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公开(公告)号：US20080169221A1
公开(公告)日：2008-07-17
申请号：US11622731
申请日：2007-01-12
CPC分类号： C10G25/00 , B01J20/12 , B01J20/20 , C10G25/003
摘要： A method for treating crude or residual fuel oil includes extracting vanadium from the fuel oil by contacting the fuel oil with an adsorbent and a solvent. The adsorbent may be modified with a compound having both acidic functionality and basic functionality. The method provides effective removal of vanadium from crude or residual fuel oil at moderate temperatures.
摘要翻译： 用于处理粗油或残余燃料油的方法包括通过使燃料油与吸附剂和溶剂接触从燃料油中提取钒。 吸附剂可以用具有酸性官能度和碱性官能团的化合物进行改性。 该方法在中等温度下有效地从原油或残余燃料油中除去钒。
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公开(公告)号：US07967976B2
公开(公告)日：2011-06-28
申请号：US11622731
申请日：2007-01-12
CPC分类号： C10G25/00 , B01J20/12 , B01J20/20 , C10G25/003
摘要： A method for treating crude or residual fuel oil includes extracting vanadium from the fuel oil by contacting the fuel oil with an adsorbent and a solvent. The adsorbent may be modified with a compound having both acidic functionality and basic functionality. The method provides effective removal of vanadium from crude or residual fuel oil at moderate temperatures.
摘要翻译： 用于处理粗油或残余燃料油的方法包括通过使燃料油与吸附剂和溶剂接触从燃料油中提取钒。 吸附剂可以用具有酸性官能度和碱性官能团的化合物进行改性。 该方法在中等温度下有效地从原油或残余燃料油中除去钒。
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公开(公告)号：US20130134098A1
公开(公告)日：2013-05-30
申请号：US13307656
申请日：2011-11-30
申请人： William Leonard Kostedt, IV , James Manio Silva , Hope Matis , Vicki Herzl Watkins , Harish Radhakrishna Acharya
发明人： William Leonard Kostedt, IV , James Manio Silva , Hope Matis , Vicki Herzl Watkins , Harish Radhakrishna Acharya
CPC分类号： C02F1/281 , B01J20/06 , B01J20/28009 , B01J20/3433 , B01J20/3475 , B01J2220/42 , B03C1/01 , B03C2201/18 , C02F1/041 , C02F1/08 , C02F1/288 , C02F1/488 , C02F1/5236 , C02F1/66 , C02F5/06 , C02F2001/5218 , C02F2101/006 , C02F2101/10 , C02F2101/20 , C02F2103/10 , C02F2303/16
摘要： Methods for treating water to remove radium include contacting the water with a magnetic adsorbent comprising manganese oxide(s), and applying a magnetic field to separate the magnetic adsorbent from the water, whereby radium is removed from the water. The methods may additionally include regenerating the magnetic adsorbent, and contacting the water with regenerated magnetic adsorbent. Alternately, calcium and/or strontium may be precipitated as carbonate salts from lime-treated water containing radium and barium without precipitating a significant fraction of the barium or radium; and removing radium from calcium- and strontium-free water by precipitating the barium and radium as carbonate salts. The barium- and radium carbonate precipitate may be redissolved in hydrochloric acid and disposed of by deep-well injection.
摘要翻译： 用于处理水以去除镭的方法包括使水与包含氧化锰的磁性吸附剂接触，并施加磁场以将磁性吸附剂与水分离，从而从水中除去镭。 所述方法还可包括再生磁吸附剂，并使水与再生磁吸附剂接触。 或者，钙和/或锶可以从含有镭和钡的石灰处理水中以碳酸盐形式沉淀而不沉淀出大部分的钡或镭; 并通过沉淀钡和镭作为碳酸盐，从钙和无锶水中去除镭。 碳酸钡和镭碳酸盐沉淀可以重新溶解在盐酸中，并通过深井注射进行处理。
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4.发明授权公开(公告)号：US06870013B2
公开(公告)日：2005-03-22
申请号：US10638622
申请日：2003-08-08
IPC分类号： C08G64/18 , C08G64/24 , C08G77/448 , C08G77/04
CPC分类号： C08G77/448 , C08G64/186 , C08G64/24 , C08G77/24 , C08G77/80
摘要： Copolyorganosiloxanecarbonates are prepared by first preparing an oligomeric aromatic polycarbonate, such as an oligomeric bisphenol A polycarbonate, in the presence of a tertiary amine as the only catalyst species; contacting the oligomeric polycarbonate mixture with a polyorganosiloxane bis(aryl)chloroformate, such as the bischloroformate of hydroxy-terminated eugenol polydimethylsiloxane; and introducing phosgene and/or chain termination agent either continuously or in stages. A feature of the process is the presence of dihydroxyaromatic compound in only one charge, at the beginning. The products have excellent physical properties, including transparency.
