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    ION CHROMATOGRAPH
    3.
    发明申请
    ION CHROMATOGRAPH 有权
    离子色谱

    公开(公告)号：US20140320146A1

    公开(公告)日：2014-10-30

    申请号：US14363027

    申请日：2012-10-15

    申请人： SHIMADZU CORPORATION

    发明人： Katsumasa Sakamoto ,  Yukio Oikawa ,  Shigeyoshi Horiike

    IPC分类号： G01N27/62

    CPC分类号： G01N27/62 ,  G01N30/96 ,  G01N2030/3038 ,  G01N2030/645 ,  G01N2030/965

    摘要： A suppressor is structured by an ion exchange section being structured by an eluate path forming member forming an eluate path and a regenerant path forming member forming a regenerant path being stacked across an ion exchange film, and a heat-conductive heat block covering the outside of the ion exchange section. A separation column, the suppressor, and an electrical conductivity meter are accommodated in a common constant temperature bath. The inside of the constant temperature bath is feedback-controlled by a temperature control section so as to be maintained at constant temperature.

    摘要翻译： 抑制器由通过形成洗脱路径的洗脱路径形成构件和形成层叠在离子交换膜上的再生路径的再生路径形成构件构成的离子交换区构成，并且覆盖外部的导热性热块 离子交换部。 分离柱，抑制器和电导率计容纳在公共恒温槽中。 恒温槽的内部由温度控制部进行反馈控制，保持恒温。

    Mobile phase treatment for chromatography
    6.
    发明申请
    Mobile phase treatment for chromatography 审中-公开
    色谱法的流动相处理

    公开(公告)号：US20060054558A1

    公开(公告)日：2006-03-16

    申请号：US10505289

    申请日：2003-02-20

    申请人： Brian Jones ,  Nathan Porter

    发明人： Brian Jones ,  Nathan Porter

    IPC分类号： B01D15/08

    CPC分类号： B01D15/161 ,  G01N30/30 ,  G01N2030/3007 ,  G01N2030/3023 ,  G01N2030/303 ,  G01N2030/3038 ,  G01N2030/3046

    摘要： A convenient and efficient method for heating or cooling the mobile phase fluid of a chromatographic system prior to its entry into the chromatographic column is described. The “preheating” or “precooling” process is carried out using an apparatus containing a short length of tubing where the mobile phase is heated or cooled. The heating or cooling is performed using a heating or cooling element that is in intimate thermal contact with the exterior of the tubing. The temperature change of the mobile phase is measured downstream by a non-invasive, low-mass sensing element on the exterior of the tubing. With a low mass heating or cooling element, the device can be very responsive and allows for rapid equilibration and convenient temperature programming of the mobile phase. This configuration also requires only a short mobile phase contact time, is non-invasive, adds no dead volume, and allows for use of columns over a wide range of internal diameter, flow rates and temperatures.

    摘要翻译： 描述了在进入色谱柱之前加热或冷却色谱系统的流动相流体的方便和有效的方法。 使用包含流动相加热或冷却的短管道的装置进行“预热”或“预冷”过程。 使用与管道外部紧密热接触的加热或冷却元件进行加热或冷却。 流动相的温度变化通过管道外部的非侵入性，低质量感测元件在下游测量。 使用低质量加热或冷却元件，该装置可以非常响应，并允许流动相的快速平衡和方便的温度编程。 这种配置也只需要很短的流动相接触时间，是非侵入性的，不会增加死体积，并允许在各种内径，流速和温度范围内使用色谱柱。

    Device for coupling a micro-chromatograph with a mass spectrometer and analysis device
    7.
    发明申请
    Device for coupling a micro-chromatograph with a mass spectrometer and analysis device 失效
    用于将微量色谱仪与质谱仪和分析装置连接的装置

    公开(公告)号：US20040025566A1

    公开(公告)日：2004-02-12

    申请号：US10181556

    申请日：2002-07-19

    发明人： Jean-Louis Gass ,  Ronan Cozic ,  Georges Ponchin

    IPC分类号： G01N030/72 ,  G01N030/12 ,  G01N030/06

    CPC分类号： G01N30/7213 ,  G01N2030/3038 ,  G01N2030/7226

    摘要： A coupling device connecting the output of a microchromatograph (nullCG) to the input of a mass spectrometer (SM), said coupling device comprising a capillary tube with one end connected in sealed fashion to the source under vacuum of the mass spectrometer through the intermediary of an interface device, and with the other end connected to the output of the microchromatograph, in slack fashion, open to the atmosphere; the length and the diameter of the capillary tube being chosen such that the flow rate inside the capillary tube is very close to the flow rate at the output from the microchromatograph; the interface device being, furthermore, provided with heating means for very precise adjustment of the flow rate registered by the capillary.

