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公开(公告)号：US09688891B2
公开(公告)日：2017-06-27
申请号：US14650138
申请日：2013-12-23
IPC分类号： B32B5/28 , B32B27/04 , B32B27/20 , C09J163/00 , C08J5/04 , C08K3/36 , C08J5/24 , C08J5/00 , C08J5/10 , B32B27/38
CPC分类号： C09J163/00 , C08J5/005 , C08J5/04 , C08J5/042 , C08J5/10 , C08J5/24 , C08J2363/00 , C08J2363/02 , C08J2363/04 , C08K3/36
摘要： A fiber reinforced polymer composition is provided comprising a fiber and an adhesive composition, wherein the adhesive composition comprises at least a thermosetting resin, a curing agent, and a hard interfacial material. When cured, the adhesive composition forms good bonds to the reinforcing fiber, and an interfacial region between the reinforcing fiber and the adhesive composition is formed which comprises the hard interfacial material. Additional embodiments include a prepreg and a method of manufacturing a composite article by curing the adhesive composition and the reinforcing fiber.
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2.发明申请公开(公告)号：US20180355132A1
公开(公告)日：2018-12-13
申请号：US15778563
申请日：2016-12-14
发明人： Alfred P. Haro , Nobuyuki Arai
CPC分类号： C08J5/24 , B29B11/16 , B29K2063/00 , B29K2307/04 , B32B5/024 , B32B5/12 , B32B2260/023 , B32B2260/046 , C08J5/04 , C08J5/042 , C08J2363/00 , C08J2481/06
摘要： A permeable laminate body containing at least one partially impregnated prepreg which includes at least component (A) containing a matrix of reinforcing fiber, component (B) containing a thermosetting resin, and, optionally, component (C) containing a particle or a fiber of a thermoplastic resin exhibits long out time processability with good storage stability, achieving when molded and cured a fiber reinforced composite having a low void ratio and providing excellent mechanical performance.
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公开(公告)号：US20180290339A1
公开(公告)日：2018-10-11
申请号：US15762175
申请日：2016-09-27
CPC分类号： B29B11/16 , B29K2063/00 , B29K2307/04 , B32B5/022 , B32B5/024 , B32B5/026 , B32B5/26 , B32B5/28 , B32B7/04 , B32B27/08 , B32B27/12 , B32B27/18 , B32B27/20 , B32B27/26 , B32B27/281 , B32B27/285 , B32B27/286 , B32B27/288 , B32B27/30 , B32B27/34 , B32B27/36 , B32B27/365 , B32B27/38 , B32B27/40 , B32B27/42 , B32B2250/05 , B32B2250/40 , B32B2260/023 , B32B2260/046 , B32B2262/0269 , B32B2262/10 , B32B2262/101 , B32B2262/103 , B32B2262/105 , B32B2262/106 , B32B2262/14 , B32B2264/0207 , B32B2264/0214 , B32B2264/0264 , B32B2264/102 , B32B2264/107 , B32B2264/108 , B32B2270/00 , B32B2307/30 , B32B2307/306 , B32B2307/50 , B32B2307/54 , B32B2307/558 , B32B2307/714 , B32B2307/718 , B32B2307/732 , C08J5/24 , C08J2363/00 , C08J2463/00 , C08J2471/00 , C08J2479/04
摘要： A prepreg comprising a layer of impregnated reinforcing fibers comprising at least one layer of reinforcing fibers impregnated by a resin composition comprising at least a thermosetting resin, a curing agent and an accelerator, such that the accelerator has a gradient concentration which is more concentrated in the resin composition in the vicinity of the reinforcing fibers than further away. The resin composition comprising a first resin composition impregnates the reinforcing fibers to provide a layer of impregnated reinforcing fibers and a surface layer comprising a second resin composition is formed on the layer of impregnated reinforcing fibers, wherein the first resin composition has at least one peak exotherm occurring at a time earlier than and/or at a temperature lower than any peak exotherm of the second resin composition. The heat generation from the first resin composition is tailored to initiate or speed up the curing of the second resin composition, leading to a substantial reduction of cure cycle time of the prepreg. Excellent handling and processing abilities of the uncured prepreg and excellent physical, thermal and mechanical properties when cured are achieved.
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公开(公告)号：US20240093003A1
公开(公告)日：2024-03-21
申请号：US17767526
申请日：2020-10-14
IPC分类号： C08K5/5313 , C08G59/32 , C08G59/38 , C08G59/44 , C08G59/50 , C08G59/68 , C08J5/24 , C08L63/00
CPC分类号： C08K5/5313 , C08G59/3227 , C08G59/38 , C08G59/44 , C08G59/504 , C08G59/686 , C08J5/243 , C08J5/249 , C08L63/00 , C08J2363/02 , C08J2429/14
摘要： This invention relates to a flame retardant fiber-reinforced composite material based on an epoxy resin composition which includes at least one epoxy resin having an epoxy functionality of at least 2 as well as at least one organic phosphinic acid or derivative thereof (e.g., an organic phosphinic acid-modified epoxy resin), reinforced with a fiber having a thermal conductivity≥3 W/m·K at room temperature, as well as a prepreg for making such a flame retardant fiber-reinforced composite material. More specifically, a composite material is provided that contains a combination of particular types of epoxy resins, curatives, and reinforcing fibers that provide sufficient flame retardance for thin-ply laminates when cured at 163° C. for 15 minutes. These cured composites are also suitable for a variety of applications requiring flame retardancy.
