公开(公告)号：US08455690B2

公开(公告)日：2013-06-04

申请号：US12532945

申请日：2008-03-27

Applicant: Yasumasa Takenaka ,  Jun-Chul Choi ,  Toshiyasu Sakakura ,  Hiroyuki Yasuda ,  Takahiro Kiyosu

Inventor： Yasumasa Takenaka ,  Jun-Chul Choi ,  Toshiyasu Sakakura ,  Hiroyuki Yasuda ,  Takahiro Kiyosu

IPC: C07C239/00

CPC classification number: B01J31/1625 ,  B01J31/1608 ,  B01J2231/64 ,  B01J2531/828 ,  C07C239/08 ,  C07C239/10 ,  C07C239/12

Abstract: The invention provides a method for producing an arylhydroxylamine compound efficiently and safely under mild conditions. The method involves contacting a nitroaryl compound with a hydrogen source in the presence of a platinum catalyst supported on amino group-coordinated silica and a poisoning agent.

Abstract translation: 本发明提供了一种在温和条件下有效安全地生产芳基羟胺化合物的方法。 该方法包括在负载在氨基配位二氧化硅和中毒剂上的铂催化剂存在下使硝基芳基化合物与氢源接触。

公开(公告)号：US20060106254A1

公开(公告)日：2006-05-18

申请号：US10545073

申请日：2004-01-22

Applicant: Mutsumi Sato ,  Keiji Oono

Inventor： Mutsumi Sato ,  Keiji Oono

IPC: B01J31/00 ,  C07C239/00

CPC classification number: B01J31/10 ,  B01J23/42 ,  B01J31/0238 ,  B01J31/0239 ,  B01J31/08 ,  B01J31/30 ,  B01J31/4038 ,  B01J2231/641 ,  B01J2531/828 ,  C07C239/08 ,  Y02P20/584

Abstract: The present invention discloses a method for producing a hydroxylamine compound wherein a nitro compound is contacted with a hydrogen source or further with a poisoning agent in the presence of a platinum catalyst fixed on an ion-exchange resin. According to the method of the present invention where a platinum catalyst fixed on a matrix of an ion-exchange resin is used, the objective hydroxylamine compound can be produced (manufactured) efficiently, more industrially and safely with little formation of a byproduct. Further, the platinum catalyst fixed on an ion-exchange resin of the present invention is hardly deactivated even if repeatedly used many times because platinum metal is fixed on a matrix of the ion-exchange resin, and handling in recovery, reuse and the like of said catalyst is extremely easy because particle size of said catalyst is very large.

公开(公告)号：US06967181B2

公开(公告)日：2005-11-22

申请号：US10301607

申请日：2002-11-22

Applicant: Ulrich Müller ,  Hartwig Voss ,  Erich Schubert ,  Friedrich Hill ,  Hermann Petersen

Inventor： Ulrich Müller ,  Hartwig Voss ,  Erich Schubert ,  Friedrich Hill ,  Hermann Petersen

IPC: B01J29/04 ,  B01J29/06 ,  B01J29/89 ,  C01B21/14 ,  C01B39/02 ,  C07B41/02 ,  C07C239/08 ,  C07C249/04 ,  C07C249/08 ,  C07D301/12

CPC classification number: C01B21/1409 ,  B01J29/04 ,  B01J29/06 ,  B01J29/89 ,  C01B39/026 ,  C07C239/08 ,  C07C249/04 ,  C07D301/12

Abstract: In a process for concentrating an at least partially crystalline solid containing at least one zeolite in a mixture comprising at least one auxiliary, for example a template compound, and said solid, the mixture is ultrafiltrated in a step (II) to divide the mixture into a retentate and a permeate, the solids content in the retentate being higher than that in the mixture and the solids content in the permeate being lower than that in the mixture. This procedure allows auxiliaries, in particular template compounds, present in the permeate to be recycled into a crystallizing step (I) upstream of step (II).

