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公开(公告)号：US20060292054A1
公开(公告)日：2006-12-28
申请号：US11159384
申请日：2005-06-23
申请人： Alexandra Chaumonnot , Aurelie Coupe , Clement Sanchez , Patrick Euzen , Cedric Boissiere , David Grosso
发明人： Alexandra Chaumonnot , Aurelie Coupe , Clement Sanchez , Patrick Euzen , Cedric Boissiere , David Grosso
IPC分类号： C01B33/26
CPC分类号： B01J35/0013 , B01J29/041 , B01J35/023 , B01J35/10 , B01J35/1023 , B01J37/0045 , C01B39/02
摘要： A mesostructured aluminosilicate material is described, constituted by at least two spherical elementary particles, each of said spherical particles being constituted by a matrix based on silicon oxide and aluminium oxide, having a pore size in the range 1.5 to 30 nm, a Si/Al molar ratio of at least 1, having amorphous walls with a thickness in the range 1 to 20 nm, said spherical elementary particles having a maximum diameter of 10 μm. A process for preparing said material and its application in the fields of refining and petrochemistry are also described.
摘要翻译： 描述了由至少两个球形基本粒子构成的介孔结构的硅铝酸盐材料，每个所述球形颗粒由基于氧化硅和氧化铝的基体构成，孔径在1.5至30nm的范围内，Si / Al 摩尔比至少为1，具有厚度在1至20nm范围内的非晶壁，所述球形基本颗粒的最大直径为10μm。 还描述了制备所述材料的方法及其在精炼和石油化学领域的应用。
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公开(公告)号：US20060030477A1
公开(公告)日：2006-02-09
申请号：US11165570
申请日：2005-06-24
申请人： Alexandra Chaumonnot , Aurelie Coupe , Clement Sanchez , Patrick Euzen , Cedric Boissiere , David Grosso
发明人： Alexandra Chaumonnot , Aurelie Coupe , Clement Sanchez , Patrick Euzen , Cedric Boissiere , David Grosso
CPC分类号： C01B37/02 , B01J29/005 , B01J29/0308 , B01J29/035 , B01J29/06 , B01J29/40 , B01J29/7003 , B01J37/0045 , B01J2229/62 , C01B39/04 , C01B39/40
摘要： A material with a hierarchical porosity is described, constituted by at least two spherical elementary particles, each of said spherical particles comprising zeolitic nanocrystals having a pore size in the range 0.2 to 2 nm and a matrix based on silicon oxide, which is mesostructured, having a pore size in the range 1.5 to 30 nm and having amorphous walls with a thickness in the range 1 to 20 nm, said spherical elementary particles having a maximum diameter of 10 μm. the matrix based on silicon oxide may contain aluminium. The preparation of said material is also described.
摘要翻译： 描述具有分层孔隙率的材料，由至少两个球形基本粒子构成，每个所述球形颗粒包含孔径在0.2至2nm范围内的沸石纳米晶体和基于氧化硅的基体，其被介孔结构化，具有 孔径在1.5至30nm的范围内，并且具有厚度在1至20nm范围内的非晶壁，所述球形基本粒子的最大直径为10μm。 基于氧化硅的基体可以含有铝。 还描述了所述材料的制备。
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公开(公告)号：US07807598B2
公开(公告)日：2010-10-05
申请号：US11889891
申请日：2007-08-17
申请人： Patrick Euzen , Alexandra Chaumonnot , Aurelie Coupe , Clement Sanchez , Cedric Boissiere , David Grosso
发明人： Patrick Euzen , Alexandra Chaumonnot , Aurelie Coupe , Clement Sanchez , Cedric Boissiere , David Grosso
IPC分类号： B01J29/06
CPC分类号： C01B39/04 , B01J20/08 , B01J20/16 , B01J20/18 , B01J20/28007 , B01J20/28083 , B01J29/041 , B01J29/08 , B01J29/40 , B01J29/60 , B01J29/7007 , B01J29/80 , B01J2229/62 , B82Y30/00 , C01B39/48
摘要： A mesostructured material that consists of at least two elementary spherical particles, each of said particles comprising a mesostructured matrix based on aluminum oxide and having a pore size of between 1.5 and 30 nm, an aluminum oxide content that represents more than 46% by weight relative to the mass of said matrix, which has amorphous walls with a thickness of between 1 and 30 nm and whereby said elementary spherical particles have a maximum diameter of 10 μm, is described. Said mesostructured matrix can also contain silicon oxide. Each of the spherical particles of the mesostructured material can also contain zeolitic nanocrystals so as to form a material with a mixed porosity that is both mesostructured and zeolitic in nature. The preparation of said material is also described.
