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1.发明授权Continuous process and apparatus for the efficient conversion of inorganic solid particles 有权用于有机转化无机固体颗粒的连续工艺和设备公开(公告)号：US06903040B2
公开(公告)日：2005-06-07
申请号：US10141800
申请日：2002-05-08
IPC分类号： C01G9/00 , B01J19/10 , B01J19/12 , B01J19/18 , B01J19/26 , B01J20/10 , B01J20/12 , B01J20/18 , B01J20/30 , B01J21/04 , B01J23/00 , B01J35/02 , B01J37/04 , C01B25/26 , C01B33/193 , C01B33/22 , C01B33/26 , C01B33/40 , C01B39/04 , C01B39/38 , C01B39/40 , C01F7/00 , C01F7/02 , C01F7/06 , C01F7/44 , C01G25/00 , C01G25/02 , C01G25/06 , B01J29/06
CPC分类号： C01F7/448 , B01J19/10 , B01J19/1862 , B01J20/041 , B01J20/043 , B01J20/06 , B01J20/10 , B01J20/12 , B01J20/18 , B01J20/30 , B01J21/04 , B01J23/007 , B01J35/023 , B01J37/04 , B01J2219/00033 , B01J2219/0004 , B01J2219/00141 , C01B39/38 , C01F7/02 , C01F7/062 , C01G25/02 , C01G25/06 , C01P2002/02 , C01P2002/04 , C01P2004/61 , C01P2004/62 , C01P2004/80 , C01P2006/12 , C01P2006/14
摘要： The invention pertains to a continuous process for the conversion of inorganic solid starting particles which either are amorphous or possess a degree of order into inorganic solid product particles which (a) when the starting particles are amorphous, possess a degree of order, or (b) when the starting particles possess a degree of order, possess a different order, a different degree of order, or no order, which product particles are suitable for use in or as a catalyst, in or as a carrier, or in or as an adsorbent, in which process the starting particles are dispersed in a liquid thus forming a suspension. The suspension flows through at least two separate conversion vessels (3) which are connected in series and the suspension is agitated in each of these vessels (3). The invention furthermore relates to an apparatus suitable for carrying out the process according to the invention. This invention allows the processing of suspension with a high Solids to Liquid Ratio.
摘要翻译： 本发明涉及将无定形或具有一定程度的无定形或无级固体的无机固体起始颗粒转化成无机固体产物颗粒的连续方法，（a）当起始颗粒是无定形的，具有一定程度时，或（b ）当起始颗粒具有一定程度的顺序时，具有不同的顺序，不同的顺序或顺序，哪些产物颗粒适合用作催化剂或作为催化剂，或作为载体，或作为或作为 吸附剂，其中起始颗粒分散在液体中，从而形成悬浮液。 悬浮液通过串联连接的至少两个分离的转化容器（3），并且悬浮液在这些容器（3）中的每一个中被搅动。 本发明还涉及适用于实施本发明方法的设备。 本发明允许处理具有高固体与液体比的悬浮液。
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2.发明授权Process for the preparation of doped pentasil-type zeolites using a doped reactant 有权使用掺杂的反应物制备掺杂的pentasil型沸石的方法公开(公告)号：US06969692B2
公开(公告)日：2005-11-29
申请号：US10647632
申请日：2003-08-25
申请人： Mike Brady , Erik Jeroen Laheij , Paul O'Connor , Dennis Stamires
发明人： Mike Brady , Erik Jeroen Laheij , Paul O'Connor , Dennis Stamires
CPC分类号： B01J29/04 , B01J29/405 , C01B39/06 , C01B39/065
摘要： A process for the preparation of a metal-doped pentasil-type zeolite comprising the steps of: a) preparing an aqueous precursor mixture comprising a silicon source and an aluminum source, at least one of these sources being doped with a rare earth metal or a transition metal of Groups Vb–VIIIb, Ib, or IIb of the Periodic System, and b) thermally treating the precursor mixture to form a metal-doped pentasil-type zeolite. With this process, metal-doped pentasil-type zeolites can be prepared while the risk of precipitation of the dopant as a separate phase is minimized.
