公开(公告)号：US06284120B1

公开(公告)日：2001-09-04

申请号：US09350021

申请日：1999-07-09

申请人： Takahiro Imamura ,  Masaki Katayama

发明人： Takahiro Imamura ,  Masaki Katayama

IPC分类号： C25D700

CPC分类号： C25D7/00 ,  C25D1/00 ,  C25D5/022 ,  G11B5/102 ,  G11B5/3103

摘要： A method of electroplating using a photoresist layer on a conductive seed layer. The photoresist layer defines a column-shaped space. Ridges are formed on the wall surfaces of the photoresist layer surrounding the column-shaped space. The ridges extend from the conductive seed layer to the opening of the column-shaped space. The electrolytic solution drives bubbles out of the column-shaped space, so that the column-shaped space is filled with the electrolytic solution without any cavities. In addition, if hydrogen bubbles are generated in the column-shaped space, the electrolytic solution serves to drive the hydrogen bubbles out of the column-shaped space along the corners of the column-shaped space.

摘要翻译： 在导电种子层上使用​​光致抗蚀剂层的电镀方法。 光致抗蚀剂层限定了柱状空间。 在围绕柱状空间的光致抗蚀剂层的壁表面上形成有脊。 脊从导电种子层延伸到柱状空间的开口。 电解液从柱状空间驱动气泡，使得柱状空间充满电解液而没有任何空腔。 此外，如果在柱状空间中产生氢气泡，则电解液用于沿柱状空间的角部将柱状空间驱动出氢气泡。

公开(公告)号：US06592740B2

公开(公告)日：2003-07-15

申请号：US10150568

申请日：2002-05-17

申请人： James A. Fife

发明人： James A. Fife

IPC分类号： C25D700

CPC分类号： H01G9/0525 ,  C01G1/02 ,  C01G33/00 ,  C01G35/00 ,  C01P2002/70 ,  C01P2004/03 ,  C01P2004/20 ,  C01P2004/50 ,  C01P2004/61 ,  C01P2006/10 ,  C01P2006/12 ,  C01P2006/14 ,  C01P2006/16 ,  C01P2006/40 ,  C01P2006/80 ,  C04B35/495 ,  C04B35/6265 ,  C04B35/6268 ,  C04B35/638 ,  C04B35/64 ,  C04B2235/02 ,  C04B2235/3251 ,  C04B2235/3253 ,  C04B2235/404 ,  C04B2235/5409 ,  C04B2235/6582 ,  C04B2235/72 ,  C04B2235/721 ,  C04B2235/77 ,  C04B2235/79 ,  C22C29/12 ,  C22C2001/1089 ,  H01G9/042 ,  H01G9/052 ,  Y10T29/49002 ,  Y10T428/12819

摘要： Methods to at least partially reduce a niobium oxide are described wherein the process includes heat treating the niobium oxide in the presence of a getter material and in an atmosphere which permits the transfer of oxygen atoms from the niobium oxide to the getter material, and for a sufficient time and at a sufficient temperature to form an oxygen reduced niobium oxide. Niobium oxides and/or suboxides are also described as well as capacitors containing anodes made by fabricating a pellet of niobium oxide and heat treating the pellet in an atmosphere which permits the transfer of oxygen to a getter material, and for a sufficient time and temperature to form an electrode body, and anodizing the electrode body.

摘要翻译： 描述了至少部分还原铌氧化物的方法，其中所述方法包括在吸气剂材料存在下和允许氧原子从氧化铌转移到吸气剂材料的气氛中热处理铌氧化物，并且对于 足够的时间和足够的温度以形成氧还原铌氧化物。 还描述了铌氧化物和/或低氧化物以及含有通过制造氧化铌颗粒制成的阳极的电容器，并且在允许将氧气传递到吸气剂材料的气氛中热处理颗粒，并且在足够的时间和温度下 形成电极体，阳极氧化电极体。

公开(公告)号：US06342146B1

公开(公告)日：2002-01-29

申请号：US09361785

申请日：1999-07-27

申请人： Geronimo Z. Velasquez

发明人： Geronimo Z. Velasquez

IPC分类号： C25D700

CPC分类号： C25D17/00 ,  C25D17/06

摘要： A continuous plating system which is horizontal, allows for submersion of the entire article to be plated, and is useful for alloy plating. The invention provides a link/hinge conveyor system, the conveyor acts as the conductor, numerous processes/baths are possible, and difficult to plate alloys, such as a tin/bismuth plate can be produced. Homogeneous alloys are possible with the present invention. Also disclosed are novel dryer, rinse and reflow systems for use with the continuous plating system.

摘要翻译： 连续的电镀系统是水平的，允许整个被镀物品的浸没，并且可用于合金电镀。 本发明提供一种连接/铰链输送机系统，该输送机作为导体，可以进行许多工艺/浴，并且难以平板化的合金，例如可以生产锡/铋板。 通过本发明，均质合金是可能的。 还公开了用于连续电镀系统的新型干燥器，冲洗和回流系统。

