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    Process for preparing glass constructions
    3.
    发明授权
    Process for preparing glass constructions 失效
    制备玻璃结构的方法

    公开(公告)号：US4433010A

    公开(公告)日：1984-02-21

    申请号：US454520

    申请日：1982-12-30

    申请人： Josef Pedain ,  Wolfgang Wellner ,  Klaus Konig ,  Hermann Gruber

    发明人： Josef Pedain ,  Wolfgang Wellner ,  Klaus Konig ,  Hermann Gruber

    IPC分类号： C03C27/10 ,  C08G18/00 ,  C08G18/08 ,  C08G18/10 ,  C08G18/42 ,  C08G18/44 ,  C08G18/78 ,  C09K3/10 ,  E06B3/663 ,  C03C17/32

    CPC分类号： C08G18/088 ,  C08G18/10 ,  C08G18/44 ,  C08G18/7831 ,  C09K3/1021 ,  E06B3/66342 ,  C08G2190/00 ,  C09K2200/0652

    摘要： The instant invention is directed to a process for the preparation of glass constructions comprising applying to glass, compositions comprising(a) a polyisocyanate component and(b) a polyol component comprising at least one dihydroxy polyester carbonate with a molecular weight of from 800 to 3000 which is a reaction product of hexanediol-(1,6) with .epsilon.-caprolactone and/or .epsilon.-hydroxycaproic acid, in a molar ratio of hexanediol-(1,6) to .epsilon.-caprolactone and/or .epsilon.-hydroxycaproic acid of from 4:1 to 1:3, and diaryl carbonates, which reaction product is optionally present as a mixture with up to 40% by weight, based on the total quantity of said polyol component, of other polyols with molecular weights of from 62 to 4000, optionally containing ester groups,the quantities of the said components corresponding to an isocyanate index of from 80 to 130, or compositions comprising(c) an isocyanate prepolymer based on said polyols, optionally present in admixture with other polyisocyanates, and optionally(d) free- or blocked-diamine chain-lengthening agents.

    摘要翻译： 本发明涉及一种制备玻璃结构的方法，包括向玻璃施加包含（a）多异氰酸酯组分的组合物和（b）包含至少一种分子量为800至3000的二羟基聚酯碳酸酯的多元醇组分 其是己二醇 - （1,6）与ε-己内酯和/或ε-羟基己酸的反应产物，其己二醇 - （1,6）与ε-己内酯和/或ε-己酸的ε-羟基己酸的摩尔比为 4:1至1:3，和碳酸二芳基酯，该反应产物任选地以基于所述多元醇组分的总量至多40重量％的混合物存在分子量为62至4000的其它多元醇 ，任选地含有酯基，所述组分的量相当于异氰酸酯指数为80-130，或组合物包含（c）基于所述多元醇的异氰酸酯预聚物，任选以与第 多异氰酸酯和任选的（d）游离或封闭的二胺链延长剂。

    Hydrocurable oxazolidine isocyanate prepolymer compositions
    5.
    发明授权
    Hydrocurable oxazolidine isocyanate prepolymer compositions 失效
    可氢化恶唑烷异氰酸酯预聚物组合物

    公开(公告)号：US4118376A

    公开(公告)日：1978-10-03

    申请号：US817083

    申请日：1977-07-18

    申请人： Josef Pedain ,  Wolfgang Wellner ,  Hermann Gruber ,  Manfred Dietrich

    发明人： Josef Pedain ,  Wolfgang Wellner ,  Hermann Gruber ,  Manfred Dietrich

    IPC分类号： C09K17/00 ,  B60T17/08 ,  C08G18/00 ,  C08G18/10 ,  C08L51/00 ,  C08L51/02 ,  C08L75/00 ,  C08L75/04 ,  C08L77/00 ,  C09D175/00 ,  C09K17/30 ,  C09K103/00

    CPC分类号： C08G18/10 ,  C08L75/04

    摘要： The present invention is concerned with a hydrocurable composition suitable for use as coatings, adhesives or grouts. The composition contains oxazolidine compounds and free isocyanate group containing prepolymers. The prepolymers are obtained by the reaction of polyisocyanates with special types of dispersions wherein the dispersed phase is synthesized in situ in a dispersing media of polyhydroxyl compounds. The dispersed phase may be a free radical addition polymer, an aminoplast polycondensate or a polyisocyanate addition product. In the last case, the non-isocyanate reactants used to form the dispersed phase are substantially more reactive with isocyanates than the dispersing media. An especially preferred composition is based on urethane oxazolidines and prepolymers of aliphatic or cycloaliphatic isocyanates with dispersions of isocyanate hydrazine or hydrazine hydrate condensates in polyhydroxy-polyethers having molecular weights of 200 to 16,000.