    摘要翻译： 将微量色谱仪（muCG）的输出连接到质谱仪（SM）的输入端的耦合装置，所述耦合装置包括一个毛细管，其一端以密封的方式通过质谱仪的真空连接到源 接口装置，另一端连接微型色谱仪的输出，以松弛的方式连接到大气; 毛细管的长度和直径被选择为使得毛细管内部的流速非常接近微量色谱仪的输出处的流速; 此外，该接口装置设置有用于非常精确地调节由毛细管记录的流量的加热装置。

    Valve
    8.
    发明授权
    Valve 失效
    阀

    公开(公告)号：US5224510A

    公开(公告)日：1993-07-06

    申请号：US606405

    申请日：1990-10-31

    申请人： Nico Pericles

    发明人： Nico Pericles

    IPC分类号： G01N30/02 ,  F16K31/00 ,  F16K31/02 ,  G01N30/20 ,  G01N30/26 ,  G01N30/30 ,  G01N30/32 ,  G01N30/36

    CPC分类号： G01N30/20 ,  F16K31/004 ,  G01N2030/3038 ,  G01N2030/328 ,  G01N30/02 ,  G01N30/32 ,  G01N30/36 ,  Y10T137/6606 ,  Y10T137/7761

    摘要： A high-pressure control valve (2) used in chromatography serves as a counter pressure control valve which, in a separating column, is intended to maintain a specific predeterminable pressure. The valve has a valve seat (12) with an outlet channel opening (18) located in its center and a valve body (13) that cooperates with the valve seat. The valve body (13) can be moved with the aid of a piezo transducer, actively in the opening direction and, while being monitored, actively in the closing direction. The opposed faces of the valve seat (12) and the valve body (13) are so shaped that an annular gap (16) that widens radially towards the outside starting from the opening (18) of the outlet channel is produced. When the valve is in the closed position, this results in the formation of a narrow sealing zone directly at the edge of the opening of the outlet channel.

    摘要翻译： 用于色谱的高压控制阀（2）用作反压控制阀，其在分离柱中旨在保持特定的可预定压力。 阀具有阀座（12），其中位于其中心的出口通道开口（18）和与阀座配合的阀体（13）。 阀体（13）可以借助于压电换能器主动地沿打开方向移动，并且在关闭方向上被主动地被监控。 阀座（12）和阀体（13）的相对面被成形为使得从出口通道的开口（18）径向向外径向扩大的环形间隙（16）。 当阀处于关闭位置时，这导致在出口通道的开口的边缘处直接形成窄的密封区。

    Method and means for vaporizing liquids by means of heating a sample capillary tube for detection or analysis
    9.
    发明授权
    Method and means for vaporizing liquids by means of heating a sample capillary tube for detection or analysis 失效
    通过加热样品毛细管进行检测或分析来蒸发液体的方法和装置

    公开(公告)号：US4960992A

    公开(公告)日：1990-10-02

    申请号：US326150

    申请日：1989-03-20

    申请人： Marvin L. Vestal ,  Calvin R. Blakely ,  Gordon J. Fergusson

    发明人： Marvin L. Vestal ,  Calvin R. Blakely ,  Gordon J. Fergusson

    IPC分类号： G01N30/30 ,  G01N30/32 ,  G01N30/72 ,  H01J49/04 ,  H01J49/10

    CPC分类号： H01J49/049 ,  G01N30/7253 ,  H01J49/0445 ,  H01J49/0486 ,  G01N2030/3038 ,  G01N2030/3053 ,  G01N30/32

    摘要： This disclosure is concerned with method and apparatus for vaporizing liquid solutions in order to detect, quantitate, and/or determine physical or chemical properties of samples present in liquid solution. Mixtures may be separated by an on-line liquid chromatographic column and the methods used for detection, quantitation, identification, and/or determination of chemical and physical properties include mass spectrometry, photoionization, flame ionization, electron capture, optical photometry, including UV, visible, and IR regions of the spectrum, light scattering, light emission, atomic absorption, and any other technique suitable for detecting or analyzing molecules or particles in a gaseous or vacuum environment. The method and apparatus involves controlled partial vaporization of the solution. Methods are disclosed for controlling the degree of partial vaporization and the temperature at which this vaporization occurs, and for maintaining this degree of vaporization essentially constant even though the solvent flow rate and/or composition may vary in either a controlled or an uncontrolled fashion. ThisGOVERNMENT SUPPORTThe invention described herein was made in the course of work under a grant or award from the Department of Health and Human Services (formerly Health Education and Welfare).CROSS REFERENCE TO RELATED APPLICATIONS