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公开(公告)号：US20150240042A1
公开(公告)日：2015-08-27
申请号：US14435577
申请日：2013-10-10
CPC分类号： C08J5/24 , C08J5/042 , C08J5/10 , C08J2300/24 , C08J2363/00 , C08J2363/02 , C08J2363/04 , C08K7/06
摘要： A fiber reinforced polymer composition is provided comprising a fiber and an adhesive composition, wherein the adhesive composition comprises at least a thermosetting resin and a curing agent, the reinforcing fiber has a tensile modulus of at least 300 GPa and the cured adhesive has a resin modulus of at least 3.2 GPa, and the adhesive composition when cured makes good bonds to the reinforcing fiber. Additional embodiments include a prepreg comprising the fiber reinforced polymer composition and a method of manufacturing a composite article by curing the adhesive composition and a reinforcing fiber.
摘要翻译： 提供一种纤维增强聚合物组合物，其包含纤维和粘合剂组合物，其中所述粘合剂组合物至少包含热固性树脂和固化剂，所述增强纤维的拉伸模量为至少300GPa，并且所述固化的粘合剂具有树脂模量 至少3.2GPa，固化时的粘合剂组合物与增强纤维形成良好的结合。 另外的实施方案包括包含纤维增强聚合物组合物的预浸料和通过固化粘合剂组合物和增强纤维来制造复合制品的方法。
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公开(公告)号：US20240101755A1
公开(公告)日：2024-03-28
申请号：US17767564
申请日：2020-10-14
CPC分类号： C08G59/3227 , C08G59/38 , C08G59/4021 , C08G59/4064 , C08G59/686 , C08J5/249 , C08K5/5313 , C08J2363/02
摘要： This invention relates to a flame retardant epoxy resin composition which includes an epoxy resin structure having an epoxy functionality of 2 or more with a measured total heat release value of not more than 23 kJ/g as well as an organic phosphinic acid structure (in reacted or unreacted form), as well as a prepreg, and a fiber reinforced composite material prepared using the epoxy resin composition. More specifically, an epoxy resin composition is provided that contains a combination of particular types of epoxy resins and curatives that provide sufficient flame retardance when cured at 163° C. for 15 minutes. The epoxy resin systems are also suitable for preparing a fiber-reinforced composite material that will also provide sufficient flame retardance for a variety of applications.
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公开(公告)号：US11565497B2
公开(公告)日：2023-01-31
申请号：US16971376
申请日：2019-03-26
摘要： A laminate body is provided which contains a thin prepreg having a component (A) containing a matrix of reinforcing fiber, a component (B) containing a thermosetting resin, and a component (C) containing particles of a thermoplastic resin. When molded and cured out of autoclave, the laminate body achieves a fiber-reinforced composite having a low void ratio and providing excellent mechanical performance.
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公开(公告)号：US11028244B2
公开(公告)日：2021-06-08
申请号：US15778563
申请日：2016-12-14
发明人： Alfred P. Haro , Nobuyuki Arai
摘要： A permeable laminate body containing at least one partially impregnated prepreg which includes at least component (A) containing a matrix of reinforcing fiber, component (B) containing a thermosetting resin, and, optionally, component (C) containing a particle or a fiber of a thermoplastic resin exhibits long out time processability with good storage stability, achieving when molded and cured a fiber reinforced composite having a low void ratio and providing excellent mechanical performance.
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9.发明申请公开(公告)号：US20150259580A1
公开(公告)日：2015-09-17
申请号：US14435494
申请日：2013-10-10
IPC分类号： C09J163/00 , C09J163/04 , C09J9/00 , C09J11/04 , C09J11/08
CPC分类号： C09J163/00 , C08J5/042 , C08J5/10 , C08J5/24 , C08J2300/24 , C08J2363/00 , C08J2363/02 , C08J2363/04 , C09J9/00 , C09J11/04 , C09J11/08 , C09J163/04
摘要： A fiber reinforced polymer composition is disclosed comprising a reinforcing fiber and an adhesive composition, wherein the adhesive composition comprises at least a thermosetting resin, a curing agent, and an interfacial material, the fiber is suitable for concentrating the interfacial material in an interfacial region between the fiber and the adhesive composition upon curing of the adhesive composition, and the cured adhesive has a resin modulus of at least 4.0 GPa. Also provided is a prepreg comprising the fiber reinforced polymer composition and a method of manufacturing a composite article by curing the reinforced polymer composition. The resulting interfacial region, viz., the reinforced interphase, is reinforced by one or more layers of the interfacial material such that substantial improvements in tensile, compression and fracture toughness may be observed.
摘要翻译： 公开了一种纤维增强聚合物组合物，其包含增强纤维和粘合剂组合物，其中所述粘合剂组合物至少包含热固性树脂，固化剂和界面材料，所述纤维适合于将界面材料浓缩在界面区域之间 在粘合剂组合物固化时的纤维和粘合剂组合物，并且固化的粘合剂具有至少4.0GPa的树脂模量。 还提供了包含纤维增强聚合物组合物的预浸料和通过固化增强的聚合物组合物制造复合制品的方法。 所产生的界面区域，即增强相间，由一层或多层界面材料增强，使得可以观察到拉伸，压缩和断裂韧性的显着改善。
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10.发明申请公开(公告)号：US20210371612A1
公开(公告)日：2021-12-02
申请号：US16963400
申请日：2019-01-30
摘要： The void content of a cured fiber-reinforced composite material is advantageously reduced, particularly when the composite material article is large in size or fabricated using an out-of-autoclave procedure, by using prepreg sheets impregnated with a thermosettable resin composition containing thermoplastic particles and modified to have one or more characteristics such as a certain level of average surface roughness. Such characteristics may be imparted to the prepreg sheet by, for example, conditioning the prepreg sheet by subjecting it to vacuum conditions in advance of being consolidated and cured as part of a prepreg stack.
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