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    Preparation of amines
    2.
    发明授权
    Preparation of amines 失效
    胺的制备

    公开(公告)号：US5530127A

    公开(公告)日：1996-06-25

    申请号：US509997

    申请日：1995-08-01

    申请人： Wolfgang Reif ,  Lothar Franz ,  Peter Stops ,  Volkmar Menger ,  Rainer Becker ,  Rudolf Kummer ,  Siegfried Winderl

    发明人： Wolfgang Reif ,  Lothar Franz ,  Peter Stops ,  Volkmar Menger ,  Rainer Becker ,  Rudolf Kummer ,  Siegfried Winderl

    IPC分类号： B01J23/88 ,  B01J21/06 ,  B01J23/885 ,  B01J37/03 ,  C07C209/08 ,  C07C209/16 ,  C07C209/18 ,  C07C211/03 ,  C07D295/023

    CPC分类号： C07C209/18 ,  C07C209/16 ,  B01J21/066 ,  B01J23/885 ,  B01J37/03 ,  Y02P20/582

    摘要： A process for the preparatiion of an amine which comprises reacting a primary or secondary alcohol and a nitrogen compound selected from the group consisting of ammonia and primary and secondary amines, at temperatures of from 80.degree. to 250.degree. C. and pressures of from 1 to 400 bar using hydrogen in the presence of a zirconium/copper/nickel catalyst, wherein the catalytically active material contains from 20 to 85 wt % of oxygen-containing zirconium compounds, calculated as ZrO.sub.2, from 1 to 30 wt % of oxygen-containing compounds of copper, calculated as CuO, from 30 to 70 wt % of oxygen-containing compounds of nickel, calculated as NiO, from 0.1 to 5 wt % of oxygen-containing compounds of molybdenum, calculated as MoO.sub.3 and from 0 to 10 wt % of oxygen-containing compounds of aluminum and/or manganese, calculated as Al.sub.2 O.sub.3 or MnO.sub.2, respectively.

    摘要翻译： 一种制备胺的方法，其包括使伯醇或仲醇与选自氨和伯胺和仲胺的氮化合物在80-250℃的温度和1至 400巴，在锆/铜/镍催化剂存在下使用氢，其中催化活性材料含有20至85重量％的以ZrO 2计算的含氧锆化合物，1至30重量％的含氧化合物 以CuO计，以NiO计的含氧化合物的含量为30-70重量％的以氧化钼计的含氧​​化合物的重量百分比为0.1-70重量％，以氧化钼计为0.0-10重量％ 分别以Al2O3或MnO2计算的铝和/或锰的含氧化合物。

    Process for preparation of diamines by catalytic amination of aminoalcohols
    4.
    发明授权
    Process for preparation of diamines by catalytic amination of aminoalcohols 失效
    通过氨基醇的催化胺化制备二胺的方法

    公开(公告)号：US5608113A

    公开(公告)日：1997-03-04

    申请号：US513632

    申请日：1995-08-10

    申请人： Rainer Becker ,  Volkmar Menger ,  Wolfgang Reif ,  Andreas Henne

    发明人： Rainer Becker ,  Volkmar Menger ,  Wolfgang Reif ,  Andreas Henne

    IPC分类号： B01J23/88 ,  B01J21/06 ,  B01J23/755 ,  B01J37/03 ,  C07B61/00 ,  C07C209/16 ,  C07C211/09

    CPC分类号： C07C209/16 ,  B01J21/066 ,  B01J23/755 ,  B01J37/03 ,  Y02P20/582

    摘要： In a process for preparing diamines from aminoalcohols and nitrogen compounds selected from the group consisting of ammonia and primary and secondary amines at from 80.degree. to 250.degree. C. and pressures of from 1 to 400 bar using hydrogen in the presence of a zirconium, copper, nickel catalyst, the catalytically active composition comprises from 20 to 85% by weight of oxygen-containing zirconium compounds, calculated as ZrO.sub.2, from 1 to 30% by weight of oxygen-containing compounds of copper, calculated as CuO, from 30 to 70% by weight of oxygen-containing compounds of nickel, calculated as NiO, from 0.1 to 5% by weight of oxygen-containing compounds of molybdenum, calculated as MoO.sub.3, and from 0 to 10% by weight of oxygen-containing compounds of aluminum and/or manganese, calculated as Al.sub.2 O.sub.3 and MnO.sub.2 respectively.