    摘要翻译： 本发明涉及适合用作涂料，粘合剂或浆料的可氢化组合物。 该组合物含有恶唑烷化合物和含游离异氰酸酯基团的预聚物。 预聚物通过多异氰酸酯与特殊类型的分散体的反应获得，其中分散相在多羟基化合物的分散介质中原位合成。 分散相可以是自由基加成聚合物，氨基塑料缩聚物或多异氰酸酯加成产物。 在最后一种情况下，用于形成分散相的非异氰酸酯反应物与分散介质基本上比异氰酸酯更具反应性。 特别优选的组合物是基于聚氨酯恶唑烷和具有异氰酸酯肼或水合肼缩合物在分子量为200至16,000的多羟基聚醚中的分散体的脂肪族或脂环族异氰酸酯的预聚物。

    Process for the preparation of polyisocyanates containing urethane groups and the products obtained
    6.
    发明授权
    Process for the preparation of polyisocyanates containing urethane groups and the products obtained 失效
    制备含有氨基甲酸酯基团的多异氰酸酯的方法和所得产品

    公开(公告)号：US4910332A

    公开(公告)日：1990-03-20

    申请号：US269230

    申请日：1988-11-09

    申请人： Lothar Kahl ,  Josef Pedain ,  Wolfgang Wellner

    发明人： Lothar Kahl ,  Josef Pedain ,  Wolfgang Wellner

    IPC分类号： C08G18/10 ,  C07C271/28 ,  C08G18/72 ,  C08G18/79 ,  C08G18/80 ,  C08G18/82

    CPC分类号： C08G18/721 ,  C07C271/28 ,  C08G18/792 ,  C08G18/8009 ,  C08G18/8064

    摘要： The present invention is directed to a process for the preparation of polyisocyanates containing urethane groups in which the content in monomeric starting diisocyanate is at most 0.4% by weight by reacting in a urethane-forming reaction(a) an excess quantity, based on component (b), of a diisocyanate component containing at least one aromatic diisocyanate which is free from urethane groups with(b) a polyol component containing at least one polyhydric alcohol in the molecular weight range of 62 to about 250followed by distillative removal of the unreacted excess starting diisocyanate (a), characterized in that before the distillative removal of the excess starting diisocyanate (a) is carried out,(c) an aliphatic polyisocyanate containing isocyanurate groups is incorporated in the urethane-containing reaction product of components (a) and (b) in a quantity of about 0.3 to 10% by weight, based on the undistilled reaction product of components (a) and (b), and the distillation residue is then optionally dissolved in an inert solvent and up to about 0.5 equivalents of an alcohol, per kg of solvent-free distillation residue on a solvent free basis is added to the resulting solution so that the amount of free starting diisocyanate (a) is further reduced and urethane groups are formed.The present invention is also directed to the polyisocyanates containing urethane groups obtained by this process.

    摘要翻译： 本发明涉及一种制备含有氨基甲酸酯基团的多异氰酸酯的方法，其中单体起始二异氰酸酯的含量至多为0.4重量％，其中在氨基甲酸酯形成反应（a）过量时，基于组分（ b），含有至少一种不含氨基甲酸酯基团的芳族二异氰酸酯的二异氰酸酯组分，（b）含有至少一种分子量范围为62至约250的多元醇的多元醇组分，然后蒸馏除去未反应的过量 起始二异氰酸酯（a），其特征在于，在蒸馏除去过量的起始二异氰酸酯（a）之前，（c）将含有异氰脲酸酯基团的脂族多异氰酸酯引入组分（a）和（ b）基于组分（a）和（b）的未蒸馏反应产物，其量为约0.3至10重量％，蒸馏残余物 然后任选地溶解在惰性溶剂中，并且在无溶剂基础上将每kg无溶剂蒸馏残余物最多至多约0.5当量的醇加入到所得溶液中，使得游离起始二异氰酸酯（a）的量进一步 还原和氨基甲酸酯基团形成。 本发明还涉及通过该方法获得的含有氨基甲酸酯基团的多异氰酸酯。

    Dispersion of post-curable coating compounds
    8.
    发明授权
    Dispersion of post-curable coating compounds 失效
    后固化涂料化合物的分散