摘要翻译： 由至少两个基本球形颗粒组成的介孔结构材料，每个所述颗粒包含基于氧化铝的孔结构基质，孔径在1.5至30nm之间，氧化铝含量相对于46重量％ 相对于具有1〜30nm厚度的非晶壁的所述基体的质量，并且由此所述基本球形颗粒的最大直径为10μm。 所述介孔结构的基质也可以含有氧化硅。 介孔结构材料的每个球形颗粒也可以含有沸石纳米晶体，以便形成具有混合孔隙率的材料，其本质上是介孔结构和沸石。 还描述了所述材料的制备。
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14.发明申请PROCESS FOR PREPARING A SPHERICAL MATERIAL WITH A HIERARCHICAL POROSITY COMPRISING METALLIC PARTICLES TRAPPED IN A MESOSTRUCTURED MATRIX 有权用于制备具有包含在结构化矩阵中捕获的金属颗粒的分层孔隙的球形材料的方法公开(公告)号：US20140021096A1
公开(公告)日：2014-01-23
申请号：US13995548
申请日：2011-12-15
申请人： Alexandra Chaumonnot , Clement Sanchez , Cedric Boissiere , Frederic Colbeau-Justin , Audrey Bonduelle
发明人： Alexandra Chaumonnot , Clement Sanchez , Cedric Boissiere , Frederic Colbeau-Justin , Audrey Bonduelle
IPC分类号： B29C65/00
CPC分类号： B29C66/727 , B01J27/186 , B01J27/188 , B01J27/19 , B01J29/005 , B01J29/0333 , B01J29/0341 , B01J29/041 , B01J29/044 , B01J29/045 , B01J29/08 , B01J29/40 , B01J29/46 , B01J29/48 , B01J29/7007 , B01J35/002 , B01J35/006 , B01J35/023 , B01J35/1019 , B01J35/1042 , B01J35/1057 , B01J35/1061 , B01J37/0045 , B01J37/033 , B01J37/10 , B01J37/20 , C01B37/02 , C01B39/06 , C01B39/40 , C10G49/04 , C10G49/08 , Y02P30/20
摘要： A process is described for the preparation of an inorganic material with a hierarchical porosity in the micropore and mesopore domains. The material has at least two elementary spherical particles having a maximum diameter of 200 microns. The process comprises: a) preparing a solution containing zeolitic nanocrystals with a maximum nanometric dimension equal to 60 nm based on silicon and/or precursor elements of proto-zeolitic entities based on silicon; b) mixing, in solution, metallic particles or at least one metallic precursor of metallic particles, a surfactant and the solution obtained in accordance with a) such that the ratio of the volumes of inorganic and organic materials, Vinorganic/Vorganic, is 0.29 to 0.50; c) aerosol atomization of the solution obtained in b) resulting in formation of spherical droplets; d) drying the droplets; g) eliminating the template and surfactant.