摘要翻译： 一种制备金属掺杂的pentasil型沸石的方法，包括以下步骤：a）制备包含硅源和铝源的水性前体混合物，这些源中的至少一个掺杂有稀土金属或 元素周期系Vb-VIIIb族，Ib族或IIb族的过渡金属，和b）热处理前体混合物以形成金属掺杂的pentasil型沸石。 通过该方法，可以制备金属掺杂的pentasil型沸石，同时使作为分离相的掺杂剂的沉淀的风险最小化。
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公开(公告)号：US20080210600A1
公开(公告)日：2008-09-04
申请号：US11629053
申请日：2005-06-16
申请人： Paul O'Connor , Erik Jeroen Laheij , Dennis Stamires , Michael F. Brady , Francisco Rene Mas Cabre , Oscar Rene Chamberlain Pravia , Henrique Soares Cerqueira , Fabio Lopes De Azevedo
发明人： Paul O'Connor , Erik Jeroen Laheij , Dennis Stamires , Michael F. Brady , Francisco Rene Mas Cabre , Oscar Rene Chamberlain Pravia , Henrique Soares Cerqueira , Fabio Lopes De Azevedo
IPC分类号： C10G11/00
CPC分类号： C10G55/06 , B01J23/007 , C10G11/16 , C10G11/18 , C10G69/02
摘要： Process for upgrading a liquid hydrocarbon feed comprising the steps of (a) preparing a slurry comprising the hydrocarbon feed having a boiling range above 350° C. and solid particles comprising a rehydratable material, (b) thermally treating said slurry at a temperature in the range of 250 to 550° C., (c) optionally separating the thermally treated slurry into (I) a lower boiling fraction and (ii) a higher boiling fraction containing the solid particles and formed coke, if any, and (d) separating the solid particles and formed coke, if any, from the thermally treated slurry resulting from step b) or the higher boiling fraction of step c).
摘要翻译： 用于升级液体烃进料的方法，包括以下步骤：（a）制备包含沸点范围高于350℃的烃进料的浆料和包含可再水化材料的固体颗粒，（b）在所述浆料的温度下热处理所述浆料 范围为250至550℃，（c）任选将热处理浆料分离成（I）低沸点馏分和（ii）含有固体颗粒和成型焦炭的较高沸点馏分（如果有的话），和（d）分离 固体颗粒和形成的焦炭（如果有的话）来自步骤b）得到的热处理浆料或步骤c）的较高沸点馏分。
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公开(公告)号：US07217400B2
公开(公告)日：2007-05-15
申请号：US10642893
申请日：2003-08-18
申请人： Edgar Evert Steenwinkel , Johannes Petrus Jozef Verlaan , Marieke Paulyne Renate Spee , Erik Jeroen Laheij , Paul O'Connor , Dennis Stamires
发明人： Edgar Evert Steenwinkel , Johannes Petrus Jozef Verlaan , Marieke Paulyne Renate Spee , Erik Jeroen Laheij , Paul O'Connor , Dennis Stamires
CPC分类号： C01G49/0063 , C01G49/0018 , C01G49/0054 , C01G49/02 , C01G49/06 , C01P2002/54 , C01P2006/12
摘要： An apparatus and continuous process for the conversion of one solid iron compound to another solid iron compound in a heterogeneous suspension wherein the suspension is formed by dispersing a solid starting iron compound in a liquid that is continuously fed through one or more agitated conversion vessels under hydrothermal conditions and converted to a solid product iron compound having different physical, chemical, or structural properties from the solid starting iron compound.
摘要翻译： 一种用于在非均相悬浮液中将一种固体铁化合物转化成另一种固体铁化合物的装置和连续方法，其中悬浮液通过将固体起始铁化合物分散在液体中而形成，该液体通过一个或多个搅拌转化容器在水热 转化成具有与固体起始铁化合物不同的物理，化学或结构特性的固体产物铁化合物。
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公开(公告)号：US07824540B2
公开(公告)日：2010-11-02
申请号：US11629053
申请日：2005-06-16
申请人： Paul O'Connor , Erik Jeroen Laheij , Dennis Stamires , Michael F. Brady , Francisco René Mas Cabre , Oscar René Chamberlain Pravia , Henrique Soares Cerqueira , Fabió Lopes De Azevedo
发明人： Paul O'Connor , Erik Jeroen Laheij , Dennis Stamires , Michael F. Brady , Francisco René Mas Cabre , Oscar René Chamberlain Pravia , Henrique Soares Cerqueira , Fabió Lopes De Azevedo
IPC分类号： C10G9/28
CPC分类号： C10G55/06 , B01J23/007 , C10G11/16 , C10G11/18 , C10G69/02
摘要： Process for upgrading a liquid hydrocarbon feed comprising the steps of (a) preparing a slurry comprising the hydrocarbon feed having a boiling range above 350° C. and solid particles comprising a rehydratable material, (b) thermally treating said slurry at a temperature in the range of 250 to 550° C., (c) optionally separating the thermally treated slurry into (I) a lower boiling fraction and (ii) a higher boiling fraction containing the solid particles and formed coke, if any, and (d) separating the solid particles and formed coke, if any, from the thermally treated slurry resulting from step b) or the higher boiling fraction of step c).
