公开(公告)号：US20160121396A1

公开(公告)日：2016-05-05

申请号：US14785237

申请日：2014-04-17

Applicant: ROCKWOOD LITHIUM GMBH

Inventor： Ulrich WIETELMANN ,  Christoph HARTNIG ,  Ute EMMEL ,  Vera NICKEL

IPC: B22F1/00 ,  H01M4/36 ,  H01M4/62 ,  H01M4/38

CPC classification number: B22F1/0088 ,  B22F1/0003 ,  B22F1/02 ,  B22F2201/016 ,  B22F2201/02 ,  B22F2301/054 ,  B22F2302/45 ,  B22F2999/00 ,  C01B21/061 ,  C01B21/0926 ,  C01D15/00 ,  C01P2006/80 ,  H01M4/134 ,  H01M4/366 ,  H01M4/382 ,  H01M4/628 ,  H01M10/052 ,  H01M2004/027 ,  B22F9/18 ,  B22F2201/013

Abstract: The invention relates to particulate lithium metal formations having a substantially spherical geometry and a core composed of metallic lithium, which are enclosed with an outer passivating but ionically conductive layer containing nitrogen. The invention further relates to a method for producing lithium metal formations by reacting lithium metal with one or more passivating agent(s) containing nitrogen, selected from the groups N2, NxHy with x=1 or 2 and y=3 or 4, or a compound containing only the elements C, H, and N, and optionally Li, at temperatures in the range between 60 and 300° C., preferably between 100 and 280° C., and particularly preferably above the melting temperature of lithium of 180.5° C., in an inert organic solvent under dispersion conditions or in an atmosphere that contains a gaseous coating agent containing nitrogen.

Abstract translation: 本发明涉及具有基本球形几何形状的颗粒状锂金属结构和由金属锂构成的芯，其由含有氮的外部钝化但离子导电层包围。 本发明还涉及通过使锂金属与一种或多种含氮的钝化剂反应来制备锂金属层的方法，所述钝化剂选自N2，NxHy，x = 1或2，y = 3或4，或 仅含有元素C，H和N以及任选的Li的化合物在温度范围为60至300℃之间，优选为100至280℃的温度下，特别优选高于约180.5℃的锂的熔融温度 在惰性有机溶剂中，在分散条件下或在含有含氮气体包衣剂的气氛中。

公开(公告)号：US09327448B2

公开(公告)日：2016-05-03

申请号：US14449839

申请日：2014-08-01

Applicant: Northwestern University

Inventor： Ramille N. Shah ,  Adam E. Jakus ,  David C. Dunand

IPC: B29C67/00 ,  B22F3/00 ,  B22F3/22

CPC classification number: B29C67/0055 ,  B22F3/008 ,  B22F3/227 ,  B22F2201/013 ,  B29C64/106

Abstract: Methods of forming three-dimensional metallic objects are provided. A metal oxide paste comprising metal oxide particles, a polymeric binder and an organic solvent is extruded through a tip to deposit sequential layers of the metal oxide paste on a substrate to form a three-dimensional metal oxide object. The three-dimensional metal oxide object is exposed to a reducing gas at a temperature and for a period of time sufficient to reduce and to sinter the metal oxide particles to form a three-dimensional metallic object. Depending upon the composition of the metal oxide paste, the three-dimensional metallic object may be composed of a single metal, a simple or complex metal-metal alloy, or a metal-ceramic composite.