    公开(公告)号：US5738912A

    公开(公告)日：1998-04-14

    申请号：US760093

    申请日：1996-12-11

    申请人： Eberhard Konig ,  Detlef-Ingo Schutze ,  Josef Pedain

    发明人： Eberhard Konig ,  Detlef-Ingo Schutze ,  Josef Pedain

    IPC分类号： C08G18/08 ,  C08G18/12 ,  C08G18/28 ,  C08G18/44 ,  C14C11/00 ,  D06N3/14 ,  B05D7/12

    CPC分类号： D06N3/14 ,  C08G18/0804 ,  C08G18/12 ,  C08G18/283 ,  C08G18/44 ,  C14C11/006

    摘要： The invention relates to a method for coating textiles and/or leather with an aqueous dispersion comprising (A) a mixture of (i) a urethane-containing blocked NCO prepolymer having a number average molecular weight of 2000 to 10,000, a content of blocked isocyanate groups (calculated as NCO) of 0.5 to 5 wt. %, an ethoxy group content of 2 to 50 wt. %, an ionic group content of 5 to 30 meq per 100 g of the prepolymer, and (ii) a polyamine having (cyclo)aliphatically bonded primary and/or secondary amino groups, wherein the equivalent ratio of blocked NCO groups of component (i) to amino groups of component (ii) is 1:0.9 to 1:1.2, and (B) an aqueous phase.

    摘要翻译： 本发明涉及一种用水分散体涂布纺织品和/或皮革的方法，其包含（A）（i）数均分子量为2000至10,000的含氨基甲酸酯的封闭NCO预聚物，封端异氰酸酯的含量 基团（以NCO计算）为0.5〜5wt。 ％，乙氧基含量为2〜50wt。 ％，每100g预聚物的离子基团含量为5至30meq，和（ii）具有（环）脂族键合的伯和/或仲氨基的多胺，其中组分（i）的封闭NCO基团的当量比 ）至组分（ⅱ）的氨基为1：0.9至1：1.2，和（B）水相。

    Polyisocyanates containing allophanate groups
    9.
    发明授权
    Polyisocyanates containing allophanate groups 失效
    含有脲基甲酸酯基的多异氰酸酯

    公开(公告)号：US5672736A

    公开(公告)日：1997-09-30

    申请号：US555200

    申请日：1995-11-08

    申请人： Martin Brahm ,  Lutz Schmalstieg ,  Josef Pedain

    发明人： Martin Brahm ,  Lutz Schmalstieg ,  Josef Pedain

    IPC分类号： C07C273/18 ,  C07C275/60 ,  C08G18/78 ,  C09D175/00 ,  C07C263/00

    CPC分类号： C08G18/7837 ,  C07C275/60

    摘要： The present invention relates to a process for preparing polyisocyanates containing allophanate groups by reacting compounds a), which i) contain urethane groups, but which are substantially free of hydroxyl groups and isocyanate groups, ii) have an average of at least two urethane groups per molecule, iii) are prepared by reacting organic isocyanates a1) with organic hydroxyl compounds a2) and iv) have an average molecular weight of at most 2,500, with excess quantities, based on the urethane groups, of distillable organic polyisocyanates b) to form polyisocyanates containing allophanate groups and subsequently removing by distillation the unreacted excess of component b) to a residual content of less than 0.5 wt. %, provided that polyisocyanates a1) and polyisocyanates b) are different. The present invention also relates to the products obtained from this process and to their use as binders or binder components in coating compositions.

    摘要翻译： 本发明涉及通过使具有氨基甲酸酯基但不含羟基和异氰酸酯基的化合物a）反应制备含有脲基甲酸酯基团的多异氰酸酯的方法，ii）基本上不含羟基和异氰酸酯基团，ii）平均具有至少两个氨基甲酸酯基团 分子，iii）通过使有机异氰酸酯a1）与有机羟基化合物a2）和iv）具有至多2500的平均分子量，基于氨基甲酸酯基团的过量的可蒸馏有机多异氰酸酯b）来制备，以形成多异氰酸酯 含有脲基甲酸酯基团，随后通过蒸馏将未反应的组分b）过量除去至少于0.5wt。 ％，条件是多异氰酸酯a1）和多异氰酸酯b）不同。 本发明还涉及从该方法获得的产品及其作为涂料组合物中的粘合剂或粘合剂组分的用途。