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    (Meth)acrylic ester of alkenylene glycols and the use thereof
    51.
    发明授权
    (Meth)acrylic ester of alkenylene glycols and the use thereof 失效
    （甲基）亚烷基二醇的丙烯酸酯及其用途

    公开(公告)号：US07405321B2

    公开(公告)日：2008-07-29

    申请号：US10558996

    申请日：2004-06-04

    Applicant: Ulrich Riegel ,  Thomas Daniel ,  Matthias Weismantel ,  Mark Elliott ,  Rudiger Funk ,  Reinhold Schwalm

    Inventor： Ulrich Riegel ,  Thomas Daniel ,  Matthias Weismantel ,  Mark Elliott ,  Rudiger Funk ,  Reinhold Schwalm

    IPC: C07C69/52 ,  C08F20/10 ,  C08F220/12

    CPC classification number: C07C69/54 ,  C07C67/08

    Abstract: The present invention relates to novel (meth)acrylic esters of polyalkoxylated glycols of the formula where AO is independently at each instance is —O—CHR3-CHR4- or —CHR3-CHR4-O— where R3 and R4 are independently H, linear or branched C1-C8-alkyl, p1 is 1, 2, 3, 4, 5, 6, 7, 8, 9, 10, 11, 12, 13, 14, 15, 16, 17, 18, 19, 20, 21, 22, 23, 24, 25, 26, 27, 28, 29, 30, 31, 32, 33, 34, or 35, p2 is 1, 2, 3, 4, 5, 6, 7, 8, 9, 10, 11, 12, 13, 14, 15, 16, 17, 18, 19, 20, 21, 22, 23, 24, 25, 26, 27, 28, 29, 30, 31, 32, 33, 34, or 35, n is 1, 2, 3, 4, 5, 6, 7, 8, 9, 10, 11, 12, 13, 14, 15, 16, 17, 18, 19, 20, 21, 22, 23, 24, 25, 26, 27, 28, 29, 30, 31, 32, 33, 34, 35, 36, 37, 38, 39, 40, 41, 42, 43, 44, 45, 46, 447, 48, 49, 50, 51, 52, 53, 54, 55, 56, 57, 58, 59, 60, 61, 62, 63, 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75, 76, 77, 78, 79, 80, 81, 82, 83, 84, 85, 86, 87, 88, 89, 90, 91, 92, 93, 94, 95, 96, 97, 98, 99, 100, R1 and R2 are independently H or CH3, wherein there is at least one AO in (AO)p1 and also at least one AO in (AO)p2 where R3 and R4 are not both H at one and the same time, a simplified process for preparing these esters and use of reaction mixtures thus obtainable.

    Abstract translation: 本发明涉及下式的聚烷氧基化二醇的（甲基）丙烯酸酯：其中AO各自独立地为-O-CHR 3 -CHR 4 - 或-CHR 3 -CHR 4 -O-，其中R 3和R 4独立地为H，直链或 支链C 1 -C 8 - 烷基，p 1为1,2,3,4,5,6,7,8,9,10,11,12,13,14,15,16,17,18,19,20,21 ，22,23,24,25,26,27,28,29,30,31,32,33,34或35中，p2分别为1,2,3,4,5,6,7,8,9,9,10,11,12,13,14,15,16,17,18,19,20,21,22,23,24,25,26,27,28,29,30,31,32,33,34或35， 10，11，12，13，14，15，16，17，18，19，20，21，22，23，24，25，26，27，28，29，30，31，32，33，34， 或35，n为1,2,3,4,5,6,7,8,9,10,11,12,13,14,15,16,17,18,19,20,21,22,23 ，24,25,26,27,28,29,30,31,32,33,34,35,36,37,38,39,40,41,42,43,44,45,46,447,48 ，49，50，51，52，53，54，55，56，57，58，59，60，61，62，63，64，65，66，67，68，69，70，，71，72，73 ，74，75，76，77，78，79，80，81，82，83，84，85，86，87，88，89，90，91，92，93，94，95，96，97，98 ，99,100，R 1和R 2独立地为H或CH 3，其中存在至少一个AO （AO）p1和（AO）p2中的至少一个AO，其中R3和R4不同时为一个，一个简单的制备这些酯的方法和使用如此获得的反应混合物。

    Synthesis of phenyl-substituted fluoranthenes by a diesel-alder reaction and the use thereof
    56.
    发明申请
    Synthesis of phenyl-substituted fluoranthenes by a diesel-alder reaction and the use thereof 有权
    苯基取代的荧蒽通过狄尔斯 - 阿尔德反应合成及其应用

    公开(公告)号：US20070069198A1

    公开(公告)日：2007-03-29

    申请号：US10573803

    申请日：2004-09-28

    Applicant: Florian Dotz ,  Reinhold Schwalm ,  Joachim Rosch

    Inventor： Florian Dotz ,  Reinhold Schwalm ,  Joachim Rosch

    IPC: H01L51/00 ,  C07C69/52 ,  C07D213/84

    CPC classification number: C07C13/66 ,  C07C2/867 ,  C07C2603/48 ,  C09K11/06 ,  C09K2211/1011 ,  H01L51/0054 ,  H01L51/0058 ,  H01L51/5012 ,  H05B33/14 ,  Y10S428/917