Abstract translation: 提供形成三维金属物体的方法。 将包含金属氧化物颗粒，聚合物粘合剂和有机溶剂的金属氧化物糊料通过尖端挤出以在基板上沉积金属氧化物浆料的顺序层以形成三维金属氧化物物体。 三维金属氧化物物体在足以减少和烧结金属氧化物颗粒以形成三维金属物体的温度和时间的温度下暴露于还原气体。 根据金属氧化物糊的组成，三维金属物体可以由单一金属，简单或复杂的金属 - 金属合金或金属 - 陶瓷复合材料构成。

公开(公告)号：US09283622B2

公开(公告)日：2016-03-15

申请号：US12867501

申请日：2009-02-27

Applicant: Ahmet Karaca ,  Bernd Sermond ,  Gerhard Wilfing

Inventor： Ahmet Karaca ,  Bernd Sermond ,  Gerhard Wilfing

IPC: B22F9/20 ,  C01B6/24 ,  C22B5/04 ,  C22B34/12 ,  C22B34/14 ,  C22C1/04 ,  C22C9/00 ,  C22C14/00 ,  C22C16/00 ,  C22C19/03 ,  C22C27/04

CPC classification number: B22F9/20 ,  B22F2998/00 ,  B22F2998/10 ,  B22F2999/00 ,  C01B6/24 ,  C22B5/04 ,  C22B34/1268 ,  C22B34/1286 ,  C22B34/14 ,  C22C1/0458 ,  C22C9/00 ,  C22C14/00 ,  C22C16/00 ,  C22C19/03 ,  C22C27/04 ,  B22F1/0011 ,  C23F1/00 ,  B22F2201/11 ,  B22F2201/013 ,  B22F2201/12 ,  B22F2201/02

Abstract: A method for manufacturing alloy powders based on titanium, zirconium and hafnium alloyed with the elements Ni, Cu, Ta, W, Re, Os, and Ir is described in which an oxide of Ti and Zr and Hf is mixed with a metal powder of the elements named and with a reducing agent, and wherein this mixture is heated in a furnace, optionally under a argonate atmosphere or, optionally under hydrogen atmosphere until the reducing reaction begins, the reaction product is leached and then washed and dried, wherein the oxide used has an average grain size of 0.5 to 20 μm, a specific surface area according to BET of 0.5 20 m2/g and a minimum content of 94 wet. −%. An easy to produce powder, in particular in relation to the ignition point and burning time, is produced.

Abstract translation: 描述了与元素Ni，Cu，Ta，W，Re，Os和Ir合金化的钛，锆和铪合金粉末的制造方法，其中将Ti和Zr和Hf的氧化物与金属粉末 所述元件命名为还原剂，并且其中将该混合物在炉中任选地在氩气气氛下或任选在氢气氛下加热直到还原反应开始，将反应产物浸出，然后洗涤并干燥，其中氧化物 使用的平均粒径为0.5〜20μm，BET比表面积为0.5±20m2 / g，最小含量为94°。 - ％。 特别是相对于点火点和燃烧时间产生粉末易于生产。

公开(公告)号：US20150343667A1

公开(公告)日：2015-12-03

申请号：US14291578

申请日：2014-05-30

Applicant: Kennametal Inc.

Inventor： J. Denny Robertson ,  Debangshu Banerjee ,  Hugo Serrano ,  Yujiao Zou

IPC: B29B11/02 ,  C22C29/08 ,  B02C18/18 ,  C22C29/06

CPC classification number: B29B11/02 ,  B22F2998/10 ,  B22F2999/00 ,  B26D2001/002 ,  B26D2001/0033 ,  B29B9/06 ,  B29B9/065 ,  C22C29/06 ,  C22C29/067 ,  C22C29/08 ,  C22C29/10 ,  C22C1/1084 ,  B22F1/0059 ,  B22F3/02 ,  B22F3/1021 ,  B22F3/04 ,  B22F3/15 ,  B22F3/225 ,  B22F3/20 ,  B22F2009/042 ,  B22F2009/043 ,  B22F2201/013 ,  B22F2201/20

Abstract: Pelletizing die and knife assemblies that may be used for pelletization of plastic extrudate are disclosed. The knife assemblies may include an extrusion die and a rotary knife hub assembly. The rotary knife hub assembly may comprise a hub having multiple pelletizer cutting knives mounted thereon. Each knife may include a cutting blade insert mounted on a body of the knife. The cutting blade inserts may comprise a composite material having a continuous metal matrix with hard metal carbide particles dispersed therein. The composite material has relatively high hardness and good wear resistance properties, but may have a hardness less than the hardness of the pelletizing die surface in order to reduce wear of the die face.

