APPARATUS AND METHODS FOR THE PREPARATION OF REACTION VESSELS
    1.
    发明申请
    APPARATUS AND METHODS FOR THE PREPARATION OF REACTION VESSELS 有权
    制备反应容器的装置和方法

    公开(公告)号:US20150010461A1

    公开(公告)日:2015-01-08

    申请号:US14379105

    申请日:2013-02-18

    发明人: Leroy Cronin

    摘要: Provided are methods for preparing and using reaction vessels obtained or obtainable by 3D-printin methods, including a method for preparing a product compound, the method comprising the steps of: (i) providing a reaction vessel that is obtained by a 3-D printing method, wherein the reaction vessel has a reaction space; (ii) providing one or more reagents, optionally together with a catalyst or a solvent, for use in the synthesis of the product compound; and (iii) permitting the one or more reagents to react in the reaction space, optionally in the presence of the catalyst and the solvent, in the reaction vessel, thereby to form the product compound.

    摘要翻译: 本发明提供了制备和使用通过3D-printin方法获得或可获得的反应容器的方法,包括制备产物化合物的方法,所述方法包括以下步骤:(i)提供通过3-D印刷获得的反应容器 方法,其中反应容器具有反应空间; (ii)提供一种或多种试剂,任选地与催化剂或溶剂一起用于产物化合物的合成; 和(iii)允许一种或多种试剂在反应容器中任选在催化剂和溶剂的存在下在反应空间中反应,从而形成产物化合物。

    APPARATUS AND METHODS FOR THE ELECTROCHEMICAL GENERATION OF OXYGEN AND/OR HYDROGEN
    2.
    发明申请
    APPARATUS AND METHODS FOR THE ELECTROCHEMICAL GENERATION OF OXYGEN AND/OR HYDROGEN 审中-公开
    氧化物和/或氢的电化学生成装置及方法

    公开(公告)号:US20140318979A1

    公开(公告)日:2014-10-30

    申请号:US14357066

    申请日:2012-11-08

    IPC分类号: C25B1/10

    摘要: The invention provides methods for producing hydrogen and oxygen, comprising the steps of: (i) oxidising a mediator at a working electrode to yield an oxidised mediator, and reducing protons at a counter electrode to yield hydrogen; and (ii) reducing an oxidised mediator at a working electrode to yield a mediator, and oxidising water at a counter electrode to yield oxygen. wherein the oxygen generation step is performed non-simultaneously to the hydrogen generation step, and the oxidised mediator of step (i) is used as the oxidised mediator of step (ii), or the mediator of step (ii) is used as the mediator of step (i), and the mediator has a reversible redox wave lying between the onset of the oxygen evolution reaction (OER) and the hydrogen evolution reaction (HER).

    摘要翻译: 本发明提供了产生氢和氧的方法,包括以下步骤:(i)在工作电极处氧化介体以产生氧化的介体,并在对电极上还原质子以产生氢; 和(ii)在工作电极处还原氧化的介质以产生介体,并且在对电极处氧化水以产生氧。 其中氧生成步骤与氢生成步骤非同时进行,步骤(i)的氧化介体用作步骤(ii)的氧化介体,或者使用步骤(ii)的介体作为介体 的步骤(i),并且介体具有位于析氧反应(OER)开始与析氢反应(HER)之间的可逆氧化还原波。

    Networked Reaction Systems
    6.
    发明申请

    公开(公告)号:US20210031162A1

    公开(公告)日:2021-02-04

    申请号:US16978591

    申请日:2019-03-06

    发明人: Leroy Cronin

    IPC分类号: B01J19/00 G06Q50/00

    摘要: The present invention provides a system for performing reactions, where the system comprises a plurality of synthesisers that are in communication via a communal reporting platform. A synthesiser is programmed for the automated synthesis of one or more chemical or biological reactions, and the synthesiser comprises a reaction vessel which is supplied by a reagent delivery system, an analytical system for analysing a reaction, and a controller for managing the reagent delivery system and the analytical system, and for communication with the reporting platform. Also provided are methods for performing a plurality or reactions using the system.

