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    ORGANIC SYNTHESIZER
    3.
    发明申请
    ORGANIC SYNTHESIZER 失效
    有机合成剂

    公开(公告)号：US20110027144A1

    公开(公告)日：2011-02-03

    申请号：US12901941

    申请日：2010-10-11

    申请人： Masatoshi Shibata ,  Yutaka Mashiyama ,  Yasuyuki Suzuki ,  Isamu Hiruta ,  Toshiaki Wada ,  Tetsuo Tomoda

    发明人： Masatoshi Shibata ,  Yutaka Mashiyama ,  Yasuyuki Suzuki ,  Isamu Hiruta ,  Toshiaki Wada ,  Tetsuo Tomoda

    IPC分类号： B01J19/18 ,  B01J19/00

    CPC分类号： B01J19/0046 ,  B01F7/001 ,  B01F7/00116 ,  B01F7/00141 ,  B01F7/003 ,  B01F7/00558 ,  B01F13/0827 ,  B01F13/089 ,  B01J2219/00283 ,  B01J2219/00346 ,  B01J2219/00389 ,  B01J2219/00477 ,  B01J2219/00481 ,  B01J2219/00495 ,  B01J2219/00585 ,  B01J2219/0072

    摘要： To provide an organic synthesizer that can conduct a pressure reaction and an atmospheric reaction in one organic synthesizer and can realize attachment of reaction vessels to the organic synthesizer and detachment of the reaction vessels from the organic synthesizer without applying any load to gas supply/discharge pipes.[Means For Solving Problems] An organic synthesizer comprising a reaction vessel support part (160), which can support two or more reaction vessels, and pressure regulation means (164) for regulating the pressure within the reaction vessel supported by the reaction vessel support part (160) by supplying/discharging gas. Two or more pressure regulation means (164) are provided for each reaction vessel supported by the reaction vessel support part (160). At least one pressure regulation means (164A) in the two or more pressure regulation means (164) is constructed so as to be detachable from and attachable to the other pressure regulation means (164B). The pressure regulation means (164) comprises gas supply/discharge pipes (174a to 174d) and openings (194a to 174d) for supporting the gas supply/discharge pipes (174a to 174d). The gas supply/discharge pipes (174a to 174d) are constructed so that a part near the front end can be flexed in a vertical direction and in a lateral direction and are connected to the supported reaction vessels for gas supply and discharge.

    摘要翻译： 提供一种能够在一种有机合成仪中进行压力反应和大气反应的有机合成仪，并且可以实现反应容器与有机合成仪的连接，并使反应容器与有机合成仪分离，而不对气体供给/排出管施加任何负荷 。 解决问题的手段一种有机合成装置，包括可支撑两个或多个反应容器的反应容器支撑部分（160）和用于调节由反应容器支撑部分支撑的反应容器内的压力的压力调节装置（164） （160）通过供给/排出气体。 为由反应容器支撑部分（160）支撑的每个反应容器提供两个或更多个压力调节装置（164）。 两个或更多个压力调节装置（164）中的至少一个压力调节装置（164A）构造成可拆卸并附接到另一压力调节装置（164B）。 压力调节装置（164）包括用于支撑供气/排出管（174a至174d）的气体供给排出管（174a至174d）和开口（194a至174d）。 气体供给排出管174a〜174d构成为能够使前端附近的部分在垂直方向和横向上弯曲并且与支撑的气体供给和排出的反应容器连接。

    Self-sealing apparatus for chemical reaction vessel
    4.
    发明申请
    Self-sealing apparatus for chemical reaction vessel 审中-公开

    公开(公告)号：US20060021673A1

    公开(公告)日：2006-02-02

    申请号：US10899995

    申请日：2004-07-27

    申请人： Stephan Rodewald

    发明人： Stephan Rodewald

    IPC分类号： B65B1/04

    CPC分类号： B65B7/2835 ,  B01J2219/00315 ,  B01J2219/00335 ,  B01J2219/00344 ,  B01J2219/00346 ,  B01L3/50825 ,  B01L2300/042 ,  B01L2300/049 ,  B01L2400/0616 ,  B01L2400/0633 ,  Y10S141/01

