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    NMR method of determining and regulating the composition of polymer mixtures in polymerization
    3.
    发明授权
    NMR method of determining and regulating the composition of polymer mixtures in polymerization 有权
    确定和调节聚合物中聚合物混合物组成的NMR方法

    公开(公告)号：US07737230B2

    公开(公告)日：2010-06-15

    申请号：US11629542

    申请日：2005-06-09

    Applicant: Shahram Mihan ,  Dieter Lilge ,  Wolfgang Rohde

    Inventor： Shahram Mihan ,  Dieter Lilge ,  Wolfgang Rohde

    IPC: C08F2/00 ,  C08F210/00

    CPC classification number: G01N24/08 ,  C08F10/02 ,  C08F110/02 ,  C08F210/16 ,  C08F2400/02 ,  G01N24/085 ,  G01R33/44 ,  Y02P20/125 ,  C08F2/00

    Abstract: Method of determining the composition of polymer mixtures comprising defined polymer components of differing mean molar masses Mn, which comprises the steps (a) recording of at least one 1H-NMR relaxation curve of the polymer mixture and (b) calculating the proportions of the polymer components by matching the measured relaxation curve with the relaxation curves of the individual polymer components. In this way, the composition of polymer mixtures can be determined quickly and simply. Furthermore, process integration for regulating the polymerization is possible.

    Abstract translation: 确定包含不同平均摩尔质量Mn的限定的聚合物组分的聚合物混合物的组成的方法，其包括步骤（a）记录聚合物混合物的至少一个1H-NMR松弛曲线，和（b）计算聚合物的比例 通过将测量的松弛曲线与各个聚合物组分的松弛曲线相匹配来获得组分。 以这种方式，可以快速且简单地确定聚合物混合物的组成。 此外，用于调节聚合的方法集成是可能的。

    Method and Roll Stand for Multiply Influencing Profiles
    5.
    发明申请
    Method and Roll Stand for Multiply Influencing Profiles 有权
    多重影响型材的方法和轧辊架

    公开(公告)号：US20070240475A1

    公开(公告)日：2007-10-18

    申请号：US10584173

    申请日：2004-11-22

    Applicant: Günter Kneppe ,  Wolfgang Rohde ,  Sabine Rohde

    Inventor： Günter Kneppe ,  Wolfgang Rohde ,  Sabine Rohde

    IPC: B21B41/04

    CPC classification number: B21B13/142 ,  B21B13/147 ,  B21B27/021 ,  B21B37/40 ,  B21B2013/025 ,  B21B2013/028

    Abstract: When rolling sheets or strips in roll stands using working rolls, which are supported on back-up rolls or on intermediate rolls having back-up rolls, whereby the setting of the roll gap is effected by axially displacing roll pairs provided with curved contours, differences from the required profile occur in the instance of larger widths of a product range due to excessive extensions in the edge areas or in the quarter areas that are manifested in the form of so-called quarter waves in the flatness of the product. In order to rectify this problem by using a simple mechanism and to improve the setting mechanism and the strategy for creating absolutely planar strips with a predetermined thickness profile over the entire width of the rolling stock, the invention provides that for forming the roll gap set profiles (10, 11) for two selected displacing positions, the contours of the rolls of one roll pair are shaped in such a manner that they produce, in the roll gap, a profile (20, 21), which is symmetric with regard to the center of the roll and which has a profile maximum in the center of the roll that can be altered by displacing the rolls, whereas the contours of the rolls of at least one second roll pair produce, in the roll gap, a profile (22, 23), which is symmetric with regard to the center of the roll and which has two identical maxima outside of the center of the roll that can be altered by displacing the rolls.

    Abstract translation: 当在辊架上轧制板材或条带时，其使用工作辊，其被支撑在备用辊上或具有支撑辊的中间辊上，由此辊间隙的设定通过轴向移位设置有弯曲轮廓的辊对来实现，差异 在产品范围较宽的情况下，由于在产品平面度上以所谓的四分之一波浪的形式表现的边缘区域或四分之一区域中的过度扩展，所以要求的分布发生。 为了通过使用简单的机构来解决这个问题，并且改进了在机车车辆的整个宽度上制造具有预定厚度轮廓的绝对平面条带的设定机构和策略，本发明提供了用于形成辊隙组合轮廓 （10,11），对于两个选定的位移位置，一个辊对的辊的轮廓成形为使得它们在辊隙中产生轮廓（20,21），轮廓（20,21）关于 辊的中心具有在辊的中心最大的轮廓，该轮廓可以通过移动辊而改变，而至少一个第二辊对的辊的轮廓在辊间隙中产生轮廓（22， 23），其对于辊的中心是对称的，并且在辊的中心之外具有两个相同的最大值，该最大值可以通过移动辊而改变。