    METHODS OF EVOLUTIONARY SYNTHESIS INCLUDING EMBODIED CHEMICAL SYNTHESES
    7.
    发明申请
    METHODS OF EVOLUTIONARY SYNTHESIS INCLUDING EMBODIED CHEMICAL SYNTHESES 有权
    包括化学合成的演化合成方法

    公开(公告)号:US20150133306A1

    公开(公告)日:2015-05-14

    申请号:US14402943

    申请日:2013-05-24

    发明人: Leroy Cronin

    IPC分类号: B01J19/00

    摘要: The invention provides a method for preparing a compound or a product having one or more characteristics that meet or exceed a user specification, the process comprising the step of selecting a first combination of chemical inputs, optionally together with physical inputs, and supplying those inputs to a reaction space, thereby to generate a first product; analysing one or more characteristics of the product generated; comparing the one or more characteristics against a user specification; using a genetic algorithm selecting a second combination of chemical inputs, optionally together with physical inputs, wherein the second combination differs from the first combination, and supplying those inputs to the reaction space, thereby to generate a second product; analysing one or more characteristics of the second product generated; comparing the one or more characteristics generated against the user specification; repeating the selecting and analysing steps for further individual combinations of chemical and/or physical inputs, to provide an array of products wherein the flow chemistry system operates continuously to provide the first, second and further products, thereby to identify one or more products meeting or exceeding the user specification.

    摘要翻译: 本发明提供了一种制备具有满足或超过用户规格的一种或多种特性的化合物或产品的方法,该方法包括选择化学输入的第一组合,可选地与物理输入一起并将这些输入提供给 反应空间,从而产生第一产物; 分析产生的产品的一个或多个特征; 将一个或多个特征与用户规范进行比较; 使用选择化学输入的第二组合的可选的物理输入的遗传算法,其中所述第二组合与所述第一组合不同,并且将所述输入提供给所述反应空间,从而产生第二乘积; 分析产生的第二产品的一个或多个特性; 比较生成的一个或多个特征与用户规范; 重复选择和分析步骤以用于进一步的化学和/或物理输入的单独组合,以提供产品阵列,其中流化学系统连续操作以提供第一,第二和其他产品,由此识别一个或多个产品会议或 超过用户规格。

    Use of Polyoxometalate Mediators
    8.
    发明公开

    公开(公告)号:US20230183868A1

    公开(公告)日:2023-06-15

    申请号:US18086364

    申请日:2022-12-21

    IPC分类号: C25B1/04 H01M8/18

    CPC分类号: C25B1/04 H01M8/188

    摘要: A method is disclosed of manufacturing a semiconductor structure comprising an (001) oriented zincblende structure group III-nitride layer, such as GaN. The layer is formed on a 3C-SiC layer on a silicon substrate. A nucleation layer is formed, recrystallized and then the zincblende structure group III-nitride layer is formed by MOVPE at temperature T3 in the range 750-1000° C., to a thickness of at least 0.5μ. There is also disclosed a corresponding semiconductor structure comprising a zincblende structure group III-nitride layer which, when characterized by XRD, shows that the substantial majority, or all, of the layer is formed of zincblende structure group III-nitride in preference to wurtzite structure group III-nitride.
    The present invention provides methods for producing hydrogen using a mediator that is capable of reversibly donating and accepting four or more electrons. A method of the invention comprises the steps of reducing a mediator by four or more electrons to yield a reduced mediator, and oxidising a reduced mediator to yield a mediator, and reducing protons to yield hydrogen.

    Method for Estimating Molecular Complexity

    公开(公告)号:US20230129380A1

    公开(公告)日:2023-04-27

    申请号:US17912382

    申请日:2021-03-19

    发明人: Leroy Cronin

    IPC分类号: G01N30/86 G01N30/72 G01N24/08

    摘要: The present invention provides a method for estimating the molecular complexity of a sample, for example to determine whether biotic or synthetic components are present in the sample. The method comprises the steps of (a) performing one of MS/MS, NMR or IR on a sample; (b) determining the unique peaks in the resulting spectrum; and (c) calculating the molecular assembly index of the sample based on the number of unique peaks in the spectrum.