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    METHOD OF PRODUCING OPTICALLY ACTIVE COMPOUND
    343.
    发明申请
    METHOD OF PRODUCING OPTICALLY ACTIVE COMPOUND 有权
    生产光学活性化合物的方法

    公开(公告)号：US20160250625A1

    公开(公告)日：2016-09-01

    申请号：US14777649

    申请日：2014-06-03

    Applicant: DEXERIALS CORPORATION

    Inventor： Hiroki KANAYA ,  Mamiko NOMURA

    IPC: B01J31/06 ,  C07C201/12 ,  B01J8/02

    CPC classification number: B01J31/062 ,  B01J8/02 ,  B01J31/06 ,  B01J37/00 ,  B01J2208/02 ,  C07B53/00 ,  C07B2200/07 ,  C07C201/12 ,  C07C201/16 ,  C07C205/48 ,  C07C2601/10 ,  C07C2601/14 ,  C07C205/19

    Abstract: An optically active compound production method using a column reactor, a column for column reactor is charged with asymmetric catalyst particles to produce the column reactor, and reaction compound is introduced into column reactor to bring reaction compound into contact with asymmetric catalyst particles, whereby reaction compound is converted to optically active compound. Asymmetric catalyst particles are preferably resin particles that are prepared from a monomer composition containing a proline derivative monomer having unsaturated bond and radical polymerization initiator and serve as catalyst for enamine mechanism reaction. Asymmetric catalyst particles are preferably resin particles prepared by micro-channel method including injecting monomer composition into continuous phase to thereby form droplets of monomer composition in continuous phase and then heating droplets to cause proline derivative monomer having an unsaturated bond to undergo radical polymerization.

    Abstract translation: 使用柱式反应器，塔式反应器塔的旋光化合物制备方法装有不对称催化剂颗粒以制备塔式反应器，并将反应化合物引入塔式反应器以使反应化合物与不对称催化剂颗粒接触，由此反应化合物 转化为光学活性化合物。 不对称催化剂颗粒优选由含有具有不饱和键的脯氨酸衍生物单体和自由基聚合引发剂的单体组合物制备并用作烯胺机理反应的催化剂的树脂颗粒。 不对称催化剂颗粒优选通过微通道法制备的树脂颗粒，包括将单体组合物注入连续相中，从而在连续相中形成单体组合物的液滴，然后加热液滴以使具有不饱和键的脯氨酸衍生物单体进行自由基聚合。

    Process for the preparation of nitroalcohols
    346.
    发明授权
    Process for the preparation of nitroalcohols 有权
    制备硝基醇的方法

    公开(公告)号：US09212126B2

    公开(公告)日：2015-12-15

    申请号：US14379798

    申请日：2013-02-07

    Applicant: Angus Chemical Company

    Inventor： David W. Moore ,  G. David Green

    IPC: C07C201/12

    CPC classification number: C07C201/12 ,  C07C205/15

    Abstract: A process of preparing a nitroalcohol, e.g., 2-nitro-2-methyl-1-propane, from a nitropolyol, e.g., 2-nitro-2-methyl-1,3-propanediol, the process comprising the step of contacting under hydrogenation conditions the nitropolyol with hydrogen, a hydrogenation catalyst and, optionally, a chelating agent.

    Abstract translation: 一种由硝基多元醇例如2-硝基-2-甲基-1,3-丙二醇制备硝基醇，例如2-硝基-2-甲基-1-丙烷的方法，该方法包括在氢化下接触的步骤 用氢气，硝基多烯醇与氢化催化剂和任选的螯合剂进行反应。

    Method of preparing chiral ketones from aldehydes
    347.
    发明授权
    Method of preparing chiral ketones from aldehydes 有权
    从醛制备手性酮的方法

    公开(公告)号：US09120721B2

    公开(公告)日：2015-09-01

    申请号：US14359847

    申请日：2012-12-13

    Applicant: Nanyang Technological University

    Inventor： Yonggui Chi ,  Bhoopendra Tiwari

    IPC: C07C211/00 ,  C07C205/00 ,  C07C207/00 ,  C07C221/00 ,  C07C201/12 ,  C07C205/02 ,  C07C205/44 ,  C07B41/06 ,  C07C225/14 ,  C07C225/16

    CPC classification number: C07C221/00 ,  C07B41/06 ,  C07C201/12 ,  C07C205/02 ,  C07C205/44 ,  C07C225/14 ,  C07C225/16

