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    Three-catalyst process for the hydrotreating of heavy hydrocarbon streams
    32.
    发明授权
    Three-catalyst process for the hydrotreating of heavy hydrocarbon streams 失效
    用于加氢处理重质烃流的三催化过程

    公开(公告)号：US4431525A

    公开(公告)日：1984-02-14

    申请号：US371815

    申请日：1982-04-26

    Applicant: Albert L. Hensley, Jr. ,  Leonard M. Quick

    Inventor： Albert L. Hensley, Jr. ,  Leonard M. Quick

    IPC: B01J35/10 ,  C10G45/04 ,  C10G45/08 ,  C10G65/04

    CPC classification number: B01J35/10 ,  B01J35/1019 ,  B01J35/1042 ,  B01J35/1061 ,  B01J35/1085 ,  C10G2300/107

    Abstract: There is disclosed a process for hydrotreating a heavy hydrocarbon stream containing metals, asphaltenes, nitrogen compounds, and sulfur compounds to reduce the contents of these contaminants. The process comprises contacting said stream in the presence of hydrogen and under suitable hydrotreating conditions in sequence with a first catalyst in a first reaction zone, a second catalyst in a second reaction zone, and a third catalyst in a third reaction zone. The first catalyst comprises a Group VIB metal and/or a Group VIII metal on a porous inorganic oxide support; the second catalyst consists essentially of at least one hydrogenation metal selected from Group VIB deposed on a support material comprising alumina; and the third catalyst comprises a hydrogenating component comprising molybdenum, chromium, and cobalt on a large-pore, catalytically-active alumina. Each catalyst has specific physical properties.

    Abstract translation: 公开了一种加氢处理含有金属，沥青质，氮化合物和硫化合物的重质烃流的方法，以减少这些污染物的含量。 该方法包括在氢气存在下，在合适的加氢处理条件下，将第一催化剂在第一反应区，第二反应区中的第二催化剂和第三反应区中的第三催化剂依次接触。 第一催化剂在多孔无机氧化物载体上包含VIB族金属和/或Ⅷ族金属; 第二催化剂基本上由至少一种氢化金属组成，所述氢化金属选自ⅤB组，其包含氧化铝的载体材料; 并且第三催化剂包含在大孔催化活性氧化铝上的包含钼，铬和钴的氢化组分。 每种催化剂都具有特定的物理性质。

    Method for preparing a catalyst carrier, a catalyst containing the carrier, and a hydrocarbon hydrodesulfurization process using the catalyst
    33.
    发明授权
    Method for preparing a catalyst carrier, a catalyst containing the carrier, and a hydrocarbon hydrodesulfurization process using the catalyst 失效
    制备催化剂载体的方法，含有载体的催化剂和使用该催化剂的烃加氢脱硫方法

    公开(公告)号：US4341625A

    公开(公告)日：1982-07-27

    申请号：US159887

    申请日：1980-06-16

    Applicant: Paul W. Tamm

    Inventor： Paul W. Tamm

    IPC: B01J23/85 ,  B01J23/88 ,  B01J27/188 ,  B01J35/10 ,  B01J37/00 ,  C10G45/08 ,  C10G45/06

    CPC classification number: B01J37/0009 ,  B01J23/85 ,  B01J23/88 ,  B01J27/188 ,  B01J35/10 ,  B01J35/1042 ,  B01J35/1061 ,  B01J35/1066 ,  B01J35/1085 ,  C10G2300/107 ,  Y10S423/13 ,  Y10S585/906

    Abstract: A method is provided for preparing a porous catalyst carrier having a pore volume of at least 0.5 cc/g, a content of micropores in which the pore diameter is between 80 and 150 A. which constitutes at least 70% of the pore volume and a content of macropores which constitutes less than 3% of the pore volume. In the method, a powdered solid comprised of predominantly alpha-alumina monohydrate and sized in the range below 500 microns is treated with a particular amount of a monobasic acid. The acid in the resulting mixture is then at least partially neutralized by admixing with a nitrogen base such as aqueous ammonia. The treated and neutralized feed is converted into a catalyst carrier by shaping as desired, drying, and calcining. Further aspects of the invention are a hydrodesulfurization catalyst prepared using the present carrier and a hydrodesulfurization process for metals-contaminated hydrocarbon feeds using the catalyst.