    摘要： According to an aspect of the invention, an apparatus for self-sealing of a reaction vessel, such that the reaction vessel may be repeatedly accessed by a fluid transfer mechanism and subsequently self-sealed, is detailed. The reaction vessel has an access opening, and the apparatus comprises a cap, a ball which is comprised of a magnetizable material (such as a ferrous metal), and a ring magnet. The cap is sized to fit over the reaction vessel access opening, and has an access port. The cap has an internal surface which faces the reaction vessel, and an external surface, which faces away from the reaction vessel. The ball is sized to fit over the cap access port, such that a portion of the ball seats partially in the cap access port on the cap internal surface, thus sealing the cap access port. According to an aspect of the invention, the ball may be comprised of a ferromagnetic material, or a magnetizable material that is preferably magnetized. The ring magnet produces a magnetic field, and is mounted to the cap on the cap external surface. The ring magnet is spaced from the cap such that the magnetic field is sufficient to hold the ball in the cap access port, and to reseat the ball in the cap access port after the reaction vessel is accessed.

    Apparatus for multiple, simultaneous synthesis of organic compounds
    5.
    发明授权
    Apparatus for multiple, simultaneous synthesis of organic compounds 失效
    用于多次同时合成有机化合物的装置

    公开(公告)号：US6074613A

    公开(公告)日：2000-06-13

    申请号：US31187

    申请日：1998-02-26

    申请人： James R. Harness ,  Larry W. Markus ,  Tadeusz J. Wozny ,  Rudy H. Haidle ,  Kenneth R. Kaufhold

    发明人： James R. Harness ,  Larry W. Markus ,  Tadeusz J. Wozny ,  Rudy H. Haidle ,  Kenneth R. Kaufhold

    IPC分类号： B01J19/00 ,  C08F2/00 ,  C40B60/14 ,  B01L3/00

    CPC分类号： B01J19/0046 ,  B01J2219/00286 ,  B01J2219/00308 ,  B01J2219/0031 ,  B01J2219/00346 ,  B01J2219/00407 ,  B01J2219/00416 ,  B01J2219/00418 ,  B01J2219/00423 ,  B01J2219/00585 ,  B01J2219/0059 ,  B01J2219/00596 ,  C40B60/14

    摘要： A method and an apparatus for multiple, simultaneous synthesis of compounds. The apparatus includes a reaction block having a heating layer, a cooling layer, each of which may perform both functions, and a collection sump. A plurality of reaction tubes are supported in the reaction block in a matrix. Each reaction tube has a top outlet, a bottom outlet and a filter above the bottom outlet. Spool valves are located to control the bottom outlets of the reaction tubes. Obturators are provided to close the top outlets of the reaction tubes and to provide venting for the reaction tubes. The collection sump alternately may be equipped with individual collection tubes for each reaction tube. Each reaction tube is formed with a restrictive waist and protrusions arranged in a pattern between the waist and its bottom outlet to improve the mixing of the resinous solid supports by creating turbulence. The restrictive waist limits the height of the vortex of solution during mixing and reaction to facilitate heating and refluxing. The method includes introducing a pressurized inert gas through the lower outlets of the reaction tubes and selectively filter the spent reactants and synthesized compounds through the filters.

    摘要翻译： 用于多次同时合成化合物的方法和装置。 该装置包括具有加热层，冷却层，每个都可以执行两个功能的反应块和收集槽。 反应管中的多个反应管以矩阵的形式被支撑。 每个反应管具有顶部出口，底部出口和在底部出口上方的过滤器。 阀芯位于控制反应管底部出口处。 提供闭塞器以封闭反应管的顶部出口并为反应管提供排气。 交替的收集池可以配备有用于每个反应管的各个收集管。 每个反应管形成有限制性的腰部和突起，以腰部和其底部出口之间的图案布置，以通过产生湍流来改善树脂固体支持物的混合。 限制性腰围在混合和反应期间限制溶液涡流的高度，以促进加热和回流。 该方法包括通过反应管的下部出口引入加压的惰性气体，并通过过滤器选择性地过滤废的反应物和合成的化合物。