    Abstract: Present invention relates to a method of preparing a chiral α- or β-substituted ketone from the corresponding β- or γ-substituted aldehyde, wherein the ketone has formula (I), (III) or (V), and the corresponding aldehyde has formula (II), (IV) or (VI), respectively, the method comprising reacting the aldehyde of formula (II), (IV) or (VI) in the presence of an amine, oxygen and an organic solvent, wherein the reaction is carried out in the absence of a metal-based catalyst or a metal-based oxidant, wherein: R is H, a substituted or unsubstituted C1-C10 alkyl, substituted or unsubstituted C2-C15 alkenyl, substituted or unsubstituted C2-C15 alkynyl, substituted or unsubstituted C3-C15 cycloalkyl, substituted or unsubstituted C3-C15 cycloalkenyl, substituted or unsubstituted C3-C15 heterocycloalkyl, substituted or unsubstituted C3-C15 heterocycloalkenyl, substituted or unsubstituted C6-C15 aryl, or substituted or unsubstituted C6-C15 heteroaryl; and R′ is H, a substituted or unsubstituted C1-C10 alkyl, substituted or unsubstituted C2-C15 alkenyl, substituted or unsubstituted C2-C15 alkynyl, substituted or unsubstituted C3-C15 cycloalkyl, substituted or unsubstituted C3-C15 cycloalkenyl, substituted or unsubstituted C3-C15 heterocycloalkyl, substituted or unsubstituted C3-C15 heterocycloalkenyl, substituted or unsubstituted C6-C15 aryl, or substituted or unsubstituted C6-C15 heteroaryl.

    Abstract translation: 本发明涉及从相应的β-取代醛或γ-取代醛制备手性α-或β-取代的酮的方法，其中酮具有式（I），（III）或（V），和相应的 醛分别具有式（II），（IV）或（VI），所述方法包括在胺，氧和有机溶剂的存在下使式（II），（IV）或（VI）的醛反应，其中 该反应在不存在金属类催化剂或金属类氧化剂的情况下进行，其中：R为H，取代或未取代的C 1 -C 10烷基，取代或未取代的C 2 -C 15烯基，取代或未取代的C 2 -C 15 取代或未取代的C 3 -C 15环烯基，取代或未取代的C 3 -C 15环烯基，取代或未取代的C 3 -C 15杂环烷基，取代或未取代的C 3 -C 15杂环烯基，取代或未取代的C 6 -C 15芳基或取代或未取代的C 6 -C 15杂芳基 ; 取代或未取代的C 1 -C 15烷基，取代或未取代的C 2 -C 15烯基，取代或未取代的C 2 -C 15炔基，取代或未取代的C 3 -C 15环烷基，取代或未取代的C 3 -C 15环烯基，取代或未取代的 C 3 -C 15杂环烷基，取代或未取代的C 3 -C 15杂环烯基，取代或未取代的C 6 -C 15芳基或取代或未取代的C 6 -C 15杂芳基。

    DERIVATISATION OF CARBON
    348.
    发明申请
    DERIVATISATION OF CARBON 审中-公开
    碳的衍生物

    公开(公告)号：US20150197481A1

    公开(公告)日：2015-07-16

    申请号：US14665832

    申请日：2015-03-23

    Applicant: SCHLUMBERGER TECHNOLOGY CORPORATION

    Inventor： Fenglou Zou ,  Nathan Lawrence ,  Timothy Jones

    IPC: C07C201/12

    CPC classification number: C07C201/12 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/156 ,  C01B32/174 ,  C01B32/194 ,  C01B32/20 ,  C01B32/21 ,  C01B32/28 ,  C01B32/354 ,  G01N27/308

    Abstract: A molecular species is covalently attached to elemental carbon by exposing the carbon to a reaction mixture containing a strong base and a compound of the formulaor in which X denotes a covalently attached atom or group capable of forming an X− anion and each Z is a moiety comprising a plurality of atoms, but which does not have a hydrogen atom directly attached to the atom which itself is directly attached to the —CH2X or —CHX group. The carbon substrate may be graphite or carbon nanotubes.

    Abstract translation: 通过将碳暴露于含有强碱和下式化合物的反应混合物中，分子物质与元素碳共价连接，或其中X表示共价连接的能够形成X-阴离子的原子或基团，并且每个Z为 部分包含多个原子，但不具有与本身直接连接至-CH 2 X或-CHX基团的原子直接相连的氢原子。 碳衬底可以是石墨或碳纳米管。

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