Abstract translation: 公开了可用于塑料挤出物造粒的造粒模和刀组件。 刀组件可以包括挤出模头和旋转刀毂组件。 旋转刀毂组件可以包括具有安装在其上的多个造粒机切割刀的轮毂。 每个刀可以包括安装在刀体上的切割刀片插入件。 切割刀片插入件可以包括具有分散在其中的硬质金属碳化物颗粒的连续金属基体的复合材料。 复合材料具有相对较高的硬度和良好的耐磨性能，但是其硬度可以小于造粒模具表面的硬度，以减少模具表面的磨损。

公开(公告)号：US20150314232A1

公开(公告)日：2015-11-05

申请号：US14678372

申请日：2015-04-03

Applicant: University of South Carolina

Inventor： Fanglin Chen ,  Shumin Fang ,  Kyle S. Brinkman

IPC: B01D53/22 ,  B01D67/00 ,  B22F5/00 ,  B01D71/02 ,  B22F3/12 ,  C01B3/50 ,  B01D69/12

CPC classification number: B01D53/22 ,  B01D53/228 ,  B01D67/0041 ,  B01D67/0083 ,  B01D69/12 ,  B01D69/141 ,  B01D71/022 ,  B01D71/024 ,  B01D2256/16 ,  B01D2323/08 ,  B01D2323/12 ,  B01D2325/20 ,  B22F3/12 ,  B22F5/006 ,  B22F2998/10 ,  C01B3/503 ,  C01B2203/0233 ,  C01B2203/0405 ,  C01B2203/0475 ,  C01B2203/0495 ,  C22C1/05 ,  C22C29/12 ,  H01M8/124 ,  H01M2300/0091 ,  Y02P70/56 ,  B22F3/1017 ,  B22F3/101 ,  B22F2201/02 ,  B22F2201/11 ,  B22F2201/013

Abstract: A hydrogen permeation membrane is provided that can include a metal and a ceramic material mixed together. The metal can be Ni, Zr, Nb, Ta, Y, Pd, Fe, Cr, Co, V, or combinations thereof, and the ceramic material can have the formula: BaZr1-x-yYxTyO3-δ where 0≦x≦0.5, 0≦y≦0.5, (x+y)>0; 0≦δ≦0.5, and T is Sc, Ti, Nb, Ta, Mo, Mn, Fe, Co, Ni, Cu, Zn, Ga, In, Sn, or combinations thereof. A method of forming such a membrane is also provided. A method is also provided for extracting hydrogen from a feed stream.

Abstract translation: 提供了可以包括混合在一起的金属和陶瓷材料的氢渗透膜。 金属可以是Ni，Zr，Nb，Ta，Y，Pd，Fe，Cr，Co，V或它们的组合，陶瓷材料可以具有下式：BaZr1-x-yYxTyO3-δ其​​中0＆nlE; x＆nlE; 0.5 ，0＆nlE; y＆nlE; 0.5，（x + y）> 0; 0＆nlE;δ＆nlE; 0.5，T是Sc，Ti，Nb，Ta，Mo，Mn，Fe，Co，Ni，Cu，Zn，Ga，In，Sn或其组合。 还提供了形成这种膜的方法。 还提供了用于从进料流中提取氢的方法。

公开(公告)号：US20150302960A1

公开(公告)日：2015-10-22

申请号：US14441944

申请日：2013-11-08

Applicant: XIAMEN TUNGSTEN CO., LTD.

