摘要:
This disclosure relates to a process for producing titanium dioxide, comprising: a) reacting a alloy comprising silicon and aluminum having a melting point of about 482° C. to about 660° C., with chlorine gas at temperatures above 190° C. to form chlorides of silicon and aluminum; b) adding titanium tetrachloride to the chlorides of silicon and aluminum of step (a); c) oxidizing the chlorides of silicon and aluminum and titanium tetrachloride of step (b); and d) forming titanium dioxide.
摘要:
Methods are described that have the capability of producing submicron/nanoscale particles, in some embodiments dispersible, at high production rates. In some embodiments, the methods result in the production of particles with an average diameter less than about 75 nanometers that are produced at a rate of at least about 35 grams per hour. In other embodiments, the particles are highly uniform. These methods can be used to form particle collections and/or powder coatings. Powder coatings and corresponding methods are described based on the deposition of highly uniform submicron/nanoscale particles.
摘要:
Methods are described that have the capability of producing submicron/nanoscale particles, in some embodiments dispersible, at high production rates. In some embodiments, the methods result in the production of particles with an average diameter less than about 75 nanometers that are produced at a rate of at least about 35 grams per hour. In other embodiments, the particles are highly uniform. These methods can be used to form particle collections and/or powder coatings. Powder coatings and corresponding methods are described based on the deposition of highly uniform submicron/nanoscale particles.
摘要:
Provided is a method for manufacturing a metal oxide hollow nanoparticles with excellent properties more easily and simply by a chemical vapor condensation employing metal β-diketonates as precursors, and a metal oxide hollow nanoparticles manufactured by the method. The method includes: preparing metal β-diketonate as a precursor; evaporating the metal β-diketonate at a predetermined temperature higher than a melting point of the metal β-diketonate; transferring the evaporated metal β-diketonate into a reaction region; thermally decomposing the transferred gaseous metal β-diketonate and simultaneously inducing a reaction of the transferred gaseous metal β-diketonate with oxygen to synthesize the metal oxide hollow nanoparticle; and condensing and collecting the synthesized metal oxide hollow nanoparticles.
摘要:
Provided is a method for manufacturing a metal oxide hollow nanoparticles with excellent properties more easily and simply by a chemical vapor condensation employing metal β-diketonates as precursors, and a metal oxide hollow nanoparticles manufactured by the method. The method includes: preparing metal β-diketonate as a precursor; evaporating the metal β-diketonate at a predetermined temperature higher than a melting point of the metal β-diketonate; transferring the evaporated metal β-diketonate into a reaction region; thermally decomposing the transferred gaseous metal β-diketonate and simultaneously inducing a reaction of the transferred gaseous metal β-diketonate with oxygen to synthesize the metal oxide hollow nanoparticle; and condensing and collecting the synthesized metal oxide hollow nanoparticles.
摘要:
Pyrogenically produced aluminum oxide, in which the BET specific surface area is greater than 115 m2/g and the Sears index is over 8 ml/2 g and the dibutyl phthalate absorption as a powder measured with a 16 g weighed portion is not measurable, is produced by means of flame oxidation or preferably flame hydrolysis, whereby a vaporizable aluminum compound is used as starting material. The aluminum oxide can be used as an ink-absorbing substance in inkjet media and also as a filler, as a substrate, as a catalytically active substance, as a starting material for the production of dispersions, as a polishing material (CMP applications), as a ceramic raw material, in the electronics industry, in the cosmetics industry, as an additive in the silicone and rubber industry, to adjust the rheology of liquid systems, as a heat stabilizer, in the paint industry.
摘要:
A process for producing an ultrafine mixed-crystal oxide characterized by producing an ultrafine mixed crystal oxide comprising primary particles in a mixed crystal state with a BET specific surface area of 10 to 200 m2/g, comprising the step of subjecting a halogenated metal to high temperature oxidation with an oxidizing gas to produce a metal oxide by a vapor phase production method, wherein said halogenated metal is in the form of a mixed gas (a mixed halogenated metal gas) comprising at least two compounds having a different metal elements selected from the group consisting of chlorides, bromides, and iodides of titanium, silicon, and aluminum, and said mixed halogenated metal gas and said oxidizing gas are independently preheated to 500null C. or more prior to a reaction, a ultrafine mixed crystal oxide obtained by the process, and use of the oxide.
摘要:
A silicon-aluminum mixed oxide produced by flame hydrolysis and having a composition of from 1 to 99.999 wt. % Al2O3, the remainder being SiO2, which mixed oxide exhibits an amorphous structure in the X-ray diffraction pattern and consists of intergrown primary particles, and in these primary particles crystallites are present. These crystallites having sizes of between one and 200 namometers and the specific surface of the powder being between 5 and 300 m2/g. These products are produced by a process wherein silicon halide and aluminum halide are vaporized in a particular ratio to one another and are homogeneously mixed with air, oxygen and hydrogen in a mixing unit by means of any carrier gas, this mixture undergoes combustion in a burner of known construction and, after the separation of the solids from the vapour phase, any traces of halide possibly adhering to the product are separated off in a further processing step by means of moist air at elevated temperature. The silicon-aluminum mixed oxide produced by flame hydrolysis are used in the form of dispersions for polishing, in particular in the electronics industry (CMP).
摘要翻译:通过火焰水解制备的硅铝混合氧化物,其组成为1至99.999wt。 %Al 2 O 3,其余为SiO 2,该混合氧化物在X射线衍射图中呈现无定形结构并且由共生的一次粒子组成,并且在这些一次粒子中存在微晶。 这些微晶的尺寸为1至200纳米,粉末的比表面积为5至300平方米/克。 这些产品通过一种方法生产,其中卤化硅和卤化铝以特定比例彼此蒸发,并通过任何载气在混合单元中与空气,氧气和氢气均匀混合,该混合物在燃烧器中燃烧 已知的结构,并且在从气相中分离出固体之后,任何痕量的可能附着在产品上的卤化物在另外的加工步骤中通过在高温下的潮湿空气分离出来。 通过火焰水解生产的硅铝混合氧化物以抛光用分散体的形式使用,特别是在电子工业(CMP)中。
摘要:
The invention relates to fine-particle oxide ceramic powders of the metal oxides MeO, whereMe=Al, Si, Zr, Hf, Ta, Nb, Mo, W, V, La and/or Y,Al.sub.2 O.sub.3 being present in the .alpha.-phase and SiO.sub.2 being present in crystalline form.
摘要翻译:本发明涉及金属氧化物MeO的细颗粒氧化物陶瓷粉末,其中Me = Al,Si,Zr,Hf,Ta,Nb,Mo,W,V,La和/或Y,Al 2 O 3存在于α- 相和SiO 2以结晶形式存在。