    Self-sealing apparatus for chemical reaction vessel
    8.
    发明授权
    Self-sealing apparatus for chemical reaction vessel 失效
    化学反应容器自密封装置

    公开(公告)号：US07546855B2

    公开(公告)日：2009-06-16

    申请号：US11604594

    申请日：2006-11-27

    申请人： Stephan Rodewald

    发明人： Stephan Rodewald

    IPC分类号： B65B1/04 ,  B65D51/00

    CPC分类号： B65B7/2835 ,  B01J2219/00315 ,  B01J2219/00335 ,  B01J2219/00344 ,  B01J2219/00346 ,  B01L3/50825 ,  B01L2300/042 ,  B01L2300/049 ,  B01L2400/0616 ,  B01L2400/0633 ,  Y10S141/01

    摘要： According to an aspect of the invention, an apparatus for self-sealing of a reaction vessel, such that the reaction vessel may be repeatedly accessed by a fluid transfer mechanism and subsequently self-sealed, is detailed. The reaction vessel has an access opening, and the apparatus comprises a cap, a ball which is comprised of a magnetizable material (such as a ferrous metal), and a ring magnet. The cap is sized to fit over the reaction vessel access opening, and has an access port. The cap has an internal surface which faces the reaction vessel, and an external surface, which faces away from the reaction vessel. The ball is sized to fit over the cap access port, such that a portion of the ball seats partially in the cap access port on the cap internal surface, thus sealing the cap access port. According to an aspect of the invention, the ball may be comprised of a ferromagnetic material, or a magnetizable material that is preferably magnetized. The ring magnet produces a magnetic field, and is mounted to the cap on the cap external surface. The ring magnet is spaced from the cap such that the magnetic field is sufficient to hold the ball in the cap access port, and to reseat the ball in the cap access port after the reaction vessel is accessed.

    摘要翻译： 根据本发明的一个方面，详细描述了一种用于自密封反应容器的设备，使得反应容器可以被流体转移机构反复进入并随后自密封。 反应容器具有进入口，该装置包括盖，由可磁化材料（例如黑色金属）构成的球和环形磁体。 盖的尺寸适合于反应容器进入口的上方，并具有进入口。 盖具有面向反应容器的内表面和面向反应容器的外表面。 该球的尺寸设置成适合盖帽进入口，使得球的一部分部分地位于帽内表面上的帽进入口中，从而密封盖进入口。 根据本发明的一个方面，球可以由铁磁材料或优选磁化的可磁化材料组成。 环形磁铁产生磁场，并且安装在盖外表面上的盖上。 环形磁体与盖子间隔开，使得磁场足以将球保持在盖子进入口中，并且在反应容器被访问之后将球重新固定在盖子进入口中。

    SELF-SEALING APPARATUS FOR CHEMICAL REACTION VESSEL
    9.
    发明申请
    SELF-SEALING APPARATUS FOR CHEMICAL REACTION VESSEL 失效
    化学反应容器的自密封装置

    公开(公告)号：US20080210689A1

    公开(公告)日：2008-09-04

    申请号：US12117796

    申请日：2008-05-09

    申请人： Stephan Rodewald

    发明人： Stephan Rodewald

    IPC分类号： B65D51/00 ,  B65D88/44

    CPC分类号： B65B7/2835 ,  B01J2219/00315 ,  B01J2219/00335 ,  B01J2219/00344 ,  B01J2219/00346 ,  B01L3/50825 ,  B01L2300/042 ,  B01L2300/049 ,  B01L2400/0616 ,  B01L2400/0633 ,  Y10S141/01

    摘要： According to an aspect of the invention, an apparatus for self-sealing of a reaction vessel, such that the reaction vessel may be repeatedly accessed by a fluid transfer mechanism and subsequently self-sealed, is detailed. The reaction vessel has an access opening, and the apparatus comprises a cap, a ball which is comprised of a magnetizable material (such as a ferrous metal), and a ring magnet. The cap is sized to fit over the reaction vessel access opening, and has an access port. The cap has an internal surface which faces the reaction vessel, and an external surface, which faces away from the reaction vessel. The ball is sized to fit over the cap access port, such that a portion of the ball seats partially in the cap access port on the cap internal surface, thus sealing the cap access port. According to an aspect of the invention, the ball may be comprised of a ferromagnetic material, or a magnetizable material that is preferably magnetized. The ring magnet produces a magnetic field, and is mounted to the cap on the cap external surface. The ring magnet is spaced from the cap such that the magnetic field is sufficient to hold the ball in the cap access port, and to reseat the ball in the cap access port after the reaction vessel is accessed.

