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    Polyester mixture including polyethylene 2,5-furandicarboxylate
    1.
    发明授权
    Polyester mixture including polyethylene 2,5-furandicarboxylate 有权

    公开(公告)号：US10189989B2

    公开(公告)日：2019-01-29

    申请号：US15300317

    申请日：2015-03-23

    Applicant: BASF SE

    Inventor： Anna K. Moeller ,  Kian Molawi ,  Motonori Yamamoto

    IPC: C08L67/02

    Abstract: The present invention relates to a polyester mixture comprising: i) from 95 to 99.95% by weight, based on components i and ii, of a polyester selected from the group consisting of: polybutylene terephthalate, polycyclohexylenedimethylene 2,5-furandicarboxylate, polybutylene adipate-co-terephthalate, polybutylene sebacate-co-terephthalate, polybutylene succinate-co-terephthalate, polybutylene 2,5-furandicarboxylate-co-succinate, polybutylene 2,5-furandicarboxylate-co-adipate, polybutylene 2,5-furandicarboxylate-co-azelate, polybutylene 2,5-furandicarboxylate-co-sebacate, polybutylene 2,5-furandicarboxylate-co-brassylate, polybutylene 2,5-furandicarboxylate-co-1,18-C18-dicarboxylate, polybutylene succinate, polybutylene adipate, polybutylene succinate-co-adipate, polybutylene succinate-co-sebacate, polybutylene sebacate or mixtures of 2 or more of the polyesters mentioned, and ii) from 0.05 to 5% by weight, based on components i and ii, of polyethylene 2,5-furandicarboxylate.

    Method for the continuous production of biodegradable polyesters
    2.
    发明授权
    Method for the continuous production of biodegradable polyesters 有权
    连续生产可生物降解聚酯的方法

    公开(公告)号：US09040639B2

    公开(公告)日：2015-05-26

    申请号：US14082271

    申请日：2013-11-18

    Applicant: BASF SE

    Inventor： Uwe Witt ,  Motonori Yamamoto

    IPC: C08G63/00 ,  C08G63/181 ,  C08G63/60 ,  C08G18/42 ,  C08G18/73 ,  C08G63/16 ,  C08G63/20 ,  C08G63/78 ,  C08G63/127

    CPC classification number: C08G63/181 ,  C08G18/4219 ,  C08G18/4241 ,  C08G18/73 ,  C08G63/127 ,  C08G63/16 ,  C08G63/20 ,  C08G63/60 ,  C08G63/78 ,  C08G2230/00

    Abstract: A process for the continuous production of a biodegradable polyester, wherea mixture of aliphatic dihydroxy compounds, aliphatic and aromatic dicarboxylic acids or their liquid esters, and, optionally, further comonomers is mixed, without addition of a catalyst, to give a paste, and i) this mixture with at least a portion of the catalyst, is continuously esterified or, transesterified; ii) the transesterification or, esterification product obtained in i) is continuously precondensed with any remaining amount of catalyst to an intrinsic viscosity of from 20 to 70 cm3/g; iii) the product obtainable from ii) is continuously polycondensed to an intrinsic viscosity of from 60 to 170 cm3/g, and iv) the product obtainable from iii) is reacted continuously with a chain extender in a polyaddition reaction to an intrinsic viscosity of from 150 to 320 cm3/g. The invention further relates to biodegradable polyesters obtained_by this process.

    Abstract translation: 连续生产可生物降解的聚酯的方法，其中脂肪族二羟基化合物，脂族和芳族二羧酸或它们的液体酯的混合物，以及任选的其它共聚单体混合，不加入催化剂，得到糊状物，和 i）与至少一部分催化剂的该混合物连续酯化或酯交换; ii）在i）中获得的酯交换反应或酯化产物用任何剩余量的催化剂连续预缩合至特性粘度为20至70cm 3 / g; iii）从ii）获得的产品连续缩聚至特性粘度为60至170cm 3 / g，并且iv）将可从iii）获得的产品在加聚反应中与扩链剂连续反应，其特性粘度为 150〜320cm3 / g。 本发明还涉及通过该方法获得的生物可降解聚酯。

    Aliphatic Polyester
    5.
    发明申请
    Aliphatic Polyester 有权
    脂肪族聚酯

    公开(公告)号：US20130214455A1

    公开(公告)日：2013-08-22

    申请号：US13848961

    申请日：2013-03-22

    Applicant: BASF SE

    Inventor： Kai Oliver Siegenthaler ,  Andreas Füßl ,  Gabriel Skupin ,  Motonori Yamamoto

    IPC: C08G63/16

    CPC classification number: C08G63/16 ,  C08G63/20 ,  C08G63/916 ,  C08K3/01 ,  C08K3/013 ,  C08K5/0008 ,  C08K5/0016 ,  C08L67/00 ,  C08L67/02 ,  C08L67/04 ,  C08L69/00 ,  C08L2666/02 ,  C08L2666/18 ,  C08L2666/14

    Abstract: A copolymer obtained by condensation of i) 90 to 99.5 mol %, based on components i) to ii), of succinic acid; ii) 0.5 to 10 mol %, based on components i) to ii), of azelaic acid, sebacic acid and/or brassylic acid; iii) 98 to 102 mol %, based on components i) to ii), of 1,3-propanediol or 1,4 butanediol, and iv) 0.01% to 5% by weight, based on the total weight of the components i) to ii), of a chain extender and/or crosslinker selected from the group consisting of an at least trihydric alcohol or an at least tribasic carboxylic acid.