摘要翻译： 用于升级液体烃进料的方法，包括以下步骤：（a）制备包含沸点范围高于350℃的烃进料的浆料和包含可再水化材料的固体颗粒，（b）在所述浆料的温度下热处理所述浆料 范围为250至550℃，（c）任选将热处理浆料分离成（I）低沸点馏分和（ii）含有固体颗粒和成型焦炭的较高沸点馏分（如果有的话），和（d）分离 固体颗粒和形成的焦炭（如果有的话）来自步骤b）得到的热处理浆料或步骤c）的较高沸点馏分。
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公开(公告)号：US09643166B2
公开(公告)日：2017-05-09
申请号：US11722388
申请日：2005-12-20
IPC分类号： B01J29/08 , B01D53/94 , B01J29/06 , B01J37/00 , C01B3/02 , C10G1/08 , C10G2/00 , C10G11/05 , C10G29/20 , C10G35/06 , C10G49/08 , B01J35/00
CPC分类号： B01J29/084 , B01D53/94 , B01J29/06 , B01J35/002 , B01J37/0045 , B01J2229/42 , C01B3/02 , C01B2203/1041 , C10G1/086 , C10G2/33 , C10G11/05 , C10G29/205 , C10G35/06 , C10G49/08
摘要： A process for preparing a catalyst is disclosed. The process generally comprises the steps of: (a) preparing a slurry comprising clay, zeolite, a sodium-free silica source, quasi-crystalline boehmite, and micro-crystalline boehmite, provided that the slurry does not comprise peptized quasi-crystalline boehmite; (b) adding a monovalent acid to the slurry; (c) adjusting the pH of the slurry to a value above about 3, and (d) shaping the slurry to form particles. This process results in attrition resistant catalysts with a good accessibility.
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公开(公告)号：US08088354B2
公开(公告)日：2012-01-03
申请号：US10579595
申请日：2004-11-19
申请人： Erik Jeroen Laheij , Paul O'Connor , Dennis Stamires , Edisson Morgado, Jr. , Marco Antonio Santos de Abreu , Márcio Fernandes , Michael Brady
发明人： Erik Jeroen Laheij , Paul O'Connor , Dennis Stamires , Edisson Morgado, Jr. , Marco Antonio Santos de Abreu , Márcio Fernandes , Michael Brady
IPC分类号： C01F7/02
CPC分类号： C04B35/6303 , B82Y30/00 , C01F7/02 , C01F7/34 , C01F7/448 , C01P2002/04 , C01P2002/70 , C01P2004/62 , C01P2004/64 , C04B35/62605 , C04B35/63 , C04B2235/3218 , C04B2235/5454 , C04B2235/549
摘要： Process for the preparation of quasi-crystalline boehmite comprising the steps of: (a) preparing an aqueous precursor mixture comprising a water-insoluble aluminum source; (b) decreasing the pH of the precursor mixture of step (a) by at least 2 units; (c) increasing the pH of the mixture of step (b) by at least 2 units, and (d) aging the mixture of step (c) under hydrothermal conditions to form a quasi-crystalline boehmite. This process provides for the hydrothermal preparation of quasi-crystalline boehmites with high peptizability. The invention therefore further relates to quasi-crystalline boehmites with a high peptizability, measured as the Z-average submicron particle size. This Z-average submicron particle size preferably is less than 500 nm, more preferably less than 300 nm, even more preferably less than 200 nm, and most preferably less than 100 nm.
摘要翻译： 制备准晶体勃姆石的方法，包括以下步骤：（a）制备包含水不溶性铝源的水性前体混合物; （b）将步骤（a）的前体混合物的pH降低至少2单位; （c）将步骤（b）的混合物的pH提高至少2单位，和（d）在水热条件下老化步骤（c）的混合物以形成准结晶勃姆石。 该方法提供了具有高可溶性性的准晶体沸石的水热制备。 因此，本发明进一步涉及具有高可溶性性的准晶体沸石，其测量为Z-平均亚微米粒度。 该Z平均亚微米粒径优选小于500nm，更优选小于300nm，甚至更优选小于200nm，最优选小于100nm。
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公开(公告)号：US20080210599A1
公开(公告)日：2008-09-04
申请号：US11813659
申请日：2006-01-06
申请人： Paul O'Connor , Erik Jeroen Laheij , Dennis Stamires , Oscar Rene Chamberlain Pravia , Rodolfo Eugenio Roncolatto , Yiu Lau Lam
发明人： Paul O'Connor , Erik Jeroen Laheij , Dennis Stamires , Oscar Rene Chamberlain Pravia , Rodolfo Eugenio Roncolatto , Yiu Lau Lam
CPC分类号： B01J38/60 , B01J21/16 , B01J23/007 , B01J29/06 , B01J29/084 , B01J29/088 , B01J29/90 , B01J38/62 , B01J38/66 , B01J2229/37 , B01J2229/42 , C10G11/05 , C10G11/18 , C10G29/00 , C10G49/02
摘要： “FCC equilibrium catalysts, even when highly contaminated with vanadium, can be upgraded to make them suitable again for use in catalytic processes, for instance, as catalyst additives in FCC, by employing a process comprising the steps of (a) treating an FCC equilibrium catalyst that contains alumina and zeolite with an acidic solution to obtain an acid-treated equilibrium catalyst, and (b) contacting the acid-treated equilibrium catalyst with an aqueous solution or suspension of a divalent metal compound.”