Abstract translation: 在将包含至少一种沸石的至少部分结晶的固体在包含至少一种助剂例如模板化合物和所述固体的混合物中浓缩的方法中，在步骤（II）中将混合物超滤以将混合物分成 渗余物和渗透物，渗余物中的固体含量高于混合物中的固体含量，并且渗透物中的固体含量低于混合物中的固体含量。 该方法允许存在于渗透物中的助剂，特别是模板化合物再循环到步骤（II）上游的结晶步骤（I）中。

公开(公告)号：US06133409A

公开(公告)日：2000-10-17

申请号：US103872

申请日：1998-06-24

Applicant: Joseph M. Salvino ,  George C. Morton ,  Helen J. Mason ,  Richard F. Labaudiniere

Inventor： Joseph M. Salvino ,  George C. Morton ,  Helen J. Mason ,  Richard F. Labaudiniere

IPC: C07C45/61 ,  C07C45/00 ,  C07C45/41 ,  C07C45/45 ,  C07C45/51 ,  C07C45/65 ,  C07C47/228 ,  C07C47/277 ,  C07C47/546 ,  C07C47/55 ,  C07C49/213 ,  C07C49/807 ,  C07C51/353 ,  C07C57/42 ,  C07C209/00 ,  C07C209/30 ,  C07C209/40 ,  C07C209/42 ,  C07C209/66 ,  C07C211/03 ,  C07C231/10 ,  C07C231/12 ,  C07C233/33 ,  C07C233/87 ,  C07C239/08 ,  C07C239/20 ,  C07C249/08 ,  C07C251/54 ,  C07C259/06 ,  C07C259/08 ,  C07C259/10 ,  C07C269/06 ,  C07C271/18 ,  C07C315/04 ,  C07C317/44 ,  C07C317/46 ,  C07D307/33 ,  C07D311/68 ,  C07D311/82 ,  C07D313/12 ,  C08F8/00 ,  C08F12/26 ,  C40B40/14 ,  C40B50/00 ,  G01N24/00 ,  C08G63/44 ,  C07C45/55 ,  C07L49/115

CPC classification number: C07D307/33 ,  C07C209/00 ,  C07C209/40 ,  C07C209/42 ,  C07C209/66 ,  C07C239/08 ,  C07C259/06 ,  C07C259/08 ,  C07C259/10 ,  C07C315/04 ,  C07C45/00 ,  C07C45/004 ,  C07C45/41 ,  C07C45/45 ,  C07C45/516 ,  C07C51/09 ,  C07D311/68 ,  C07D311/82 ,  C07D313/12 ,  C08F8/00 ,  C08F8/30 ,  C08J7/12 ,  G01N24/00 ,  C07B2200/11 ,  C08F2810/30

Abstract: This invention is directed to a process for the solid phase synthesis of aldehyde, ketone, oxime, amine, hydroxamic acid and .alpha.,.beta.-unsaturated carboxylic acid and aldehyde compounds and to polymeric hydroxylamine resin compounds useful therefor.

Abstract translation: 本发明涉及醛，酮，肟，胺，异羟肟酸和α，β-不饱和羧酸和醛化合物的固相合成方法，以及可用于其的聚合羟胺树脂化合物的方法。

公开(公告)号：US6024855A

公开(公告)日：2000-02-15

申请号：US133851

申请日：1998-08-13

Applicant: Hossein Sharifian ,  John H. Wagonknecht

Inventor： Hossein Sharifian ,  John H. Wagonknecht

IPC: B01D61/44 ,  B01D61/52 ,  B01J37/34 ,  C07C239/08 ,  C25B20060101 ,  C25B1/00 ,  C25B11/04

CPC classification number: B01D61/44 ,  B01D61/445 ,  B01D61/52 ,  B01J37/348 ,  C07C239/08 ,  C25B1/00 ,  C25B11/0442

