摘要:
A lithium ion-conducting compound, having a garnet-like crystal structure, and having the general formula: Lin[A(3-a′-a″)A′(a′)A″(a″)][B(2-b′-b″)B′(b′)B″(b″)][C′(c′)C″(c″)]O12, where A, A′, A″ stand for a dodecahedral position of the crystal structure, where A stands for La, Y, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm and/or Yb, A′ stands for Ca, Sr and/or Ba, A″ stands for Na and/or K, 0
摘要:
In a method for preparing an ester from an hydroxybenzoic acid and a fatty alcohol for use in a binder system for powder injection molding, transesterification of an ester of the hydroxybenzoic acid and a low alcohol using the fatty alcohol is carried out, the fatty alcohol and the ester of the hydroxybenzoic acid and the low alcohol forming a reaction mixture and being used in an essentially equimolar ratio. The transesterification is carried out at a temperature at which the ester of the hydroxybenzoic acid and the low alcohol and the fatty alcohol are present as a homogeneous melt. The binder system for a powder injection molding contains 80 to 98 wt. % of a metal powder and/or a ceramic powder and 1 to 19 wt. % of a polymeric binder component, and 1 to 19 wt. % of at least one ester prepared by the transesterification.
摘要:
The invention relates to a dental furnace wherein a firing chamber is heated up in a first heating-up period at a first heating-up rate of more than 501 K/min, in particular more than 1001 K/min, which heats the furnace to at least 10001 C, in particular to 1100-12501 C. The first heating-up period is followed by an intermediate heating period, which is at least five minutes long, in particular at least ten minutes long, the gradient or heating-up rate of which is adapted to the material to be sintered in the dental furnace (10), and wherein this is followed by an end heating-up period (44) during which heating up is effected at a heating-up rate of more than 301 K/min, in particular approximately 501 K/min, and wherein during this the furnace temperature is held for at least five minutes, in particular for at least 25 minutes, above the temperature toward the end of the first heating-up period, and wherein forced cooling of the furnace (10) is performed after this.
摘要:
The invention relates to a process for the continuous thermal removal of binder from a metallic and/or ceramic shaped body which has been produced by injection molding, extrusion or pressing using a thermoplastic composition and comprises at least one polyoxymethylene homopolymer or copolymer as binder in a binder removal oven, which comprises the steps (a) removal of binder from the shaped body in a binder removal oven at a temperature which is from 5 to 20° C. below, preferably from 10 to 15° C. below, the temperature of a second temperature stage over a period of from 4 to 12 hours in a first temperature stage in an oxygen-comprising atmosphere, (b) removal of binder from the shaped body at a temperature in the range >160 to 200° C. over a period of from 4 to 12 hours in an oxygen-comprising atmosphere in a second temperature stage and (c) removal of binder from the shaped body at a temperature in the range from 200 to 600° C. over a period of from 2 to 8 hours in a third temperature stage in an oxygen-comprising or neutral or reducing atmosphere, with the shaped bodies being transported through the binder removal oven during process steps (a) and (b).
摘要:
A ceramic coating process comprises introducing a suspension including a fine ceramic particulate suspended in a liquid carrier into a plasma torch. The method includes melting the fine ceramic particulate in the plasma torch; propelling the fine ceramic particulate toward a substrate; and forming a coating on the substrate, the coating comprises splats of the fine ceramic particulate.
摘要:
Articles and methods in which an electric field is used to actuate a material are generally described. Provided in one embodiment is a method including applying an electric field to a ceramic material. Applying the electric field to the ceramic material can transform the ceramic material from a first solid phase to a second distinct solid phase. The applied electric field is less than a breakdown electric field of the ceramic material, according to certain embodiments.
摘要:
A panel includes a display window and a supporting body integrated with the display window. The display window is made of sapphire and the supporting body is made of ceramic materials. The supporting body is integrally formed with the supporting body by sintering process. A method for manufacturing the panel is also provided.
摘要:
An oxide-based solid electrolyte according to the present invention may be LixLa3M2O12 and may have a cubic phase. The oxide-based solid electrolyte may further include first and second dopants. A method of preparing an oxide-based solid electrolyte according to the concept of the present invention may include mixing a lithium compound, a lanthanum compound, a metal compound, a first dopant precursor, and a second dopant precursor to prepare an intermediate, and crystallizing the intermediate to prepare LixLa3M2O12 crystals having a cubic phase.
摘要:
A process for fabricating pre-sintered zirconia blanks that are then computer machined and sintered to form dental appliances having highly advantageous features. The principal steps of a preferred embodiment of that process comprise a) preparing a ceramic slurry of binderless zirconia powder; b) subjecting the slurry to attrition milling down to about a 5-29 nm crystallite size; c) preparing a vacuum assisted and pressure assisted slip casting mold and pouring the milled slurry into the slip-casting mold; d) after casting, excess slurry is poured from the mold and a consolidated zirconia blank is removed; e) drying the blank and pre-sintering it to form solid blanks ready for CAD/CAM machining and sintering to net shape. The attrition is run with ball bearings that are of the sample material to prevent contamination. It also is run, up to 24 hours, to break down the crystallites to overcome the high density of zirconia.
摘要:
A solid oxide fuel cell (SOFC) includes a cathode electrode, a solid oxide electrolyte, and an anode electrode. The electrolyte and/or electrode composition includes zirconia stabilized with (i) scandia, (ii) ceria, and (iii) at least one of yttria and ytterbia. The composition does not experience a degradation of ionic conductivity of greater than 15% after 4000 hrs at a temperature of 850° C.