    Abstract translation: 通过i）90至99.5mol％的缩合得到的共聚物，基于组分i）至ii）琥珀酸; ii）基于组分i）至ii）的0.5至10mol％的壬二酸，癸二酸和/或丁酸; iii）基于组分i）至ii）的98至102摩尔％的1,3-丙二醇或1,4-丁二醇，和iv）基于组分i）的总重量为0.01重量％至5重量％ 至ii），选自至少三元醇或至少三元羧酸的扩链剂和/或交联剂。

    Polyester
    6.
    发明授权
    Polyester 有权

    公开(公告)号：US11597799B2

    公开(公告)日：2023-03-07

    申请号：US16609233

    申请日：2018-05-02

    Applicant: BASF SE

    Inventor： Michael Bernhard Schick ,  Motonori Yamamoto

    IPC: C08G63/688 ,  A61K8/85 ,  A61Q5/06 ,  C08G18/08 ,  C08G18/32 ,  C08G18/34 ,  C08G18/38 ,  C08G18/73 ,  C08G63/78 ,  C09J167/02

    Abstract: The present invention relates to a polyester consisting of (A) repeat units derived from an acid component, which consists of (a1) 2,5-furandicarboxylic acid, (a2) an aliphatic C4-C36 dicarboxylic acid or a mixture of a plurality of aliphatic C4-C36 dicarboxylic acids, and (a3) a sulfonate group-containing dicarboxylic acid, and of (B) repeat units derived from a di-ol/amine component, and optionally of further repeat units (C) and/or branching components (E), and of (D) repeat units derived from at least one di- or oligofunctional compound selected from the group consisting of a di- or oligoisocyanate and a di- or oligoisocyanurate. In addition, the present invention relates to the production of these polyesters and their use.

    Furandicarboxylic acid-containing polyesters
    7.
    发明授权
    Furandicarboxylic acid-containing polyesters 有权

    公开(公告)号：US11072683B2

    公开(公告)日：2021-07-27

    申请号：US16471807

    申请日：2017-11-24

    Applicant: BASF SE

    Inventor： Motonori Yamamoto ,  Michael Bernhard Schick

    IPC: C08G63/16

    Abstract: The invention relates to polyesters containing: A) an acid component composed of: a1) 25 to 100 mol % of 2,5-furandicarboxylic acid or its esters or mixtures thereof a2) 0 to 75 mol % of an aliphatic C4-C36-dicarboxylic acid or its esters or mixtures thereof and a3) 1 to 10 mol % of a sulfonate-containing compound, wherein the mol percentages of the components a1) to a3) sum to 100, and B) a diol component composed of: b1) 98 to 100 mol % based on the components a1) to a3) of component A of a C2- to C12-alkanediol or mixtures thereof and b2) 0 to 2 mol % based on the components a1) to a3) of a branching agent comprising at least 3 functional groups; and optionally further components. The invention further relates to the production of the polyesters and the use thereof and to aqueous dispersions and polyester mixtures comprising these polyesters.

    Aliphatic polyester
    10.
    发明授权
    Aliphatic polyester 有权
    脂肪族聚酯

    公开(公告)号：US09234073B2

    公开(公告)日：2016-01-12

    申请号：US13848961

    申请日：2013-03-22

    Applicant: BASF SE

    Inventor： Kai Oliver Siegenthaler ,  Andreas Füβl ,  Gabriel Skupin ,  Motonori Yamamoto

    IPC: B29C45/00 ,  C08G63/16 ,  C08G63/20 ,  C08G63/91 ,  C08L67/00 ,  C08K3/00 ,  C08K5/00 ,  C08L67/02 ,  C08L67/04 ,  C08L69/00

    CPC classification number: C08G63/16 ,  C08G63/20 ,  C08G63/916 ,  C08K3/01 ,  C08K3/013 ,  C08K5/0008 ,  C08K5/0016 ,  C08L67/00 ,  C08L67/02 ,  C08L67/04 ,  C08L69/00 ,  C08L2666/02 ,  C08L2666/18 ,  C08L2666/14

    Abstract: A method of producing a molded article involving preparing a copolymer obtained by condensation of (i) 90 to 99.5 mol %, based on components i) to ii), of succinic acid; (ii) 0.5 to 10 mol %, based on components i) to ii), of 4 to 10 mol % sebacic acid; (iii) 98 to 102 mol %, based on components i) to ii), of 1,3-propanediol or 1,4-butanediol; (iv) 0.05 to 0.5% by weight, based on the total weight of components i) to iii), of a crosslinker; and (v) 0.35 to 2% by weight, based on the total weight of components i) to iii), of 1,6-hexamethylene diisocyanate. The copolymer is injection molded or blow molded to form a molded article having a wall thickness above 200 μm.

    Abstract translation: 一种制备模制品的方法，包括制备通过（i）基于组分i）至ii）的90至99.5mol％的琥珀酸缩合得到的共聚物; （ii）基于组分i）至ii）的0.5至10mol％的4至10mol％癸二酸; （iii）基于组分i）至ii）的98至102摩尔％的1,3-丙二醇或1,4-丁二醇; （iv）0.05至0.5重量％，基于组分i）至iii）的交联剂的总重量; 和（v）0.35至2重量％，基于组分i）至iii）的1,6-六亚甲基二异氰酸酯的总重量。 共聚物被注射成型或吹塑成型，以形成壁厚在200μm以上的模塑制品。

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