Abstract: In one embodiment, the present invention relates to a method of preparing a hydroxylammonium salt, involving the steps of: providing an electrochemical cell containing an anode, a cathode, and a divider positioned between the anode and the cathode, to define a catholyte compartment between the cathode and the divider and an anolyte compartment between the anode and the divider; charging the catholyte compartment with a first solution comprising a nitrogen containing compound and a mediator and the anolyte compartment with a second solution comprising an ionic compound; passing a current through the electrochemical cell to produce a hydroxylammonium salt in the catholyte compartment; and recovering the hydroxylammonium salt from the catholyte compartment. In another embodiment, the present invention relates to a method of preparing hydroxylamine, involving the steps of: providing an electrochemical cell containing an anode, a cathode and a divider positioned between the cathode and the anode, to define a catholyte compartment between the cathode and the divider, and an anolyte compartment between the divider and the anode; charging the catholyte compartment with a solution comprising a hydroxylammonium salt and a mediator, and the anolyte compartment with a first electrolyte solution; passing a current through the electrochemical cell to produce hydroxylamine in the catholyte compartment; and recovering hydroxylamine from the catholyte compartment.

Abstract translation: 在一个实施方案中，本发明涉及一种制备羟基铵盐的方法，其包括以下步骤：提供包含位于阳极和阴极之间的阳极，阴极和分隔体的电化学电池，以在阴极和阴极之间限定阴极电解液室， 阴极和分隔器以及在阳极和分隔器之间的阳极电解液室; 用包含含氮化合物和介体的第一溶液和所述阳极电解液室与含有离子化合物的第二溶液对所述阴极电解液室进行充电; 使电流通过电化学电池以在阴极电解液室中产生羟基铵盐; 并从阴极电解液室回收羟基铵盐。 在另一个实施方案中，本发明涉及一种制备羟胺的方法，包括以下步骤：提供包含阳极，阴极和位于阴极和阳极之间的分隔体的电化学电池，以在阴极和阴极之间限定阴极电解液室， 分隔器和分隔器和阳极之间的阳极电解液室; 用包含羟基铵盐和介体的溶液对阴极电解液室进行充电，和阳极电解液室用第一电解质溶液充电; 使电流通过电化学电池以在阴极电解液室中产生羟胺; 并从阴极电解液室回收羟胺。

公开(公告)号：US5830568A

公开(公告)日：1998-11-03

申请号：US588963

申请日：1996-01-19

Applicant: Takeshi Kondo

Inventor： Takeshi Kondo

IPC: E06B5/00 ,  B01D61/44 ,  B01D61/52 ,  B01J37/34 ,  B32B17/10 ,  B60J1/00 ,  C03C17/00 ,  C03C17/34 ,  C03C27/12 ,  C07C239/08 ,  C25B1/00 ,  C25B11/04 ,  B32B5/16

CPC classification number: B32B17/10788 ,  B01D61/44 ,  B01D61/445 ,  B01D61/52 ,  B01J37/348 ,  B32B17/10036 ,  B32B17/10587 ,  B32B17/10605 ,  B32B17/10633 ,  B32B17/10688 ,  B32B17/10761 ,  B32B17/10853 ,  C03C17/009 ,  C03C17/34 ,  C07C239/08 ,  C25B1/00 ,  C25B11/0442 ,  C03C2217/445 ,  C03C2217/475 ,  C03C2217/476 ,  Y10T428/25 ,  Y10T428/252 ,  Y10T428/256 ,  Y10T428/257 ,  Y10T428/259 ,  Y10T428/2998 ,  Y10T428/31623 ,  Y10T428/31627 ,  Y10T428/3163 ,  Y10T428/31645 ,  Y10T428/31649

Abstract: The invention provides a laminated glass and a method of producing the same. This laminated glass includes first and second transparent glass plates and an interlayer film interposed therebetween. This interlayer film has functional ultra-fine particles which have a particle diameter of up to 0.2 .mu.m and are dispersed therein. Due to the incorporation of the ultra-fine particles thereinto, the interlayer film is provided with various additional functions such as heat insulation, ultraviolet ray absorption and the maintenance of a sufficient radio transmittance. Therefore, the laminated glass becomes suitable as an architectural or automotive laminated glass.

