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    Method for production of carbon nanotube
    11.
    发明授权
    Method for production of carbon nanotube 有权
    碳纳米管生产方法

    公开(公告)号：US08518363B2

    公开(公告)日：2013-08-27

    申请号：US12440317

    申请日：2007-09-07

    申请人： Suguru Noda ,  Hisashi Sugime ,  Yukio Yamaguchi

    发明人： Suguru Noda ,  Hisashi Sugime ,  Yukio Yamaguchi

    IPC分类号： D01C5/00

    CPC分类号： B01J38/12 ,  B01J23/745 ,  B01J23/881 ,  B01J23/882 ,  B01J23/94 ,  B01J35/04 ,  B01J37/347 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/162 ,  C01B32/17 ,  C01B2202/02 ,  Y02P20/584

    摘要： [Problems to be Solved]There is provided a method for production of a carbon nanotube, which allows for production of the carbon nanotube in a large scale and at a low cost.[Solution]The temperature of a catalyst loaded on a support is raised by heating the support and a raw material gas containing a carbon source is supplied on the catalyst to synthesize the carbon nanotube. The synthesized carbon nanotube is recovered, and after the recovery, the catalyst is subjected to a regeneration treatment to repeatedly utilize the support. Since the catalyst deteriorates, the catalyst is regenerated periodically or nonperiodically during the production. The regeneration treatment of the catalyst involves an oxidation treatment of the catalyst. Further, after the oxidation treatment, a reducing gas is fed to and brought into contact with the catalyst surface to reduce the catalyst. As the support, a honeycomb is used.

    摘要翻译： [待解决的问题]提供了一种生产碳纳米管的方法，其可以大规模和低成本地生产碳纳米管。 [解决方案]通过加热载体来提高负载在载体上的催化剂的温度，并在催化剂上提供含有碳源的原料气体以合成碳纳米管。 回收合成的碳纳米管，回收后，对催化剂进行再生处理，反复利用载体。 由于催化剂劣化，催化剂在生产过程中周期性或非周期性地再生。 催化剂的再生处理涉及催化剂的氧化处理。 此外，在氧化处理之后，还原气体被供给到催化剂表面并与催化剂表面接触以还原催化剂。 作为支撑体，使用蜂窝体。

    Method for forming a catalyst suitable for growth of carbon nanotubes
    15.
    发明授权
    Method for forming a catalyst suitable for growth of carbon nanotubes 有权
    形成适合碳纳米管生长的催化剂的方法

    公开(公告)号：US08338296B2

    公开(公告)日：2012-12-25

    申请号：US13096310

    申请日：2011-04-28

    申请人： Hari Pathangi Sriraman ,  Ann Witvrouw ,  Philippe M. Vereecken

    发明人： Hari Pathangi Sriraman ,  Ann Witvrouw ,  Philippe M. Vereecken

    IPC分类号： H01L21/441

    CPC分类号： B01J23/74 ,  B01J23/755 ,  B01J35/0013 ,  B01J37/347 ,  B01J37/348 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/162 ,  H01L29/0673

    摘要： The present disclosure is related to a method for forming a catalyst nanoparticle on a metal surface, the nanoparticle being suitable for growing a single nanostructure, in particular a carbon nanotube, the method comprising at least the steps of: providing a substrate, having a metal layer on at least a portion of the substrate surface, depositing a sacrificial layer at least on the metal layer, producing a small hole in the sacrificial layer, thereby exposing the metal layer, providing a single catalyst nanoparticle into the hole, removing the sacrificial layer. The disclosure is further related to growing a carbon nanotube from the catalyst nanoparticle.

    摘要翻译： 本公开涉及在金属表面上形成催化剂纳米颗粒的方法，所述纳米颗粒适于生长单个纳米结构，特别是碳纳米管，所述方法至少包括以下步骤：提供具有金属的基材 在衬底表面的至少一部分上层叠，至少在金属层上沉积牺牲层，在牺牲层中产生小孔，由此暴露金属层，向单孔提供单个催化剂纳米颗粒，去除牺牲层 。 本公开还涉及从催化剂纳米颗粒生长碳纳米管。

    METHOD FOR FORMING A CATALYST SUITABLE FOR GROWTH OF CARBON NANOTUBES
    19.
    发明申请
    METHOD FOR FORMING A CATALYST SUITABLE FOR GROWTH OF CARBON NANOTUBES 有权
    形成适用于碳纳米管生长的催化剂的方法

    公开(公告)号：US20110315951A1

    公开(公告)日：2011-12-29

    申请号：US13096310

    申请日：2011-04-28

    申请人： Hari Pathangi Sriraman ,  Ann Witvrouw ,  Philippe M. Vereecken

    发明人： Hari Pathangi Sriraman ,  Ann Witvrouw ,  Philippe M. Vereecken

    IPC分类号： H01L29/66 ,  H01L21/20 ,  B05D5/12 ,  C25D15/00 ,  B82Y30/00 ,  B82Y40/00

    CPC分类号： B01J23/74 ,  B01J23/755 ,  B01J35/0013 ,  B01J37/347 ,  B01J37/348 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/162 ,  H01L29/0673

    摘要： The present disclosure is related to a method for forming a catalyst nanoparticle on a metal surface, the nanoparticle being suitable for growing a single nanostructure, in particular a carbon nanotube, the method comprising at least the steps of: providing a substrate, having a metal layer on at least a portion of the substrate surface, depositing a sacrificial layer at least on the metal layer, producing a small hole in the sacrificial layer, thereby exposing the metal layer, providing a single catalyst nanoparticle into the hole, removing the sacrificial layer. The disclosure is further related to growing a carbon nanotube from the catalyst nanoparticle.

    摘要翻译： 本公开涉及在金属表面上形成催化剂纳米颗粒的方法，所述纳米颗粒适于生长单个纳米结构，特别是碳纳米管，所述方法至少包括以下步骤：提供具有金属的基材 在衬底表面的至少一部分上层叠，至少在金属层上沉积牺牲层，在牺牲层中产生小孔，由此暴露金属层，向单孔提供单个催化剂纳米颗粒，去除牺牲层 。 本公开还涉及从催化剂纳米颗粒生长碳纳米管。