    Abstract translation: 提供了一种制备孔体积为至少0.5cc / g的多孔催化剂载体的方法，孔径为80至150的微孔含量，其构成孔体积的至少70％，和 构成小于孔体积的3％的大孔的含量。 在该方法中，主要由α-氧化铝一水合物组成的粉末状固体，其尺寸在500微米以下，用特定量的一元酸处理。 然后通过与氮碱如氨水混合，将所得混合物中的酸至少部分中和。 经处理和中和的进料通过根据需要成型，干燥和煅烧而转化成催化剂载体。 本发明的其它方面是使用本载体制备的加氢脱硫催化剂和使用该催化剂的金属污染的烃进料的加氢脱硫方法。

    Process for preparing a heavy crude conversion catalyst
    34.
    发明授权
    Process for preparing a heavy crude conversion catalyst 失效
    制备重质粗转化催化剂的方法

    公开(公告)号：US3993601A

    公开(公告)日：1976-11-23

    申请号：US533313

    申请日：1974-12-16

    Applicant: Fred M. Long ,  Willard H. Sawyer

    Inventor： Fred M. Long ,  Willard H. Sawyer

    IPC: B01J23/74 ,  B01J23/85 ,  B01J35/10 ,  B01J37/00 ,  C10G45/08 ,  B01J21/04 ,  B01J23/10 ,  B01J23/84

    CPC classification number: B01J37/0009 ,  B01J23/74 ,  B01J23/85 ,  B01J35/10 ,  C10G45/08 ,  B01J35/1019 ,  B01J35/1042 ,  B01J35/1047 ,  B01J35/1061 ,  B01J35/1085

    Abstract: This invention relates to novel catalysts, of two distinct types, useful for the catalytic hydroconversion of the 1050.degree. F.+ hydrocarbon material contained in heavy crudes and residua such that the resulting product will be suitable for further processing in conventional refinery operations allowing maximization of clean liquid products. Catalysts, which include Group VIB and Group VIII metals, preferably in admixture, and preferably including a Group IVA metal, notably germanium, having certain critical ranges of physical characteristics inclusive of large uniform pore sizes, are used for the conversion, these having been shown to possess improved catalytic activity and selectivity for the hydroconversion of the 1050.degree. F.+ materials of the heavy feeds and residua. Novel methods are described for the preparation of such catalysts, as well as for use of such catalyst. One of the catalysts, i.e., one having properties inclusive of a large number of pores in the 100-275A pore size diameter range, is particularly suitable as a first stage catalyst and the other, which has properties inclusive of a large number of pores in the 100-200A pore size diameter, is especially suitable as a second stage catalyst for use in processing the effluent of said first stage.

    Abstract translation: 本发明涉及两种不同类型的新型催化剂，其可用于重质原油和残余物中所含的1050°F +烃材料的催化加氢转化，使得所得产物将适用于常规精炼操作中的进一步加工，从而使 清洁液体产品。 使用包括VIB族和VIII族金属的催化剂，优选以混合物形式，优选包括具有特定临界范围物理特性（包括大的均匀孔径）的IVA族金属，特别是锗，用于转化，这些已经显示 具有改善催化活性和选择性的1050°F +重料和残渣的材料的加氢转化。 描述了用于制备这种催化剂的新方法，以及使用这种催化剂。 一种催化剂，即在100-275A孔径范围内具有包括大量孔的特性的催化剂，特别适合作为第一级催化剂，另一种具有包括大量孔的性质 100-200A孔径直径，特别适用于用于处理所述第一阶段的流出物的第二阶段催化剂。

    Hydrocracking catalyst
    37.
    发明授权
    Hydrocracking catalyst 有权
    加氢裂化催化剂

    公开(公告)号：US09199228B2

    公开(公告)日：2015-12-01

    申请号：US13266713

    申请日：2010-04-15

    Applicant: László Domokos ,  Cornelis Ouwehand

    Inventor： László Domokos ,  Cornelis Ouwehand

    IPC: B01J29/06 ,  B01J29/16 ,  B01J29/08 ,  B01J29/14 ,  B01J29/80 ,  C10G47/16 ,  C10G47/18 ,  C10G47/20 ,  B01J29/70 ,  B01J29/78 ,  B01J35/10