Abstract translation: 本发明提供一种夹层玻璃及其制造方法。 该夹层玻璃包括第一透明玻璃板和第二透明玻璃板以及介于其间的中间膜。 该中间膜具有粒径为0.2μm以下且分散在其中的功能性超细颗粒。 由于其中加入了超细颗粒，所以中间膜具有各种附加功能，例如绝热，紫外线吸收和维持足够的无线电透射率。 因此，夹层玻璃适合作为建筑或汽车夹层玻璃。

公开(公告)号：US5731462A

公开(公告)日：1998-03-24

申请号：US768834

申请日：1996-12-18

Applicant: Christophe Calais ,  Remy Teissier

Inventor： Christophe Calais ,  Remy Teissier

IPC: C07C239/08 ,  C07C291/02 ,  C07C249/02 ,  C07C209/00 ,  C07C209/40 ,  C07C249/00

CPC classification number: C07C291/02 ,  C07C239/08

Abstract: The subject of the present invention is a new process for obtaining nitrones. It more particularly relates to a process for obtaining N-monosubstituted hydroxylamine comprising a stage in which a nitrone is formed from a secondary amine in the presence of an oxidizing agent and of at least one C.dbd.O containing species chosen from the group consisting of carbon dioxide, hydrogencarbonates and carbonates.

Abstract translation: 本发明的主题是获得硝酮的新方法。 更具体地涉及一种获得N-单取代羟胺的方法，其包括在氧化剂存在下由仲胺形成硝化酮的阶段和至少一种含C = O的选自碳 二氧化碳，碳酸氢盐和碳酸盐。

公开(公告)号：US4723030A

公开(公告)日：1988-02-02

申请号：US762358

申请日：1985-08-05

Applicant: Gary C. Davis

Inventor： Gary C. Davis

IPC: C07C255/42 ,  C07C67/00 ,  C07C227/00 ,  C07C227/04 ,  C07C229/60 ,  C07C239/00 ,  C07C239/08 ,  C07C239/18 ,  C07C253/00 ,  C07C83/00 ,  C07C101/00

CPC classification number: C07C239/08 ,  C07C239/18

Abstract: A method is provided for enhancing the production rate of arylhydroxylamines by moderated catalytic hydrogenation reactions. Small quantities of acid introduced to the reaction medium doubles the hydrogenation rate of nitroaromatic compounds without a significant loss in selectivity to arylhydroxylamines.

Abstract translation: 提供了通过中等催化氢化反应提高芳基羟胺的生产速率的方法。 引入到反应介质中的少量酸使硝基芳族化合物的氢化速率加倍，而对芳基羟胺的选择性没有显着损失。

公开(公告)号：US20170267629A1

公开(公告)日：2017-09-21

申请号：US15613589

申请日：2017-06-05

Applicant: Dow AgroSciences LLC

Inventor： William C. Lo ,  James E. Hunter ,  Gerald B. Watson ,  Akshay Patny ,  Pravin S. Iyer ,  Joshodeep Boruwa

IPC: C07C233/66 ,  A01N47/10 ,  A01N47/28 ,  A01N47/36 ,  A61K45/06 ,  A61K31/167 ,  A01N37/46 ,  A01N41/10 ,  A01N47/22 ,  A01N47/38 ,  A01N37/20 ,  A01N37/28 ,  C07D241/12 ,  C07D295/192 ,  C07C335/14 ,  C07C243/14 ,  A61K31/5375 ,  A61K31/505 ,  A61K31/4965 ,  A61K31/426 ,  A61K31/4245 ,  A61K31/4196 ,  A61K31/17 ,  A61K31/166 ,  A01N53/00 ,  A01N47/32 ,  A01N43/653 ,  A01N43/54 ,  C07D277/32 ,  C07D401/10 ,  A01N37/18 ,  A01N37/34 ,  A01N43/08 ,  A01N43/16 ,  A01N43/20 ,  A01N43/40 ,  A01N43/50 ,  A01N43/60 ,  A01N43/78 ,  A01N43/82 ,  C07C233/65 ,  C07C255/57 ,  C07C63/70 ,  C07D207/16 ,  C07D213/61 ,  C07D295/12 ,  C07D331/04 ,  C07D271/10 ,  C07D249/14 ,  C07D239/26 ,  C07C255/46 ,  C07C259/08 ,  C07C271/22 ,  C07C271/24 ,  C07C275/24 ,  C07C211/27 ,  C07C211/29 ,  C07C211/30 ,  C07C211/42 ,  C07C233/13 ,  C07C233/56 ,  C07C233/83 ,  C07C237/06 ,  C07C237/24 ,  C07C239/08 ,  C07C243/22 ,  C07C243/32 ,  C07C251/44 ,  C07C327/46 ,  A01N43/10 ,  A01N43/56 ,  A01N61/00