摘要翻译： 通过在叔胺作为唯一的催化剂种存在下首先制备低聚芳族聚碳酸酯如低聚双酚A聚碳酸酯来制备共聚有机硅氧烷， 使低聚聚碳酸酯混合物与聚有机硅氧烷二（芳基）氯甲酸酯接触，例如羟基封端的丁子香酚聚二甲基硅氧烷的双氯甲酸酯; 并连续或分阶段引入光气和/或链终止剂。 该方法的特征是在开始时仅在一次充电中存在二羟基芳族化合物。 该产品具有优异的物理性能，包括透明度。
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公开(公告)号：US06723864B2
公开(公告)日：2004-04-20
申请号：US10223030
申请日：2002-08-16
IPC分类号： G07F718
摘要： Siloxane bischloroformates are prepared in a continuous process by phosgenating siloxane bisphenols in a flow reactor using a substantial excess of phosgene and sodium hydroxide. While very high levels (>95%) of conversion of the siloxane bisphenol to the corresponding siloxane bischloroformate are achieved using a flow reactor according to the method of the invention, only more modest conversion (˜90%) of the siloxane bisphenol to the corresponding siloxane bischloroformate is attained when analogous batch processes are employed. The process holds promise for use in the manufacture of silicone-containing copolycarbonates which requires high purity siloxane bischloroformate intermediates.
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6.发明授权公开(公告)号：US06392079B1
公开(公告)日：2002-05-21
申请号：US09281498
申请日：1999-03-30
IPC分类号： C07C6996
摘要： A continuous process for the preparation of monofunctional aromatic chloroformates (MAC) having the structure (I) wherein n is an integer from 1 to 5, and R1 represents hydrogen, a branched or unbranched alkyl group having from 1-15 carbon atoms, an aryl group which may be substituted or unsubstituted, a cycloaliphatic group which may be substituted or unsubstituted, or an arylalkyl group which may be substituted or unsubstituted, the method comprising the steps of a) introducing 1) an aqueous caustic solution; 2) a carbonyl chloride; 3) at least one monofunctional hydroxyaromatic compound; and 4) at least one inert organic solvent into a continuous reaction system; and b) effecting contact between 1), 2), 3) and 4) for a time and at conditions sufficient to produce a MAC of structure (I).
摘要翻译： 制备具有结构（I）的单官能芳族氯甲酸酯（MAC）的连续方法，其中n为1至5的整数，并且R 1表示氢，具有1-15个碳原子的支链或非支链烷基，芳基 可以被取代或未取代的基团，可被取代或未取代的脂环族基团或可被取代或未取代的芳基烷基，所述方法包括以下步骤：a）引入1）苛性碱水溶液; 2）碳酰氯; 3 ）至少一种单官能羟基芳族化合物; 和4）至少一种惰性有机溶剂进入连续反应体系; 和b）在足以产生结构（I）的MAC的条件下，在1），2），3）和4）之间进行接触。
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公开(公告)号：US06214235B1
公开(公告)日：2001-04-10
申请号：US09055461
申请日：1998-04-06
申请人： James Manio Silva
发明人： James Manio Silva
IPC分类号： B01D1500
CPC分类号： B01D15/00 , C01D3/16 , C07C209/86 , C07C211/63
摘要： The present invention relates to a process to remove quaternary ammonium salt (QS), from brine solution. The process uses an adsorbent selected from the group consisting of activated carbon and pyrolyzed sulfonated polystyrene divinylbenzene resin, or mixtures thereof which aids in removing the quaternary ammonium salt (QS). The process can be generally carried out at a temperature ranging from about −10° C. to about 90° C., at a pH ranging from about 1 to about 13.