Inventor： Hiroshi NAGATA ,  Chonghu WU

IPC: H01F1/057 ,  C21D6/00 ,  C22C1/06 ,  C22C38/00 ,  C22C38/16 ,  C22C38/14 ,  C22C38/06 ,  C22C33/00 ,  B22F9/04 ,  B22F3/12 ,  B22F3/04 ,  H01F1/08 ,  H01F1/053 ,  H01F1/055 ,  H01F41/02 ,  C21D3/06

CPC classification number: H01F1/0573 ,  B22F3/04 ,  B22F3/12 ,  B22F9/04 ,  B22F2999/00 ,  C21D3/06 ,  C21D6/007 ,  C22C1/06 ,  C22C33/00 ,  C22C38/002 ,  C22C38/005 ,  C22C38/007 ,  C22C38/02 ,  C22C38/04 ,  C22C38/06 ,  C22C38/10 ,  C22C38/12 ,  C22C38/14 ,  C22C38/16 ,  C22C2202/02 ,  H01F1/0536 ,  H01F1/0557 ,  H01F1/0577 ,  H01F1/086 ,  H01F41/0266 ,  B22F2009/045 ,  B22F2201/013

Abstract: The present invention discloses manufacturing methods of a powder for compacting rare earth magnet and rare earth magnet that omit jet milling process, which comprise the steps as follows: 1) casting: casting the molten alloy of rare earth magnet raw material by strip casting method to obtain a quenched alloy with average thickness in a range of 0.2˜0.4 mm; 2) hydrogen decrepitation: decrepitating the quenched alloy hydrogen under a hydrogen pressure between 0.01˜1 MPa for 0.5˜24 h to obtain the powder. The present invention improves the manufacturing processes which are before the process of jet milling for omitting the process of jet milling, thus simplifying the process; which may also acquire a low cost production by efficiently using the precious rare earth resource.

Abstract translation: 本发明公开了一种用于压实稀土磁体和稀土磁体的粉末的制造方法，该方法包括以下步骤：1）铸造：通过带式铸造法将稀土磁体原料的熔​​融合金铸造成 获得平均厚度在0.2〜0.4mm范围内的淬火合金; 2）氢气爆裂：在0.01〜1MPa的氢气压力下将淬火的合金氢气破裂0.5〜24h，得到粉末。 本发明改进了在喷射研磨过程之前的制造过程，以省略喷射铣削的过程，从而简化了工艺过程; 也可以通过有效利用稀土资源获得低成本生产。

公开(公告)号：US20150246393A1

公开(公告)日：2015-09-03

申请号：US14556105

申请日：2014-11-29

Applicant: Hyundai Motor Company

Inventor： Hak-Soo Kim ,  Boo-Yong Jung

IPC: B22F5/00 ,  F02F3/00 ,  B22F3/24 ,  B22F3/12 ,  B22F3/17

CPC classification number: B22F5/00 ,  B22F3/1007 ,  B22F3/12 ,  B22F3/17 ,  B22F3/24 ,  B22F2003/033 ,  B22F2003/247 ,  B22F2003/248 ,  B22F2998/10 ,  B22F2999/00 ,  F02F3/0015 ,  F16C7/023 ,  F16C2220/20 ,  F16C2220/46 ,  F16C2223/08 ,  B22F3/02 ,  B22F2203/11 ,  B22F2201/013 ,  B22F2201/02

Abstract: Disclosed is a method of manufacturing a connecting rod by using semi-closed sinter forging. The method includes: a first step of positioning a metal powder of a sintering material in a closed mold and then forming a preliminary formed body by using a general forming press; a second step of heating the formed preliminary formed body to sinter the preliminary formed body; a third step of semi-closed forging the sintered preliminary formed body to manufacture a forged part; a fourth step of cooling the manufactured forged part to normal temperature; a fifth step of removing a flash from the cooled forged part through a punching process; and a sixth step of manufacturing the connecting rod through a shot blast treatment in order to remove a foreign substance existing on a surface of the forged part from which the flash is removed.