摘要翻译： 描述了在微孔和中孔域中具有分级孔隙率的无机材料的制备方法。 该材料具有至少两个最大直径为200微米的基本球形颗粒。 该方法包括：a）基于硅原子沸石实体的硅和/或前体元素，制备含有最大纳米尺寸等于60nm的沸石纳米晶体的溶液; b）在溶液中混合金属颗粒或金属颗粒的至少一种金属前体，表面活性剂和根据a）获得的溶液，使得无机和有机材料Vinorganic / Vorganic的体积比为0.29至 0.50; c）在b）中获得的溶液的气溶胶雾化导致球形液滴的形成; d）干燥液滴; g）消除模板和表面活性剂。
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15.发明授权Mesostructured aluminosilicate material made of spherical particles of specific size 有权由具有特定尺寸的球形颗粒制成的中等结构的硅铝酸盐材料公开(公告)号：US08563135B2
公开(公告)日：2013-10-22
申请号：US12935335
申请日：2009-02-26
CPC分类号： C01B39/04 , B01J20/18 , B01J20/28004 , B01J20/28019 , B01J20/28057 , B01J20/28083 , B01J21/12 , B01J29/041 , B01J35/1057 , B01J35/1061 , B01J35/109 , Y10T428/2991 , Y10T428/2993
摘要： A mesostructured aluminosilicate material is described, which consists of at least two elementary spherical particles, each one of said spherical particles consisting of a matrix based on silicon oxide and aluminium oxide, said matrix having a pore diameter ranging between 1.5 and 30 nm, a Si/Al molar ratio at least equal to 1 and amorphous walls of thickness ranging between 1 and 30 nm, said elementary spherical particles having a diameter D such that 10
摘要翻译： 描述了介质结构的硅铝酸盐材料，其由至少两个基本球形颗粒组成，每个所述球形颗粒由基于氧化硅和氧化铝的基体组成，所述基体的孔径范围为1.5至30nm，Si / Al摩尔比至少等于1，厚度范围在1至30nm之间的无定形壁，所述基本球形颗粒的直径D使得10（D）（mum）@ 100。 还描述了制备所述材料及其在精炼和石油化学领域中的应用的方法。
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公开(公告)号：US20110039102A1
公开(公告)日：2011-02-17
申请号：US12676707
申请日：2008-08-18
IPC分类号： C01B37/02 , C01B39/40 , C01B37/00 , C01B33/113
CPC分类号： C01B39/00 , B01J20/0288 , B01J20/18 , B01J20/28019 , B01J20/28057 , B01J20/2808 , B01J20/28083 , B01J20/28085 , B01J20/28092 , B01J21/08 , B01J21/12 , B01J29/035 , B01J29/08 , B01J29/40 , B01J29/7007 , B01J35/1061 , B01J35/1066 , B01J35/109 , B01J37/0045 , B01J37/033 , C01B37/00 , C01B37/02 , C07C4/18 , Y02P20/52 , Y10T428/2982 , C07C15/04 , C07C11/06
摘要： Material with hierarchical porosity consisting of at least two elementary spherical particles having a maximum diameter of 200 microns, at least one of said spherical particles comprising at least one matrix based on silicon oxide, said material having a macropore volume measured by mercury porosimetry ranging between 0.05 and 1 ml/g, a mesopore volume measured by nitrogen volumetric analysis ranging between 0.01 and 1 ml/g and a micropore volume measured by nitrogen volumetric analysis ranging between 0.03 and 0.4 ml/g, said matrix having amorphous walls. The preparation of said material is also described.