    摘要翻译： 根据本发明的一个方面，详细描述了一种用于自密封反应容器的设备，使得反应容器可以被流体转移机构反复进入并随后自密封。 反应容器具有进入口，该装置包括盖，由可磁化材料（例如黑色金属）构成的球和环形磁体。 盖的尺寸适合于反应容器进入口的上方，并具有进入口。 盖具有面向反应容器的内表面和面向反应容器的外表面。 该球的尺寸设置成适合盖帽进入口，使得球的一部分部分地位于帽内表面上的帽进入口中，从而密封盖进入口。 根据本发明的一个方面，球可以由铁磁材料或优选磁化的可磁化材料构成。 环形磁铁产生磁场，并且安装在盖外表面上的盖上。 环形磁体与盖子间隔开，使得磁场足以将球保持在盖子进入口中，并且在反应容器被访问之后将球重新固定在盖子进入口中。

    Self-sealing apparatus for chemical reaction vessel
    10.
    发明申请
    Self-sealing apparatus for chemical reaction vessel 失效
    化学反应容器自密封装置

    公开(公告)号：US20070068598A1

    公开(公告)日：2007-03-29

    申请号：US11604594

    申请日：2006-11-27

    申请人： Stephan Rodewald

    发明人： Stephan Rodewald

    IPC分类号： B65B1/04

    CPC分类号： B65B7/2835 ,  B01J2219/00315 ,  B01J2219/00335 ,  B01J2219/00344 ,  B01J2219/00346 ,  B01L3/50825 ,  B01L2300/042 ,  B01L2300/049 ,  B01L2400/0616 ,  B01L2400/0633 ,  Y10S141/01

    摘要： According to an aspect of the invention, an apparatus for self-sealing of a reaction vessel, such that the reaction vessel may be repeatedly accessed by a fluid transfer mechanism and subsequently self-sealed, is detailed. The reaction vessel has an access opening, and the apparatus comprises a cap, a ball which is comprised of a magnetizable material (such as a ferrous metal), and a ring magnet. The cap is sized to fit over the reaction vessel access opening, and has an access port. The cap has an internal surface which faces the reaction vessel, and an external surface, which faces away from the reaction vessel. The ball is sized to fit over the cap access port, such that a portion of the ball seats partially in the cap access port on the cap internal surface, thus sealing the cap access port. According to an aspect of the invention, the ball may be comprised of a ferromagnetic material, or a magnetizable material that is preferably magnetized. The ring magnet produces a magnetic field, and is mounted to the cap on the cap external surface. The ring magnet is spaced from the cap such that the magnetic field is sufficient to hold the ball in the cap access port, and to reseat the ball in the cap access port after the reaction vessel is accessed.

    摘要翻译： 根据本发明的一个方面，详细描述了一种用于自密封反应容器的设备，使得反应容器可以被流体转移机构反复进入并随后自密封。 反应容器具有进入口，该装置包括盖，由可磁化材料（例如黑色金属）构成的球和环形磁体。 盖的尺寸适合于反应容器进入口的上方，并具有进入口。 盖具有面向反应容器的内表面和面向反应容器的外表面。 该球的尺寸设置成适合盖帽进入口，使得球的一部分部分地位于帽内表面上的帽进入口中，从而密封盖进入口。 根据本发明的一个方面，球可以由铁磁材料或优选磁化的可磁化材料构成。 环形磁铁产生磁场，并且安装在盖外表面上的盖上。 环形磁体与盖子间隔开，使得磁场足以将球保持在盖子进入口中，并且在反应容器被访问之后将球重新固定在盖子进入口中。