    Abstract: Fluoranthene derivatives of the general formula I where the symbols have the following meanings: R1, R2, R3, R4, R5 are each hydrogen, alkyl, an aromatic radical, a fused aromatic ring system, a heteroaromatic radical or —CH═CH2, (E)- or (Z)-CH═CH—C6H5, acryloyl, methacryloyl, methylstyryl, —O—CH═CH2 or glycidyl; where at least one of the radicals R1, R2 and/or R3 is not hydrogen; X is an alkyl radical, an aromatic radical, a fused aromatic ring system, a heteroaromatic radical or a radical of the formula (I′) or an oligophenyl group; n is from 1 to 10 or, in the case of X=oligophenyl group, 1-20; with the proviso that R1, R2, R3 and X are not at the same time phenyl when R4 and R5 are hydrogen. Furthermore, the invention relates to a process for preparing them and the use of fluoranthene derivatives as emitter molecule in organic light-emitting diodes (OLEDs), a light-emitting layer comprising the fluoranthene derivatives of the invention as emitter molecules, an OLED comprising the light-emitting layer of the invention and devices comprising the OLED of the invention.

    Abstract translation: 其中符号具有以下含义的通式I的荧蒽衍生物：R 1，R 2，R 3，R 4， R 5各自为氢，烷基，芳族基，稠合芳环系，杂芳族基或-CH-CH 2，（E） - 或（Z）-CH-CH-C 6 H 5，丙烯酰基，甲基丙烯酰基，甲基苯乙烯基，-O-CH-CH 2或 缩水甘油基 其中基团R 1，R 2和/或R 3中的至少一个不是氢; X是烷基，芳族基团，稠合芳族环系统，杂芳族基团或式（I'）的基团或低级苯基; n为1至10，或在X =低聚苯基的情况下为1-20; 条件是R 4，R 2，R 3和X不在同时为R 4时的苯基， SUP>和R 5是氢。 此外，本发明涉及其制备方法以及在有机发光二极管（OLED）中使用荧蒽衍生物作为发射体分子的方法，包含本发明的荧蒽衍生物作为发射体分子的发光层，包含 本发明的发光层和包含本发明的OLED的器件。

    Curable aqueous polyurethane dispersions
    57.
    发明授权
    Curable aqueous polyurethane dispersions 失效
    可固化水性聚氨酯分散体

    公开(公告)号：US07169841B2

    公开(公告)日：2007-01-30

    申请号：US10311307

    申请日：2001-06-26

    Applicant: Reinhold Schwalm ,  Bernd Bruchmann ,  Frank Voellinger ,  Erich Beck ,  Wolfgang Schrof ,  Uwe Meisenburg

    Inventor： Reinhold Schwalm ,  Bernd Bruchmann ,  Frank Voellinger ,  Erich Beck ,  Wolfgang Schrof ,  Uwe Meisenburg

    IPC: C08J3/00 ,  C08K3/20 ,  C08L75/00 ,  C08F8/30 ,  C08F283/04

    CPC classification number: C09D175/16 ,  C08G18/7837 ,  C08G18/8175 ,  Y10T428/31551 ,  C08G18/0823

    Abstract: A curable aqueous polyurethane dispersion substantially comprises a) at least one compound having two free isocyanate groups, at least one allophanate group and at least one C═C double bond capable of free radical polymerization, a carbonyl group or an oxygen atom in the form of an ether function being bonded directly to the double bond, b) at least one compound having at least one group reactive toward isocyanate groups and having a C═C double bond capable of free-radical polymerization, c) if required, at least one compound having at least two groups reactive towards isocyanate groups and selected from hydroxyl, mercapto, primary and/or secondary amino groups, d) at least one compound having at least one group reactive towards isocyanate groups and having at least one acid group, e) at least one basic compound for neutralizing or partially neutralizing the acid groups of the compounds d), and a thermal initiator and is used for coating substrates.

    Abstract translation: 可固化的水性聚氨酯分散体基本上包含a）至少一种具有两个游离异氰酸酯基团的化合物，至少一个脲基甲酸酯基团和至少一个能够自由基聚合的CC双键，羰基或乙醚形式的氧原子 b）至少一种具有至少一个对异氰酸酯基团具有反应性并具有能够进行自由基聚合的CC双键的化合物，c）如果需要，至少一种具有至少两个的化合物 对异氰酸酯基反应并且选自羟基，巯基，伯和/或仲氨基的基团，d）至少一种具有至少一个对异氰酸酯基团具有反应性并具有至少一个酸基团的化合物，e）至少一种碱性化合物 用于中和或部分中和化合物d）的酸基和热引发剂，并用于涂覆基材。

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