CPC classification number: C07C233/66 ,  A01N37/10 ,  A01N37/18 ,  A01N37/20 ,  A01N37/28 ,  A01N37/34 ,  A01N37/46 ,  A01N41/10 ,  A01N43/08 ,  A01N43/10 ,  A01N43/16 ,  A01N43/20 ,  A01N43/36 ,  A01N43/40 ,  A01N43/50 ,  A01N43/54 ,  A01N43/56 ,  A01N43/60 ,  A01N43/653 ,  A01N43/78 ,  A01N43/82 ,  A01N43/84 ,  A01N47/10 ,  A01N47/22 ,  A01N47/28 ,  A01N47/32 ,  A01N47/36 ,  A01N47/38 ,  A01N53/00 ,  A01N61/00 ,  A61K31/166 ,  A61K31/167 ,  A61K31/17 ,  A61K31/4196 ,  A61K31/4245 ,  A61K31/426 ,  A61K31/4965 ,  A61K31/505 ,  A61K31/5375 ,  A61K45/06 ,  C07C63/70 ,  C07C211/27 ,  C07C211/29 ,  C07C211/30 ,  C07C211/42 ,  C07C233/13 ,  C07C233/56 ,  C07C233/65 ,  C07C233/83 ,  C07C237/06 ,  C07C237/24 ,  C07C239/08 ,  C07C243/14 ,  C07C243/22 ,  C07C243/32 ,  C07C251/44 ,  C07C255/46 ,  C07C255/57 ,  C07C259/08 ,  C07C271/22 ,  C07C271/24 ,  C07C275/24 ,  C07C327/46 ,  C07C335/14 ,  C07C2601/02 ,  C07C2601/04 ,  C07C2602/08 ,  C07C2602/10 ,  C07D207/16 ,  C07D207/26 ,  C07D209/08 ,  C07D209/48 ,  C07D211/58 ,  C07D213/40 ,  C07D213/61 ,  C07D237/32 ,  C07D239/26 ,  C07D241/12 ,  C07D249/08 ,  C07D249/14 ,  C07D271/10 ,  C07D277/28 ,  C07D277/32 ,  C07D277/64 ,  C07D295/108 ,  C07D295/12 ,  C07D295/192 ,  C07D307/06 ,  C07D307/52 ,  C07D331/04 ,  C07D401/10 ,  C07D405/04

Abstract: This document discloses molecules having the following formula (“Formula One”): and processes associated therewith.

公开(公告)号：US20170260125A1

公开(公告)日：2017-09-14

申请号：US15511674

申请日：2015-08-26

Applicant: Kureha Corporation

Inventor： Hisashi KANNO

IPC: C07C211/65 ,  H01G9/20 ,  H01L51/42 ,  H01L51/00 ,  H01L51/44

CPC classification number: C07C211/65 ,  C07C211/15 ,  C07C239/08 ,  C07C239/20 ,  H01G9/2009 ,  H01L51/005 ,  H01L51/4253 ,  H01L51/442

Abstract: The present invention provides a novel compound to be used in a solar cell. The compound of the present invention is an organic-inorganic hybrid compound represented by Formula (I). R1CH2N+H3M1X13   (I) where, R1 is a C1-C5 alkyl group or C2-C5 alkenyl group substituted with at least one halogen atom; M1 is a divalent metal ion; X1 is a monovalent halogen atom ion; and X13 is formed from one type of halogen atom ion or a combination of two or more types of halogen atom ions.