摘要翻译： 具有分层孔隙率的材料，其由至少两个最大直径为200微米的基本球形颗粒组成，所述球形颗粒中的至少一种包含至少一种基于氧化硅的基体，所述材料具有通过水银孔率测定法测量的大孔体积为0.05 和1ml / g，通过氮体积分析测量的介孔体积在0.01至1ml / g之间，通过氮容积分析测量的微孔体积在0.03至0.4ml / g之间，所述基质具有无定形壁。 还描述了所述材料的制备。
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17.发明申请SPHERICAL MATERIAL BASED ON HETEROPOLYANIONS TRAPPED IN A MESOSTRUCTURED OXIDE MATRIX AND USE THEREOF AS CATALYST IN HYDROCARBON REFINING PROCESSES 审中-公开基于在结构化氧化物基质中捕获的异黄酮的球形材料及其作为烃类精炼工艺中的催化剂的用途公开(公告)号：US20140005031A1
公开(公告)日：2014-01-02
申请号：US13995508
申请日：2011-12-15
申请人： Alexandra Chaumonnot , Clement Sanchez , Cedric Boissiere , Frederic Colbeau-Justin , Karin Marchand , Elodie Devers , Audrey Bonduelle , Denis Uzio , Antoine Daudin , Bertrand Guichard , Denis Uzio , Antoine Daudin
发明人： Alexandra Chaumonnot , Clement Sanchez , Cedric Boissiere , Frederic Colbeau-Justin , Karin Marchand , Elodie Devers , Audrey Bonduelle , Denis Uzio , Antoine Daudin , Bertrand Guichard , Denis Uzio , Antoine Daudin
IPC分类号： B01J27/199 , B01J27/19 , B01J27/188 , B01J23/882
CPC分类号： B01J27/199 , B01J23/882 , B01J27/186 , B01J27/188 , B01J27/19 , B01J29/0333 , B01J29/0341 , B01J29/041 , B01J29/044 , B01J29/045 , B01J35/002 , B01J35/006 , B01J35/023 , B01J35/1019 , B01J35/1042 , B01J35/1057 , B01J35/1061 , B01J37/0045 , B01J37/033 , B01J37/10 , B01J37/20 , C01B37/00 , C01B37/005 , C01B37/02 , C01B39/04 , C01B39/06 , C10G3/45 , C10G3/46 , C10G3/48 , C10G3/49 , C10G3/50 , C10G45/06 , C10G47/12 , C10G2300/1011 , C10G2300/104 , C10G2300/1044 , C10G2300/1055 , C10G2300/202 , C10G2300/301 , C10G2400/02 , C10G2400/04 , C10G2400/06 , C10L1/04 , C10L1/06 , C10L1/08 , Y02P30/10 , Y02P30/20
摘要： Inorganic material having at least two elementary spherical particles, each of said spherical metallic particles: a polyoxometallate with formula (XxMmOyHh)q−, where H is hydrogen, O is oxygen, X is phosphorus, silicon, boron, nickel or cobalt and M is one or more vanadium, niobium, tantalum, molybdenum, tungsten, iron, copper, zinc, cobalt and nickel, x is 0, 1, 2 or 4, m is 5, 6, 7, 8, 9, 10, 11, 12 or 18, y is 17 to 72, h is 0 to 12 and q is 1 to 20.
摘要翻译： 具有至少两个基本球形颗粒的无机材料，每个所述球形金属颗粒：具有式（XxMmOyHh）q-的多金属氧酸盐，其中H是氢，O是氧，X是磷，硅，硼，镍或钴，M是 一种或多种钒，铌，钽，钼，钨，铁，铜，锌，钴和镍，x为0,1,2或4，m为5,6,7,8,9,10,11,12 或18，y为17〜72，h为0〜12，q为1〜20。
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18.发明申请MESOSTRUCTURED ALUMINOSILICATE MATERIAL MADE OF SPHERICAL PARTICLES OF SPECIFIC SIZE 有权特殊尺寸的球形颗粒的结构化铝氧化物材料公开(公告)号：US20110105300A1
公开(公告)日：2011-05-05
申请号：US12935335
申请日：2009-02-26
CPC分类号： C01B39/04 , B01J20/18 , B01J20/28004 , B01J20/28019 , B01J20/28057 , B01J20/28083 , B01J21/12 , B01J29/041 , B01J35/1057 , B01J35/1061 , B01J35/109 , Y10T428/2991 , Y10T428/2993
摘要： A mesostructured aluminosilicate material is described, which consists of at least two elementary spherical particles, each one of said spherical particles consisting of a matrix based on silicon oxide and aluminium oxide, said matrix having a pore diameter ranging between 1.5 and 30 nm, a Si/Al molar ratio at least equal to 1 and amorphous walls of thickness ranging between 1 and 30 nm, said elementary spherical particles having a diameter D such that 10
摘要翻译： 描述了介质结构的硅铝酸盐材料，其由至少两个基本球形颗粒组成，每个所述球形颗粒由基于氧化硅和氧化铝的基体组成，所述基体的孔径范围为1.5至30nm，Si / Al摩尔比至少等于1，厚度范围在1至30nm之间的非晶壁，所述基本球形颗粒的直径D使得10
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公开(公告)号：US09656421B2