Abstract translation: 公开了通过使用半封闭烧结锻造制造连杆的方法。 该方法包括：第一步骤，将烧结材料的金属粉末定位在闭合的模具中，然后通过使用普通成形压机形成初步成形体; 第二步骤，加热形成的初步成形体以烧结初步成形体; 半封闭锻造烧结预成形体以制造锻造部件的第三步骤; 将制造的锻造部件冷却至常温的第四步骤; 通过冲压工艺从冷却的锻造部件去除闪光的第五步骤; 以及通过喷丸处理制造连杆的第六步骤，以去除存在于从其中去除闪光的锻造部件的表面上的异物。

公开(公告)号：US09108275B2

公开(公告)日：2015-08-18

申请号：US14050501

申请日：2013-10-10

Applicant: Federal-Mogul Corporation

Inventor： David Michael Saxton

IPC: B23K31/00 ,  B23K35/24 ,  B23K37/00 ,  B22F7/04 ,  B23K20/227 ,  B32B15/01 ,  F16C33/14 ,  B23K1/00 ,  B23K1/19 ,  B21B1/38 ,  B23K20/04 ,  B22F3/18 ,  C22C21/00 ,  C22C38/00 ,  B23K35/30 ,  B23K35/02 ,  F16C33/12 ,  C22C1/04

CPC classification number: B23K35/24 ,  B21B1/38 ,  B22F3/18 ,  B22F7/04 ,  B22F2003/185 ,  B22F2999/00 ,  B23K1/0008 ,  B23K1/19 ,  B23K20/04 ,  B23K20/2275 ,  B23K35/0244 ,  B23K35/302 ,  B23K37/003 ,  B23K2101/185 ,  B23K2103/20 ,  B32B3/263 ,  B32B7/04 ,  B32B15/012 ,  B32B15/013 ,  B32B15/015 ,  B32B2250/02 ,  B32B2255/06 ,  B32B2255/205 ,  B32B2264/105 ,  B32B2475/00 ,  B32B2605/08 ,  C22C1/0425 ,  C22C21/00 ,  C22C38/00 ,  F16C33/122 ,  F16C33/14 ,  F16C2223/32 ,  F16C2223/80 ,  Y10T428/12069 ,  B22F2201/013 ,  B22F2202/05

Abstract: A continuous hot bonding method for producing a bi-material strip with a strong bond therebetween is provided. The method comprises sanding a first strip formed of steel; and applying a layer of first particles, typically formed of copper, to the sanded first strip. The method next includes heating the first strip and the layer of the first particles, followed by pressing a second strip formed of an aluminum alloy onto the heated layer of the first particles. The aluminum alloy of the second strip includes tin particles, and the heat causes the second particles to liquefy and dissolve into the melted first particles. The first particles and the second particles bond together to form bond enhancing metal particles, which typically comprise bronze.

Abstract translation: 提供了一种连续热粘合方法，用于制造其间具有很强粘合力的双材料条。 该方法包括对由钢形成的第一条带进行砂磨; 以及将通常由铜形成的第一颗粒层施加到砂磨的第一条带上。 该方法接下来包括加热第一条带和第一颗粒层，然后将由铝合金形成的第二条带压在第一颗粒的加热层上。 第二条带的铝合金包括锡颗粒，并且热使得第二颗粒液化并溶解到熔融的第一颗粒中。 第一颗粒和第二颗粒结合在一起以形成粘结增强金属颗粒，其通常包括青铜。

公开(公告)号：US09067264B2

公开(公告)日：2015-06-30

申请号：US13480436

申请日：2012-05-24

Applicant: Vladimir S. Moxson ,  Volodymyr A. Duz ,  Andrey G. Klevtsov ,  Viktor D. Sukhoplyuyev ,  Mihajlo D. Sopka ,  Yury V. Shuvalov ,  Mykhailo Matviychuk

Inventor： Vladimir S. Moxson ,  Volodymyr A. Duz ,  Andrey G. Klevtsov ,  Viktor D. Sukhoplyuyev ,  Mihajlo D. Sopka ,  Yury V. Shuvalov ,  Mykhailo Matviychuk

IPC: C01B6/02 ,  C01B6/24 ,  B22F3/24 ,  B22F9/18 ,  B22F9/20 ,  B22F3/10

CPC classification number: B22F9/20 ,  B22F3/1007 ,  B22F3/1017 ,  B22F3/24 ,  B22F9/18 ,  B22F2998/10 ,  B22F2999/00 ,  C01B6/02 ,  C01B6/24 ,  B22F3/11 ,  B22F2003/248 ,  B22F9/04 ,  B22F3/02 ,  B22F2201/013