    摘要翻译： 在使用氢存在下，在锆存在下，使用氢气从80℃至250℃，压力为1至400巴的氨基和伯胺和仲胺从氨基醇和氮化合物中制备二胺的方法中， 镍催化剂，催化活性组合物包含20至85重量％的以ZrO 2计算的含氧锆化合物，1至30重量％的以CuO计的含氧化合物铜30至70 按NiO计的含镍化合物的重量百分比为0.1至5重量％的按MoO 3计算的含氧化合物的钼和0至10重量％的含氧化合物的铝和 /或锰，分别计算为Al2O3和MnO2。

    Device for connecting components with various electrical potentials and subject to vibration
    7.
    发明授权
    Device for connecting components with various electrical potentials and subject to vibration 失效
    用于连接具有各种电位并受振动的部件的装置

    公开(公告)号：US06722907B2

    公开(公告)日：2004-04-20

    申请号：US10239108

    申请日：2002-09-19

    申请人： Peter-Josef Bauer ,  Thomas Lott ,  Rainer Becker ,  Michael Speth ,  Christian Meyer

    发明人： Peter-Josef Bauer ,  Thomas Lott ,  Rainer Becker ,  Michael Speth ,  Christian Meyer

    IPC分类号： H01R13627

    CPC分类号： H02K5/24 ,  H02K11/33

    摘要： The invention concerns a device for connecting vibrating components having different electric potentials, in particular for connecting a stator housing (8) for an electric motor (1) with a housing (4) for control electronics (6) inside a clutch actuator of a motor vehicle, containing electrical contact means (30) for establishing an electrically conductive connection between the components, and means (26) for establishing its mechanical connection. The invention provides that the means for establishing the mechanical connection have at least one plastic ring (26) held in an opening (16) of a first component (2, 4, 6) and a neck-shaped attachment segment (14) formed in a second component (1, 8), whereby, by pushing the neck-shaped attachment segment (14) of the second component (1, 8) into the opening (16) of the first component (2, 4, 6), the plastic ring (26) can be compressed in the radial direction, forming a non-positive connection between the two components, and, simultaneously, the electrical contact means (30) can be engaged with each other.

    摘要翻译： 本发明涉及用于连接具有不同电位的振动部件的装置，特别是用于将用于电动机（1）的定子壳体（8）与电动机的离合器致动器内的控制电子装置（6）连接的壳体（4） 车辆，包含用于在所述部件之间建立导电连接的电接触装置（30），以及用于建立其机械连接的装置（26）。本发明提供用于建立机械连接的装置具有至少一个塑料环（26） 保持在形成在第二部件（1,8）中的第一部件（2,4,6）和颈部附接部分（14）的开口（16）中，由此通过将颈部附接部分 第二部件（1,8）的第二部件（14）插入到第一部件（2,4,6）的开口（16）中，塑料环（26）可以沿径向方向被压缩，从而在第二部件 两个组成部分，同时， 电接触装置（30）可彼此接合。

    Catalyst and method for the production of polytetrahydrofuran
    8.
    发明授权
    Catalyst and method for the production of polytetrahydrofuran 失效
    用于生产聚四氢呋喃的催化剂和方法

    公开(公告)号：US06362312B1

    公开(公告)日：2002-03-26

    申请号：US09529180

    申请日：2000-04-10

    申请人： Karsten Eller ,  Heinz Rütter ,  Michael Hesse ,  Rainer Becker

    发明人： Karsten Eller ,  Heinz Rütter ,  Michael Hesse ,  Rainer Becker

    IPC分类号： C07C4311

    CPC分类号： C08G65/20 ,  C08G61/125 ,  C08G65/2657

    摘要： In a process for preparing polytetrahydrofuran, polytetrahydrofuran copolymers or diesters or monoesters thereof comprises polymerizing tetrahydrofuran in the presence of at least one telogen and/or comonomer over an acid-activated calcium montmorillonite as catalyst, the calcium montmorillonite has a BET surface area of at least 300 m2/g, an acidity of at least 0.02 mmol/g at pKa

