Abstract:
The present disclosure provides a gas chromatography-ion mobility spectrometry apparatus, including a housing, an injection port mounted to and connected with the housing and configured for input of a gas containing a sample therein, a multicapillary column configured for separation of a gas substance and an ion mobility tub configured for analysis of the gas substance. The gas chromatography-ion mobility spectrometry apparatus further includes: a gas path part connected with the ion mobility tube and configured for providing the gas to the ion mobility tube and receiving a gas discharged from the ion mobility tube; and a buffer base part detachably mounted to the housing and configured to isolation vibration outside the buffer base part, the ion mobility tube being disposed on the buffer base part, wherein the gas path part is mounted in an interior space of the buffer base part.
Abstract:
A sample introduction device comprises a sampling unit, a gas suction pump, adsorption units, a piston cylinder and a desorption cylinder that comprises a desorption chamber, a carrier-gas inlet, a split/purge vent and an analyzer nozzle communicating with the desorption chamber. A heating film and a temperature sensor are provided on outer wall of the desorption cylinder. The piston cylinder above the desorption cylinder comprises two piston chambers, each of which is provided with the adsorption unit and in communication with the desorption chamber. The piston cylinder comprises a sample-gas inlet connected to the sampling unit and a gas-suction-pump orifice connected to the gas suction pump, each of which can communicate with both piston chambers. Each adsorption unit comprises an adsorption cylinder-like screen for holding adsorbents and a piston rod slidably mounted in the piston chamber. Each adsorption cylinder-like screen can simultaneously communicate with the sample-gas inlet and gas-suction-pump orifice.
Abstract:
The present disclosure provides an ion mobility spectrometer, which comprises: a power supply circuit, configured to provide a power supply voltage; a corona discharge configured to generate ions to be subjected to measurement, through corona discharge; an ion migration circuit configured to control migration of the ions; a migration zone structure configured to realize, under control of the ion migration circuit, mobility spectrum measurement of the ions which pass through the migration zone structure; a redundant charge extraction electrode arranged between the corona discharge structure and the migration zone structure, so that the ions which are generated by the corona discharge structure can pass therethrough to reach the migration zone structure; and a redundant charge extraction circuit, wherein the redundant charge extraction electrode is connected to the ground through the redundant charge extraction circuit.
Abstract:
Inspection devices and inspection methods are disclosed. The inspection method includes: performing X-ray scanning on an object being inspected so as to generate an image of the object being inspected; dividing the image of the object being inspected to determine at least one region of interest; detecting interaction between a cosmic ray and the region of interest to obtain a detection value; calculating a scattering characteristic value and/or an absorption characteristic value of the cosmic ray in the region of interest based on size information of the region of interest and the detection value; and discriminating a material attribute of the region of interest by means of the scattering characteristic value and/or the absorption characteristic value. With the above technical solutions, inspection accuracy and inspection efficiency may be improved.
Abstract:
The present invention discloses a gas analyzing apparatus and a sampling device. The gas analyzing apparatus includes a sampling device and an ion mobility spectrum analysis device. The sampling device includes a multi-capillary column and a temperature control system. The ion mobility spectrum analysis device is adapted for analyzing a gas leaded-in by the sampling device and includes a reaction cavity for reaction between sample molecules and reaction ions, the cavity having a sampling opening for leading-in of the gas. An outlet end of the multi-capillary column is inserted directly into the cavity of the ion mobility spectrum analysis device through the sampling opening of the ion mobility spectrum analysis device.
Abstract:
A GC-IMS system is disclosed. The system includes a sample transfer device. The sample transfer device connects the gas chromatograph to the reaction region and, the sample from the gas chromatograph is transferred to the reaction region by the sample transfer device. With the GC-IMS system, generation of sample molecular ion fragments can be avoided so that the spectrum is easily identified; moreover, the application field of the GC-IMS system is extended to a range of analysis of organic macromolecule samples which have a high polarity, are difficult to volatilize, and are thermally instable. On the other hand, the GC-IMS system overcomes the defect of ion destruction due to neutralization reaction among positive and negative ions so as to evade the detection.
Abstract:
The present disclosure is directed to a rapid process for the preparation of gadolinium oxysulfide having a general formula of Gd2O2S, referred to as GOS, scintillation ceramics by using the combination of spark plasma primary sintering (SPS) and hot isostatic pressing secondary sintering.
Abstract translation:本公开涉及通过使用火花等离子体一次烧结(SPS)和热等静压二次烧结的组合制备具有通式Gd 2 O 2 S(称为GOS)闪烁陶瓷的通式Gd 2 O 2 S的快速方法。