摘要翻译： 即使高度被钒污染的FCC平衡催化剂也可以升级，以使其再次适用于催化过程，例如FCC中的催化剂添加剂，通过采用包括以下步骤的方法：（a）处理FCC平衡 催化剂，其含有氧化铝和沸石与酸性溶液以获得酸处理的平衡催化剂，和（b）使酸处理的平衡催化剂与二价金属化合物的水溶液或悬浮液接触。
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9.发明申请Oxidic Metal Composition, Its Preparation And Use As Catalyst Composition 审中-公开氧化金属组合物，其制备和用作催化剂组合物公开(公告)号：US20090269266A1
公开(公告)日：2009-10-29
申请号：US11915708
申请日：2006-06-02
IPC分类号： B01D53/50 , B01J23/10 , B01J23/02 , B01J27/236 , B01J27/232
CPC分类号： C10G11/18 , B01J21/063 , B01J21/066 , B01J23/002 , B01J23/10 , B01J23/22 , B01J23/30 , B01J23/34 , B01J23/40 , B01J23/63 , B01J23/6522 , B01J23/85 , B01J23/888 , B01J23/889 , B01J23/8906 , B01J29/06 , B01J29/084 , B01J35/0006 , B01J37/0045 , B01J37/03 , B01J37/036 , B01J2523/00 , C10G11/05 , B01J2523/3712 , B01J2523/47 , B01J2523/69 , B01J2523/48 , B01J2523/55 , B01J2523/842 , B01J2523/822
摘要： Oxidic composition consisting essentially of oxidic forms of a first metal, a second metal, and optionally a third metal, the first metal being either Ca or Ba and being present in the composition in an amount of from about 5 to about 80 wt %, the second metal being Al and being present in the composition in an amount of from about 5 to about 80 wt %, the third metal being selected from the group consisting of La, Ti, and Zr, and being present in an amount of from 0 to about 17 wt %—all weight percentages calculated as oxides and based on the weight of the oxidic composition, the oxidic composition being obtainable by(a) preparing a physical mixture comprising solid compounds of the first, the second, and the optional third metal, (b) optionally aging the physical mixture, without anionic clay being formed, and (c) calcining the mixture.This composition is suitable for use in FCC processes for the passivation of metals with only minimal influence on the zeolite's hydrothermal stability.
摘要翻译： 基本上由第一金属，第二金属和任选的第三金属的氧化形式组成的氧化组合物，第一金属是Ca或Ba，并且以约5至约80wt％的量存在于组合物中， 第二金属为Al，并且以约5至约80重量％的量存在于组合物中，第三金属选自La，Ti和Zr，并且以0至 约17重量％的重量百分比计算为氧化物，并且基于氧化组合物的重量，氧化组合物可通过（a）制备包含第一，第二和任选的第三金属的固体化合物的物理混合物获得， （b）任选地老化物理混合物，而不形成阴离子粘土，和（c）煅烧该混合物。 该组合物适用于FCC工艺中钝化金属，对沸石的水热稳定性影响最小。
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公开(公告)号：US07448561B2
公开(公告)日：2008-11-11
申请号：US10536340
申请日：2003-12-02
IPC分类号： B02C19/18
CPC分类号： C01F7/005 , B01J3/008 , B01J8/20 , B01J16/00 , B01J2208/00672 , B01J2219/0004 , B82Y30/00 , C01B13/366 , C01B39/38 , C01P2004/62 , C01P2004/64 , C01P2006/22 , Y02P20/544
摘要： A combined process for the conversion of solid starting particles into solid intermediate particles and reducing the median diameter of the intermediate particles to obtain product particles. This process involves flowing a suspension of starting particles through a series of at least two conversion vessels, thereby converting at least part of the starting particles into intermediate particles, adding a supercritical fluid to one or more of the conversion vessels, thereby forming a supercritical suspension, and releasing pressure from the supercritical suspension, thereby expanding the suspension and converting the intermediate particles into product particles.
摘要翻译： 用于将固体起始颗粒转化成固体中间体颗粒并降低中间颗粒的中值直径以获得产物颗粒的组合方法。 该方法包括使起始颗粒的悬浮液流过一系列至少两个转化容器，从而将至少部分起始颗粒转化为中间体颗粒，向一个或多个转化容器中加入超临界流体，从而形成超临界悬浮液 并从超临界悬浮液释放压力，从而使悬浮液膨胀并将中间颗粒转化成产物颗粒。
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