摘要翻译： 本发明涉及从盐水溶液中除去季铵盐（QS）的方法。 该方法使用选自活性炭和热解磺化聚苯乙烯二乙烯基苯树脂的吸附剂，或其混合物，其有助于除去季铵盐（QS）。 该方法通常可以在约-10℃至约90℃，约1至约13的pH范围内进行。
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公开(公告)号：US6103092A
公开(公告)日：2000-08-15
申请号：US177588
申请日：1998-10-23
申请人： James Manio Silva
发明人： James Manio Silva
IPC分类号： B01D19/00 , C01D3/14 , C02F1/20 , C02F1/28 , C02F1/42 , C02F1/58 , C02F1/62 , C02F1/64 , C02F9/00 , C25B15/08 , C25B1/34
摘要： The method reduces the concentration of multivalent metal cations such as calcium, magnesium, iron, nickel, and chromium in brine solution containing a water-soluble metal chelating agent such as sodium gluconate. The method comprises subjecting the brine to primary brine treatment, and then readjusting the brine solution to a pH ranging from about 1.5 to about 5.5, and contacting the brine solution with at least one resin bed comprising a chelating ion exchange resin, typically at a temperature ranging from about 10.degree. C. to about 90.degree. C. and at a flow rate ranging from about 4 to about 32 resin bed volumes per hour; and recovering the brine solution.
摘要翻译： 该方法在含有水溶性金属螯合剂如葡萄糖酸钠的盐水溶液中降低多价金属阳离子如钙，镁，铁，镍和铬的浓度。 该方法包括对盐水进行一级盐水处理，然后将盐水溶液重新调节至约1.5至约5.5的pH，并将盐水溶液与至少一种包含螯合离子交换树脂的树脂床接触，通常在温度 范围为约10℃至约90℃，流速为约4至约32树脂床体积/小时; 并回收盐水溶液。
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公开(公告)号：US20120097614A1
公开(公告)日：2012-04-26
申请号：US13189864
申请日：2011-07-25
CPC分类号： C02F9/00 , B01J39/00 , B01J39/16 , B01J45/00 , B01J2220/56 , C02F1/048 , C02F1/42 , C02F1/66 , C02F1/683 , C02F1/74 , C02F2001/5218 , C02F2101/006 , C02F2101/203 , C02F2101/206 , G21F9/12
摘要： A method for treating low barium frac water includes contacting a frac water stream with a radium selective complexing resin to produce a low radium stream, passing the low radium stream through a thermal brine concentrator to produce a concentrated brine; and passing the concentrated brine through a thermal crystallizer to yield road salt.
摘要翻译： 用于处理低钡压裂水的方法包括使压裂水流与镭选择性络合树脂接触以产生低镭物流，使低镭物流通过热盐水浓缩器以产生浓缩的盐水; 并将浓缩的盐水通过热结晶器以产生路盐。
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公开(公告)号：US20110114567A1
公开(公告)日：2011-05-19
申请号：US13015466
申请日：2011-01-27
申请人： Zijun Xia , Rihua Xiong , Jiyang Xia , Chengqian Zhang , James Manio Silva , Weiming Zhang , Wei Cai
发明人： Zijun Xia , Rihua Xiong , Jiyang Xia , Chengqian Zhang , James Manio Silva , Weiming Zhang , Wei Cai
CPC分类号： C02F1/4604 , B01D21/0042 , B01D21/286 , C02F1/4691 , C02F1/4693 , C02F9/00 , C02F2001/5218 , C02F2103/08 , C02F2201/4613 , Y02A20/134
摘要： A precipitation device comprises a precipitation element disposed within a vessel and configured to define a precipitation zone and a solid-liquid separation zone between the precipitation element and the vessel, the precipitation zone configured to receive a first stream of saline liquid and to precipitate solids from the saline liquid, the solid-liquid separation zone configured to settle the solids by gravity, and an exit port located in an upper portion of the vessel and configured for exit of a second stream of liquid of lower salinity than the first stream, wherein a ratio of a diameter of the vessel to a diameter of the precipitation element ranges from about 1.5 to about 2.8. Associated system and method are also provided.
摘要翻译： 沉淀装置包括设置在容器内并用于限定沉淀区和沉淀元件与容器之间的固液分离区的沉淀元件，沉淀区构造成容纳第一流的盐水液体并将固体从 所述盐水液体，所述固液分离区被配置为通过重力沉积所述固体;以及出口，其位于所述容器的上部，并被配置为用于排出比所述第一流低的盐度的第二液体流，其中， 容器的直径与沉淀元素的直径的比率在约1.5至约2.8之间。 还提供了相关系统和方法。
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