公开(公告)日：2017-05-23
申请号：US13995548
申请日：2011-12-15
申请人： Alexandra Chaumonnot , Clement Sanchez , Cedric Boissiere , Frederic Colbeau-Justin , Audrey Bonduelle
发明人： Alexandra Chaumonnot , Clement Sanchez , Cedric Boissiere , Frederic Colbeau-Justin , Audrey Bonduelle
IPC分类号： B01J29/035 , B29C65/00 , B01J27/186 , B01J27/188 , B01J27/19 , B01J29/00 , B01J29/03 , B01J29/04 , B01J29/46 , B01J29/48 , B01J35/00 , B01J35/02 , B01J35/10 , B01J37/00 , B01J37/03 , B01J37/10 , B01J37/20 , C10G49/04 , C10G49/08 , C01B37/02 , C01B39/06 , C01B39/40 , B01J29/08 , B01J29/40 , B01J29/70
CPC分类号： B29C66/727 , B01J27/186 , B01J27/188 , B01J27/19 , B01J29/005 , B01J29/0333 , B01J29/0341 , B01J29/041 , B01J29/044 , B01J29/045 , B01J29/08 , B01J29/40 , B01J29/46 , B01J29/48 , B01J29/7007 , B01J35/002 , B01J35/006 , B01J35/023 , B01J35/1019 , B01J35/1042 , B01J35/1057 , B01J35/1061 , B01J37/0045 , B01J37/033 , B01J37/10 , B01J37/20 , C01B37/02 , C01B39/06 , C01B39/40 , C10G49/04 , C10G49/08 , Y02P30/20
摘要： A process is described for the preparation of an inorganic material with a hierarchical porosity in the micropore and mesopore domains. The material has at least two elementary spherical particles having a maximum diameter of 200 microns. The process comprises: a) preparing a solution containing zeolitic nanocrystals with a maximum nanometric dimension equal to 60 nm based on silicon and/or precursor elements of proto-zeolitic entities based on silicon; b) mixing, in solution, metallic particles or at least one metallic precursor of metallic particles, a surfactant and the solution obtained in accordance with a) such that the ratio of the volumes of inorganic and organic materials, Vinorganic/Vorganic, is 0.29 to 0.50; c) aerosol atomization of the solution obtained in b) resulting in formation of spherical particles; d) drying the particles; g) eliminating any remaining precursor elements of proto-zeolitic entities based on silicon and the surfactant.
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公开(公告)号：US08685366B2
公开(公告)日：2014-04-01
申请号：US12676696
申请日：2008-08-29
CPC分类号： C01B37/00 , B01J20/18 , B01J20/28019 , B01J20/28057 , B01J20/2808 , B01J20/28083 , B01J20/28085 , B01J21/08 , B01J21/12 , B01J29/035 , B01J29/084 , B01J29/40 , B01J29/7007 , B01J35/1057 , B01J35/1061 , B01J35/1066 , B01J35/1095 , B01J37/0045 , B01J37/10 , C01B37/02 , C01B39/00
摘要： Hierarchical porosity material consisting of at least two elementary spherical particles having a maximum diameter of 200 microns, at least one of said spherical particles comprises at least one matrix based on silicon oxide and exhibiting crystallized walls, said material having a macropore volume measured by mercury porosimetry ranging between 0.05 and 1 ml/g, a mesopore volume measured by nitrogen volumetric analysis ranging between 0.01 and 1 ml/g and a micropore volume measured by nitrogen volumetric analysis ranging between 0.03 and 0.4 ml/g. The preparation of said material and use of same as adsorbent or as acidic solid is also described.
摘要翻译： 由至少两个最大直径为200微米的基本球形颗粒组成的分级孔隙率材料，所述球形颗粒中的至少一种包括至少一种基于氧化硅的基质并显示结晶的壁，所述材料具有通过水银孔率法测量的大孔体积 范围在0.05和1ml / g之间，通过氮容积分析测量的介孔体积在0.01和1ml / g之间，通过氮容积分析测量的微孔体积在0.03至0.4ml / g之间。 还描述了所述材料的制备及其与吸附剂或酸性固体的用途。
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