    摘要翻译： 本公开涉及用于蒸发液体溶液以便检测，定量和/或确定液体溶液中存在的样品的物理或化学性质的方法和装置。 混合物可以通过在线液相色谱柱分离，用于检测，定量，鉴定和/或测定化学和物理性质的方法包括质谱法，光离子化，火焰离子化，电子捕获，光学光度法，包括UV， 可见光和红外光谱区域，光散射，发光，原子吸收以及适用于在气态或真空环境中检测或分析分子或颗粒的任何其他技术。 该方法和装置包括溶液的受控部分蒸发。 公开了用于控制部分蒸发程度和发生该蒸发的温度的方法，并且为了使该蒸发程度基本上恒定，即使溶剂流速和/或组成可以以受控或不受控制的方式变化。 这种“热喷涂”方法和装置允许溶剂基本上蒸发，以产生含有一部分未蒸发溶剂的超音速自由射流，作为夹带在射流中的液滴。 比溶剂挥发性低的溶质优先包含在液滴中。 公开了用于控制过程发生温度的方法，以防止溶质的不希望的化学改性（例如热解），并防止溶质过早蒸发。

    Method and means for vaporizing liquids for detection or analysis
    10.
    发明授权
    Method and means for vaporizing liquids for detection or analysis 失效
    用于蒸发液体进行检测或分析的方法和装置

    公开(公告)号：US4814612A

    公开(公告)日：1989-03-21

    申请号：US31150

    申请日：1987-03-25

    申请人： Marvin L. Vestal ,  Calvin R. Blakely ,  Gordon J. Fergusson

    发明人： Marvin L. Vestal ,  Calvin R. Blakely ,  Gordon J. Fergusson

    IPC分类号： G01N30/30 ,  G01N30/32 ,  G01N30/72 ,  H01J49/04 ,  H01J49/10 ,  H01J49/28

    CPC分类号： H01J49/049 ,  G01N30/7253 ,  H01J49/0445 ,  H01J49/0486 ,  G01N2030/3038 ,  G01N2030/3053 ,  G01N30/32

    摘要： This disclosure is concerned with method and apparatus for vaporizing liquid solutions in order to detect, quantitate, and/or determine physical or chemical properties of samples present in liquid solution. Mixtures may be separated by an on-line liquid chromatographic column and the methods used for detection, quantitation, identification, and/or determination of chemical and physical properties include mass spectrometry, photoionization, flame ionization, electron capture, optical photometry, including UV, visible, and IR regions of the spectrum, light scattering, light emission, atomic absorption, and any other technique suitable for detecting or analyzing molecules or particles in a gaseous or vacuum environment. The method and apparatus involves controlled partial vaporization of the solution. Methods are disclosed for controlling the degree of partial vaporization and the temperature at which this vaporization occurs, and for maintaining this degree of vaporization essentially constant even though the solvent flow rate and/or composition may vary in either a controlled or an uncontrolled fashion. This "thermospray" method and apparatus allows the solvent to be substantially vaporized to produce a supersonic free jet containing a fractionGOVERNMENT SUPPORTThe invention described herein was made in the course of work under a grant or award from the Department of Health and Human Services (formerly Health Education and Welfare).

    摘要翻译： 本公开涉及用于蒸发液体溶液以便检测，定量和/或确定液体溶液中存在的样品的物理或化学性质的方法和装置。 混合物可以通过在线液相色谱柱分离，用于检测，定量，鉴定和/或测定化学和物理性质的方法包括质谱法，光离子化，火焰离子化，电子捕获，光学光度法，包括UV， 可见光和红外光谱区域，光散射，发光，原子吸收以及适用于在气态或真空环境中检测或分析分子或颗粒的任何其他技术。 该方法和装置包括溶液的受控部分蒸发。 公开了用于控制部分蒸发程度和发生该蒸发的温度的方法，并且为了使该蒸发程度基本上恒定，即使溶剂流速和/或组成可以以受控或不受控制的方式变化。 这种“热喷涂”方法和装置允许溶剂基本上蒸发，以产生含有一部分未蒸发溶剂的超音速自由射流，作为夹带在射流中的液滴。 比溶剂挥发性低的溶质优先包含在液滴中。 公开了用于控制过程发生温度的方法，以防止溶质的不希望的化学改性（例如热解），并防止溶质过早蒸发。