    CPC classification number: B01J29/166 ,  B01J29/084 ,  B01J29/146 ,  B01J29/7007 ,  B01J29/7815 ,  B01J29/80 ,  B01J35/1038 ,  B01J35/1061 ,  B01J35/1085 ,  B01J37/0009 ,  B01J37/0201 ,  B01J2229/16 ,  B01J2229/18 ,  B01J2229/20 ,  B01J2229/40 ,  B01J2229/42 ,  C10G47/16 ,  C10G47/18 ,  C10G47/20 ,  C10G2300/70

    Abstract: Process of preparing a hydrocracking catalyst carrier comprising amorphous binder and zeolite Y, which process comprises subjecting zeolite Y having a silica to alumina molar ratio of at least 10 to calcination at a temperature of from 700 to 1000° C., hydrocracking catalyst carrier comprising amorphous binder and zeolite Y having a silica to alumina molar ratio of at least 10, the infrared spectrum of which catalyst has a peak at 3690 cm−1, substantially reduced peaks at 3630 cm−1 and 3565 cm−1 and no peak at 3600 cm−1, hydrocracking catalyst carrier comprising an amorphous binder and zeolite Y having a silica to alumina molar ratio of at least 10, which catalyst has an acidity as measured by exchange with perdeuterated benzene of at most 20 micro-mole/gram, hydrocracking catalyst derived from such carrier and hydrocracking process with the help of such catalyst.

    Abstract translation: 制备包含无定形粘合剂和沸石Y的加氢裂化催化剂载体的方法，该方法包括将二氧化硅与氧化铝摩尔比至少为10的沸石Y在700至1000℃的温度下煅烧，加氢裂化催化剂载体包含非晶态 粘结剂和二氧化硅与氧化铝摩尔比至少为10的沸石Y，其催化剂在3690cm -1处具有峰值的红外光谱，在3630cm-1和3565cm -1处基本上减少的峰，在3600cm处没有峰 -1，包含无定形粘合剂的加氢裂化催化剂载体和二氧化硅与氧化铝摩尔比至少为10的沸石Y，该催化剂具有通过与每氘代苯交换至多20微摩尔/克的加氢裂化催化剂得到的酸度 从这种载体和加氢裂化过程中借助于这种催化剂。

    CATALYST AND CATALYST CARRIER
    39.
    发明申请
    CATALYST AND CATALYST CARRIER 有权
    催化剂和催化剂载体

    公开(公告)号：US20140100379A1

    公开(公告)日：2014-04-10

    申请号：US13648303

    申请日：2012-10-10

    Applicant: Michael A. Richard ,  John R. Lockemeyer

    Inventor： Michael A. Richard ,  John R. Lockemeyer

    IPC: B01J27/02 ,  C07D301/04

    CPC classification number: B01J27/047 ,  B01J21/04 ,  B01J23/50 ,  B01J23/66 ,  B01J27/02 ,  B01J27/055 ,  B01J35/1085 ,  B01J35/109 ,  B01J35/1095 ,  C07D301/04 ,  C07D301/10 ,  Y02P20/52

    Abstract: The carrier of the present invention includes at least 85 wt percent alpha alumina, at least 0.06 wt percent SiO2 and no more than 0.04 wt percent Na2O. The carrier has a water absorption no greater than 0.35 g/g and a ratio of water absorption (g/g) to surface area (m2/g) no greater than 0.50 g/m2. Another aspect of the invention is a catalyst for the epoxidation of olefins which comprises the above described carrier and silver dispersed thereon, where the carrier has a monomodal, bimodal or multimodal pore distribution and where the quantity of silver is between 5 and 50 wt %, relative to the weight of the catalyst. A reactor to system for the epoxidation of olefins is also disclosed.

    Abstract translation: 本发明的载体包括至少85wt％的α氧化铝，至少0.06wt％的SiO 2和不超过0.04wt％的Na 2 O. 载体的吸水率不大于0.35g / g，吸水率（g / g）与表面积（m2 / g）不大于0.50g / m 2。 本发明的另一方面是用于烯烃环氧化的催化剂，其包含分散在其上的上述载体和银，其中载体具有单峰，双峰或多峰孔分布，并且其中银的量为5至50重量％ 相对于催化剂的重量。 还公开了用于烯烃的环氧化反应器的反应器。

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