Abstract: The invention relates to energy-saving manufacturing of purified hydrogenated titanium powders or alloying titanium hydride powders, by metallo-thermic reduction of titanium chlorides, including their hydrogenation, vacuum separation of titanium hydride sponge block from magnesium and magnesium chlorides, followed by crushing, grinding, and sintering of said block without need for any hydro-metallurgical treatment of the produced powders. Methods disclosed contain embodiments of processes for manufacturing high purity high-purity powders and their use in manufacturing near-net shape titanium and titanium-alloy articles by sintering titanium hydride and alloyed titanium hydride powders produced from combined hydrogen-magnesium reduction of titanium chlorides, halides and hydrides of other metals. Additional titanium hydride powder introduced with titanium tetrachloride beneficially affects the kinetics of magnesium-thermic reduction due to formation of additionally-emitted atomic hydrogen, which helps to reduce presence of oxides, and so cleans inter-particle interfaces of the product and enhances diffusion between all components of the powder mixture.

Abstract translation: 本发明涉及通过金属热还原氯化钛，包括氢化，氢化镁海绵块与镁和氯化镁的真空分离，然后进行粉碎，研磨，纯化氢化钛粉末或合金化氢化钛粉末的节能制造 ，并且所述块的烧结，而不需要对生产的粉末进行任何氢化冶金处理。 公开的方法包括制造高纯度高纯度粉末的方法的实施方案及其在制造近净形状钛和钛合金制品中的用途，其通过烧结氢化钛和由氯化钛，卤化物的组合氢 - 镁还原制备的合金氢化钛粉末 和其他金属的氢化物。 引入四氯化钛的另外的氢化钛粉末有利地影响由于形成额外发射的原子氢而导致的镁热还原的动力学，这有助于减少氧化物的存在，并且因此清除产物的颗粒间界面并增强所有的 粉末混合物的组分。

公开(公告)号：US20150130121A1

公开(公告)日：2015-05-14

申请号：US14079768

申请日：2013-11-14

Applicant: Ulrich Gerhard BAUDIS

Inventor： Ulrich Gerhard BAUDIS

IPC: F27B19/02 ,  C22B5/00 ,  C22B9/05 ,  B22F9/18

CPC classification number: F27B19/02 ,  B22F9/18 ,  B22F9/20 ,  B22F9/22 ,  B22F2999/00 ,  C22B5/04 ,  C22B34/10 ,  C22B34/1268 ,  C22B34/1277 ,  C22B34/14 ,  F27D2005/0075 ,  Y10T428/2982 ,  B22F2201/013 ,  B22F2201/016 ,  B22F2201/02 ,  B22F2201/04 ,  B22F2201/30 ,  B22F2201/40

Abstract: A reaction vessel for making phlegmatized metal powder or alloy powder has a retort crucible with a heat-proof, coolable cover, a heatable reduction furnace into which the retort crucible may be inserted, and an inner crucible placed within the retort crucible and removable therefrom. At least one inlet is built into the coolable cover for adding a passivating gas. A heat-proof flange welded onto the retort crucible attaches the retort crucible to the heat-proof, coolable cover. A cooler welded onto a lower face of the heat-proof flange provides a cooling agent to the reaction vessel.

Abstract translation: 用于制造钝化金属粉末或合金粉末的反应容器具有带有耐热冷却盖的蒸煮坩埚，可插入蒸煮坩埚的可加热还原炉，以及放置在蒸煮坩埚内并可从其中除去的内坩埚。 至少一个入口内置在可冷却盖中，用于添加钝化气体。 焊接在蒸馏坩埚上的防热法兰将蒸馏坩埚连接到耐热可冷却的盖子上。 焊接到耐热凸缘的下表面上的冷却器向反应容器提供冷却剂。