    摘要翻译： 在制备聚四氢呋喃的方法中，聚四氢呋喃共聚物或二酯或其单酯包括在至少一种前体和/或共聚单体存在下，在酸活化的钙蒙脱石作为催化剂上聚合四氢呋喃，所述钙蒙脱石的BET表面积至少为 300m 2 / g，在pKa <3时酸度至少为0.02mmol / g，孔径在30至200之间的孔体积至少为0.40cm 3 / g。

    Method for producing polytetrahydrofuran with low color index
    9.
    发明授权
    Method for producing polytetrahydrofuran with low color index 失效
    低颜色指数聚四氢呋喃的制备方法

    公开(公告)号：US06197979B1

    公开(公告)日：2001-03-06

    申请号：US09485459

    申请日：2000-02-10

    申请人： Rainer Becker ,  Karsten Eller ,  Heinz Rütter ,  Michael Hesse

    发明人： Rainer Becker ,  Karsten Eller ,  Heinz Rütter ,  Michael Hesse

    IPC分类号： C07D30793

    CPC分类号： C08G65/20 ,  B01J23/24

    摘要： In a process for preparing polytetrahydrofuran, tetrahydrofuran copolymers, diesters or monoesters of these polymers having a low color number by polymerization of tetrahydrofuran in the presence of at least one telogen and/or comonomer over a heterogeneous catalyst, the polymerization is carried out in the presence of hydrogen.

    摘要翻译： 在通过在非均相催化剂的存在下，在至少一种环糊精和/或共聚单体的存在下通过四氢呋喃聚合而制备聚四氢呋喃的这些聚合物的四氢呋喃共聚物，二酯或单酯具有低色数的聚合反应在存在下进行 的氢。

    Removal of halides from halide-containing nitrile mixtures
    10.
    发明授权
    Removal of halides from halide-containing nitrile mixtures 失效
    从含卤素腈混合物中除去卤化物

    公开(公告)号：US6153784A

    公开(公告)日：2000-11-28

    申请号：US24457

    申请日：1998-02-17

    申请人： Heinz-Josef Kneuper ,  Hans-Jurgen Weyer ,  Horst Neuhauser ,  Johann-Peter Melder ,  Andreas Henne ,  Karl-Heinz Ross ,  Rainer Becker

    发明人： Heinz-Josef Kneuper ,  Hans-Jurgen Weyer ,  Horst Neuhauser ,  Johann-Peter Melder ,  Andreas Henne ,  Karl-Heinz Ross ,  Rainer Becker

    IPC分类号： B01J27/18 ,  B01J31/02 ,  C07B61/00 ,  C07C209/48 ,  C07C211/09 ,  C07C253/14 ,  C07C253/34 ,  C07C255/04

    CPC分类号： C07C253/14 ,  C07C209/48 ,  C07C253/34

    摘要： Halides are removed from halide-containing nitrile mixtures by(a) thermally treating the halide-containing nitrile mixture,(b) subsequently adding a base to the thermally treated nitrile mixture and(c) subsequently separating off the base from the nitrile mixture.Amines are prepared by(A) reacting alkyl halides with metal cyanides in an at least two-phase reaction medium in the presence of halide-containing phase-transfer catalysts to give alkanenitriles,(B) separating off the resulting halide-containing alkanenitrile mixture phase and(C) further treating the halide-containing alkanenitrile mixture phase, as described in the stages(a)-(c) removing halides from halide-containing nitrile mixtures and(d) hydrogenating nitrites obtained in stage (c) to give amines, in the presence of suspended or fixed-bed catalysts.

    摘要翻译： 通过（a）热处理含卤素腈混合物，（b）随后向经热处理的腈混合物中加入碱，和（c）随后将腈与腈混合物分离，从卤化物腈混合物中除去卤化物。 胺通过（A）在卤化物相转移催化剂存在下在至少两相反应介质中将烷基卤与金属氰化物反应得到烷腈，（B）将所得的含卤素的烷腈混合物相分离 （C）进一步处理含卤化物的腈腈混合物相，如步骤（a） - （c）所述从卤化物腈混合物中除去卤化物，和（d）氢化阶段（c）中得到的亚硝酸盐，得到胺， 在悬浮或固定床催化剂存在下。