed-chain fuel-range hydrocarbons suitable for production of alternate fuels including gasolines, jet fuels, and diesel fuels. Fuel-range hydrocarbons may be derived from ethylene-containing feedstocks and ethanol-containing feedstocks.
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8.发明授权公开(公告)号：US09777224B2
公开(公告)日：2017-10-03
申请号：US15345305
申请日：2016-11-07
Applicant: BATTELLE MEMORIAL INSTITUTE
Inventor： Michael A. Lilga , Asanga B. Padmaperuma
IPC: C10L1/16 , C07C1/00 , C07C13/15 , C10G3/00 , C07D307/33
CPC classification number: C10G3/44 , C07D307/33 , C10G2400/04 , Y02P30/20
Abstract: Methods are disclosed for converting a biomass-derived product containing levulinic acid and/or gamma-valerolactone to a transportation fuel precursor product containing diesel like hydrocarbons. These methods are expected to produce fuel products at a reduced cost relative to conventional approaches.
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9.发明申请公开(公告)号：US20160281246A1
公开(公告)日：2016-09-29
申请号：US15078784
申请日：2016-03-23
Applicant: BATTELLE MEMORIAL INSTITUTE , BATTELLE ENERGY ALLIANCE, LLC
Inventor： Michael A. Lilga , Asanga B. Padmaperuma , Tedd E. Lister , Eric J. Dufek , Lucia M. Petkovic , Luis A. Diaz-Aldana
CPC classification number: C25B3/04 , C07B31/00 , C07C1/24 , C25B1/04 , C25B9/04 , C25B9/08 , C25B15/02 , C25B15/08 , Y02E60/366 , C07C11/02
Abstract: A system and process are disclosed for electrochemically upgrading bio-oils and bio-crudes that enhance yields of selected reduction products for subsequent production of bio-based fuels.
Abstract translation: 公开了用于电化学升级生物油和生物原油的系统和方法，其提高了所选择的还原产物的产量，用于随后生产生物基燃料。
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公开(公告)号：US09434659B2
公开(公告)日：2016-09-06
申请号：US14607871
申请日：2015-01-28
Applicant: Battelle Memorial Institute
Inventor： Michael A. Lilga , John G. Frye, Jr. , Suh-Jane Lee , Karl O. Albrecht
CPC classification number: C07C1/24 , B01J19/00 , B01J21/066 , B01J21/08 , B01J23/06 , B01J23/08 , B01J23/10 , B01J27/1806 , B01J37/031 , B01J37/04 , B01J37/086 , B01J37/088 , B01J2523/00 , B01J2523/33 , B01J2523/35 , B01J2523/3781 , B01J2523/48 , C07C1/2078 , C07C1/30 , C07C29/60 , C07C49/203 , C07C2521/04 , C07C2521/06 , C07C2523/02 , C07C2523/08 , C07C2523/10 , C07C2527/167 , C07C2529/40 , C07C2529/70 , C07C33/03 , C07C11/167 , B01J2523/31 , B01J2523/3706 , B01J2523/23 , B01J2523/3762 , B01J2523/3775 , B01J2523/3793 , B01J2523/27 , B01J2523/3743 , B01J2523/36 , B01J2523/25 , B01J2523/51 , B01J2523/11 , B01J2523/305 , B01J2523/22 , B01J2523/375 , B01J2523/3768 , B01J2523/3725 , B01J2523/3718 , B01J2523/3737 , B01J2523/3756 , B01J2523/3787 , B01J2523/3712 , B01J2523/68 , B01J2523/49 , B01J2523/69 , B01J2523/41
Abstract: A composition comprising 2,3-butanediol is dehydrated to methyl vinyl carbinol and/or 1,3-butadiene by exposure to a catalyst comprising (a) MxOy wherein M is a rare earth metal, a group IIIA metal, Zr, or a combination thereof, and x and y are based upon an oxidation state of M, or (b) M3a(PO4)b where M3 is a group IA, a group IIA metal, a group IIIA metal, or a combination thereof, and a and b are based upon the oxidation state of M3. Embodiments of the catalyst comprising MxOy may further include M2, wherein M2 is a rare earth metal, a group IIA metal, Zr, Al, or a combination thereof. In some embodiments, 2,3-butanediol is dehydrated to methyl vinyl carbinol and/or 1,3-butadiene by a catalyst comprising MxOy, and the methyl vinyl carbinol is subsequently dehydrated to 1,3-butadiene by exposure to a solid acid catalyst.
Abstract translation: 将包含2,3-丁二醇的组合物通过暴露于包含（a）M x Oy的催化剂脱水成甲基乙烯基甲醇和/或1,3-丁二烯，其中M是稀土金属，IIIA族金属，Zr或组合 并且x和y基于M的氧化态，或（b）M3a（PO4）b，其中M3是IA族，IIA族金属，IIIA族金属或其组合，a和b 是基于M3的氧化态。 包含M x O y的催化剂的实施方案可以进一步包括M2，其中M2是稀土金属，IIA族金属，Zr，Al或它们的组合。 在一些实施方案中，通过包含M x O y的催化剂将2,3-丁二醇脱水成甲基乙烯基甲醇和/或1,3-丁二烯，然后通过暴露于固体酸催化剂将甲基乙烯基甲醇脱水为1,3-丁二烯 。
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