Gas chromatography-ion mobility spectrometry apparatus

    公开(公告)号:US10234436B2

    公开(公告)日:2019-03-19

    申请号:US15827703

    申请日:2017-11-30

    Abstract: The present disclosure provides a gas chromatography-ion mobility spectrometry apparatus, including a housing, an injection port mounted to and connected with the housing and configured for input of a gas containing a sample therein, a multicapillary column configured for separation of a gas substance and an ion mobility tub configured for analysis of the gas substance. The gas chromatography-ion mobility spectrometry apparatus further includes: a gas path part connected with the ion mobility tube and configured for providing the gas to the ion mobility tube and receiving a gas discharged from the ion mobility tube; and a buffer base part detachably mounted to the housing and configured to isolation vibration outside the buffer base part, the ion mobility tube being disposed on the buffer base part, wherein the gas path part is mounted in an interior space of the buffer base part.

    Sample introduction device
    72.
    发明授权

    公开(公告)号:US10032616B2

    公开(公告)日:2018-07-24

    申请号:US14985219

    申请日:2015-12-30

    Abstract: A sample introduction device comprises a sampling unit, a gas suction pump, adsorption units, a piston cylinder and a desorption cylinder that comprises a desorption chamber, a carrier-gas inlet, a split/purge vent and an analyzer nozzle communicating with the desorption chamber. A heating film and a temperature sensor are provided on outer wall of the desorption cylinder. The piston cylinder above the desorption cylinder comprises two piston chambers, each of which is provided with the adsorption unit and in communication with the desorption chamber. The piston cylinder comprises a sample-gas inlet connected to the sampling unit and a gas-suction-pump orifice connected to the gas suction pump, each of which can communicate with both piston chambers. Each adsorption unit comprises an adsorption cylinder-like screen for holding adsorbents and a piston rod slidably mounted in the piston chamber. Each adsorption cylinder-like screen can simultaneously communicate with the sample-gas inlet and gas-suction-pump orifice.

    ION MOBILITY SPECTROMETER
    73.
    发明申请

    公开(公告)号:US20180182606A1

    公开(公告)日:2018-06-28

    申请号:US15832193

    申请日:2017-12-05

    CPC classification number: H01J49/168 G01N27/622 H01J49/0013 H01J49/022

    Abstract: The present disclosure provides an ion mobility spectrometer, which comprises: a power supply circuit, configured to provide a power supply voltage; a corona discharge configured to generate ions to be subjected to measurement, through corona discharge; an ion migration circuit configured to control migration of the ions; a migration zone structure configured to realize, under control of the ion migration circuit, mobility spectrum measurement of the ions which pass through the migration zone structure; a redundant charge extraction electrode arranged between the corona discharge structure and the migration zone structure, so that the ions which are generated by the corona discharge structure can pass therethrough to reach the migration zone structure; and a redundant charge extraction circuit, wherein the redundant charge extraction electrode is connected to the ground through the redundant charge extraction circuit.

    Gas chromatograph-ion mobility spectrometer system
    76.
    发明授权
    Gas chromatograph-ion mobility spectrometer system 有权
    气相色谱 - 离子迁移谱系统

    公开(公告)号:US09513266B2

    公开(公告)日:2016-12-06

    申请号:US14577653

    申请日:2014-12-19

    CPC classification number: G01N30/7206 G01N27/622 G01N27/64 H01J49/0422

    Abstract: A GC-IMS system is disclosed. The system includes a sample transfer device. The sample transfer device connects the gas chromatograph to the reaction region and, the sample from the gas chromatograph is transferred to the reaction region by the sample transfer device. With the GC-IMS system, generation of sample molecular ion fragments can be avoided so that the spectrum is easily identified; moreover, the application field of the GC-IMS system is extended to a range of analysis of organic macromolecule samples which have a high polarity, are difficult to volatilize, and are thermally instable. On the other hand, the GC-IMS system overcomes the defect of ion destruction due to neutralization reaction among positive and negative ions so as to evade the detection.

    Abstract translation: 公开了一种GC-IMS系统。 该系统包括样品转移装置。 样品转移装置将气相色谱仪连接到反应区域,样品转移装置将样品从气相色谱仪转移到反应区域。 使用GC-IMS系统,可以避免样品分子离子片段的产生,从而可以容易地鉴定光谱; 此外,GC-IMS系统的应用领域扩展到具有高极性,难以挥发和热不稳定的有机大分子样品的分析范围。 另一方面,GC-IMS系统克服了由于正离子和负离子之间的中和反应引起的离子破坏的缺陷,以避免检测。

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