    Method of operating a rolling mill for hot-rolling and cold-rolling of flat products
    9.
    发明授权
    Method of operating a rolling mill for hot-rolling and cold-rolling of flat products 有权
    操作平板产品的热轧和冷轧轧机的方法

    公开(公告)号：US06142000A

    公开(公告)日：2000-11-07

    申请号：US281485

    申请日：1999-03-30

    Applicant: Wolfgang Rohde

    Inventor： Wolfgang Rohde

    IPC: B21B31/16 ,  B21B37/00 ,  B21B37/28 ,  B21B37/38 ,  B21B37/42 ,  B21B37/58 ,  B21B38/10

    CPC classification number: B21B37/28 ,  B21B37/42 ,  B21B37/58 ,  B21B2038/002 ,  B21B38/105

    Abstract: A method of operating a rolling mill for hot-rolling and cold-rolling of flat products in one or more roll stands each having two or more rolls, wherein the roll gaps are regulated so as to correct the differential force between the drive side and the operator side of the roll stands, while compensating the adjustment value-controlled regulation of the roll gaps which corrects the bending and balancing forces. Prior to further processing of the flat products, the regulation is supplied with an additional correction adjustment value formed from the horizontal forces measured in all individual rolls.

    Abstract translation: 一种用于在具有两个或更多个辊的一个或多个轧辊机架中对平板产品进行热轧和冷轧的轧机的方法，其中辊间隙被调节以校正驱动侧和 同时补偿校正弯曲和平衡力的辊间隙的调整值控制调节。 在进一步处理扁平产品之前，向所述调节装置提供由在所有单个辊中测量的水平力形成的附加校正调整值。

    Amidinato catalyst systems for the polymerization of olefins
    10.
    发明授权
    Amidinato catalyst systems for the polymerization of olefins 失效
    用于烯烃聚合的胺基催化剂体系

    公开(公告)号：US5707913A

    公开(公告)日：1998-01-13

    申请号：US469356

    申请日：1995-06-06

    Applicant: Ruger Schlund ,  Martin Lux ,  Frank Edelmann ,  Ulrike Reissmann ,  Wolfgang Rohde

    Inventor： Ruger Schlund ,  Martin Lux ,  Frank Edelmann ,  Ulrike Reissmann ,  Wolfgang Rohde

    IPC: C08F4/60 ,  C08F4/622 ,  C08F4/623 ,  C08F4/64 ,  C08F10/00 ,  C08F110/02 ,  B01J31/00 ,  B01J37/00 ,  C08G4/02

    CPC classification number: C08F10/00 ,  C08F110/02 ,  C08F4/65912

    Abstract: Catalyst systems which are suitable for the polymerization of olefinically unsaturated hydrocarbons contain, as active components, A) an amidinato metal complex of the formula A ##STR1## where M is a metal from group IIIb, IVb, Vb or VIb of the Periodic Table of Elements or a metal from the lanthanide group, X is a negative leaving atom or a negative leaving group, and the radicals X may be identical or different if (n-m)>1, R.sup.1, R.sup.2 and R.sup.3 are each a C-organic or Si-organic radical, n is the valency of M in the metal complex A and m is from 1 to 5, with the proviso that n-m.gtoreq.0, and, B) an activator in a molar ratio of activator B to metal complex A of from 0.5:1 to 10,000:1.

    Abstract translation: 适用于烯属不饱和烃的聚合的催化剂体系含有作为活性组分的A）A A的脒基金属络合物，其中M是元素周期表IIIb，IVb，Vb或VIb族的金属 的元素或来自镧系元素的金属，X是负离子原子或负离去基团，并且如果（nm）> 1，R 1，R 2和R 3各自为C-有机基团，则基团X可以相同或不同， Si-有机基团，n是M在金属络合物A中的化合价，m为1至5，条件是nm≥0，B）活化剂B与金属络合物的摩尔比的活化剂 A为0.5：1至10,000：1。

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