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    Multiautoclave for combinatorial synthesis of zeolites and other materials
    5.
    发明授权
    Multiautoclave for combinatorial synthesis of zeolites and other materials 失效
    用于组合合成沸石和其他材料的多孔沸石

    公开(公告)号：US06821486B1

    公开(公告)日：2004-11-23

    申请号：US09308562

    申请日：1999-07-16

    申请人： Duncan Akporiaye ,  Ivar Martin Dahl ,  Arne Karlsson ,  Rune Wendelbo

    发明人： Duncan Akporiaye ,  Ivar Martin Dahl ,  Arne Karlsson ,  Rune Wendelbo

    IPC分类号： B01L300

    CPC分类号： B01J3/04 ,  B01J19/0046 ,  B01J2219/00313 ,  B01J2219/00319 ,  B01J2219/00335 ,  B01J2219/00349 ,  B01J2219/00477 ,  B01J2219/00585 ,  B01J2219/00596 ,  B01J2219/00601 ,  B01J2219/00745 ,  B01J2219/00747 ,  B01J2219/00754 ,  C01B39/02 ,  C40B30/08 ,  C40B40/18 ,  C40B60/14

    摘要： The invention relates to a multi-autoclave and details of its design, a method for automated synthesis of zeolites in the multi-autoclave, and furthermore, to applications of the multi-autoclave for an automated synthesis which is optimized simultaneously with regard to several synthesis parameters in the synthesis of zeolites. The multi-autoclave consists typically of a pressure vessel/autoclave having from 10 to 10,000 small, separated chambers lined with an inert material, with each chamber typically having a volume of 0.2-2 ml. The chambers preferably are formed as through-going perforations in a central block and the perforations are sealed by balls, septa, stoppers or such which are placed at the bottom and top of each through-going perforation. Metal plates are placed over and under the central block so that a closing mechanism is pressed against the edges of the perforations with sufficient load to enable the chambers to be filled with aqueous mixtures and to be heated to 200° C. without the occurrence of leakage. Top and bottom plates and closing mechanisms can be integrated so that all the perforations are sealed simultaneously when these are placed at the top and bottom sides of the central block.

    摘要翻译： 本发明涉及一种多级高压釜及其设计的细节，一种在多重高压釜中自动合成沸石的方法，此外，涉及多个高压釜用于自动化合成的应用，其在多个合成中同时被优化 沸石合成中的参数。 多压釜通常由压力容器/高压釜组成，压力容器/高压釜具有内衬有惰性材料的10至10,000个小的分开的室，每个室通常具有0.2-2ml的体积。 这些室优选地在中心块中形成为穿孔穿孔，并且穿孔由球，隔片，塞子等密封，这些孔，隔片，塞子等放置在每个贯穿孔的底部和顶部。 将金属板放置在中央块的上方和下方，使得闭合机构以足够的负载压靠穿孔的边缘，以使得腔室能够充满含水混合物并且被加热到200℃，而不会发生泄漏 。 顶板和底板和关闭机构可以集成，使得当这些孔被放置在中心块的顶部和底部侧面时，所有的穿孔同时被密封。

    Crystalline metallophosphates
    9.
    发明授权
    Crystalline metallophosphates 失效
    结晶金属磷酸盐

    公开(公告)号：US6001328A

    公开(公告)日：1999-12-14

    申请号：US142498

    申请日：1999-04-14

    申请人： Karl Petter Lillerud ,  Erling N. Halvorsen ,  Arne Karlsson ,  Duncan Akporiaye ,  Jorun Hustveit

    发明人： Karl Petter Lillerud ,  Erling N. Halvorsen ,  Arne Karlsson ,  Duncan Akporiaye ,  Jorun Hustveit

    IPC分类号： C01B25/36 ,  B01J29/04 ,  B01J29/82 ,  B01J29/85 ,  C01B33/20 ,  C01B37/08 ,  C01B39/54 ,  C07C1/20 ,  B01J29/83 ,  C01B25/45

    CPC分类号： C01B37/08 ,  B01J29/85 ,  C07C1/20 ,  C07C2529/85 ,  Y10S423/30

    摘要： Microporous crystalline metallophosphate composition having an essential framework structure whose chemical composition in the as synthesised form expressed in terms of mole rations of oxides is: mR(M.sub.x Al.sub.y P.sub.z)O.sub.2 where M is silicon, x+y+z=1, m may have a value from 0.02 to 0.3, R is at least one templating agent, x, y and z represent the mole fractions of silicon, aluminium and phosphorous presentin the product, and where x may have a value from 0 to 0.5, y may have a value from 0.25 to 0.5 and z may have a value from 0.25 to 0.5, and where one reactive form of fluoride may be present in an effective amount to form the product, and having a characteristic X-ray powder diffraction pattern containing at least the d-spacings as set forth in Table 1.

    摘要翻译： PCT No.PCT / NO97 / 00076 Sec。 371 1999年4月14日第 102（e）1999年4月14日PCT 1997年3月13日PCT公布。 出版物WO97 / 33693 日期1997年9月18日具有必要骨架结构的微孔结晶金属磷酸盐组合物，其化学成分以氧化物摩尔比表示，为：mR（MxAlyPz）O 2，其中M为硅，x + y + z = 1， m可以具有0.02至0.3的值，R是至少一种模板剂，x，y和z表示存在于产物中的硅，铝和磷的摩尔分数，并且其中x可以具有0至0.5的值，y 可以具有0.25至0.5的值，z可以具有0.25至0.5的值，并且其中一种反应性形式的氟化物可以以有效的量存在以形成产物，并且具有包含以下物质的特征X射线粉末衍射图 最小的d-间距如表1所示。