公开(公告)号：US06805785B2

公开(公告)日：2004-10-19

申请号：US10205749

申请日：2002-07-26

申请人： Tetsuo Nanno ,  Yohei Hattori ,  Fumihiko Yoshii

发明人： Tetsuo Nanno ,  Yohei Hattori ,  Fumihiko Yoshii

IPC分类号： C25D700

CPC分类号： H01M4/0442 ,  H01M4/0416 ,  H01M4/28 ,  H01M4/32 ,  H01M4/661 ,  H01M10/30

摘要： The following steps are conducted: preparing a metal salt carried-substrate A by soaking a sintered nickel substrate in an acidic solution containing cobalt ions and at least one metal ions of magnesium ions, iron ions and manganese ions, and drying thus soaked substrate; preparing a hydroxide carried-substrate B by soaking the substrate A in an alkaline solution to deposit cobalt hydroxide and at least one metal hydroxide of magnesium hydroxide, iron hydroxide and manganese hydroxide in the pores and on the surface of the substrate A; obtaining an oxide carried-substrate C by oxidizing the cobalt hydroxide to produce cobalt oxide having a mean cobalt valence of over 2; and obtaining an active material carried-substrate D by soaking the substrate C in a solution containing nickel nitrate dissolved therein, drying thus soaked substrate C, and then soaking thus dried substrate C in an alkaline solution, to fill the active material in the substrate C.

摘要翻译： 进行以下步骤：通过将烧结的镍基底浸入含有钴离子和至少一种镁离子，铁离子和锰离子的金属离子的酸性溶液中并使其干燥而浸渍基底来制备金属盐载带基材A. 通过将碱性溶液浸渍在碱性溶液中，在孔中和基材A的表面上沉积氢氧化钴和至少一种氢氧化镁，氢氧化铁和氢氧化锰的金属氢氧化物，从而制备氢氧化物承载基板B. 通过氧化氢氧化钴得到平均钴价超过2的钴氧化物来获得氧化物承载衬底C; 通过将基板C浸渍在溶解有硝酸镍的溶液中而干燥，浸渍基板C，然后将干燥后的基板C浸渍在碱性溶液中，从而填充基板C中的活性物质 。

公开(公告)号：US06562217B1

公开(公告)日：2003-05-13

申请号：US09403271

申请日：1999-12-27

申请人： Yoshiaki Tanaka ,  Yoshiaki Kodera ,  Manabu Matsubara ,  Kazuhiko Kanki ,  Tatsuo Suzuki ,  Kazuo Ukai

发明人： Yoshiaki Tanaka ,  Yoshiaki Kodera ,  Manabu Matsubara ,  Kazuhiko Kanki ,  Tatsuo Suzuki ,  Kazuo Ukai

IPC分类号： C25D700

CPC分类号： C23C18/1619 ,  C23C18/1653 ,  C23C18/31 ,  C25D5/10 ,  C25D7/00 ,  C25D17/22 ,  H01L21/6715 ,  H01L24/11 ,  H01L24/13 ,  H01L2224/05001 ,  H01L2224/05022 ,  H01L2224/05155 ,  H01L2224/05166 ,  H01L2224/05171 ,  H01L2224/0518 ,  H01L2224/05572 ,  H01L2224/05624 ,  H01L2224/05655 ,  H01L2224/05666 ,  H01L2224/05671 ,  H01L2224/0568 ,  H01L2224/13099 ,  H01L2224/13561 ,  H01L2224/136 ,  H01L2224/13609 ,  H01L2224/16 ,  H01L2924/01005 ,  H01L2924/01006 ,  H01L2924/01013 ,  H01L2924/01015 ,  H01L2924/01019 ,  H01L2924/01022 ,  H01L2924/01023 ,  H01L2924/01024 ,  H01L2924/01025 ,  H01L2924/01027 ,  H01L2924/01029 ,  H01L2924/0103 ,  H01L2924/01032 ,  H01L2924/01033 ,  H01L2924/01042 ,  H01L2924/01046 ,  H01L2924/01047 ,  H01L2924/01049 ,  H01L2924/01051 ,  H01L2924/01061 ,  H01L2924/01074 ,  H01L2924/01078 ,  H01L2924/01079 ,  H01L2924/01082 ,  H01L2924/01322 ,  H01L2924/014 ,  H01L2924/07811 ,  H01L2924/12041 ,  H01L2924/12044 ,  H01L2924/13034 ,  H01L2924/14 ,  H01L2924/19041 ,  H01L2924/19042 ,  H01L2924/19043 ,  H01L2924/3025 ,  Y10T428/26 ,  Y10T428/2991 ,  Y10T428/2998 ,  H01L2924/00 ,  H01L2924/00014 ,  H01L2224/05639 ,  H01L2224/05644 ,  H01L2224/05647 ,  H01L2224/05664 ,  H01L2224/05124 ,  H01L2224/05144 ,  H01L2224/05147 ,  H01L2224/05164 ,  H01L2924/013

摘要： A method for making conductive particles that efficiently permit a plated layer of uniform thickness to be formed over each of the particles without aggregating the particles in a plating liquid. The apparatus comprises: a disk-shaped bottom plate secured to the top part of a vertical drive shaft; a porous body arranged on the upper surface of the outer periphery of the bottom plate and allowing only the plating liquid to pass therethrough; a contact ring arranged on the upper surface of the porous body to conduct electricity; a hollow cover including a truncated cone cover with an opening at its upper central portion and a hollow cylinder of the same diameter as that of the opening attached to the upper end of the truncated cone cover, the upper end portion of the hollow cylinder being folded back on the inner wall side thereof; a rotatable processing chamber formed so as to hold the porous body and the contact ring between the outer periphery of the hollow cover and the bottom plate; a supply pipe to supply the plating liquid from the opening into the processing chamber; a container to receive the plating liquid scattered from the pores of the porous body; a discharge pipe to discharge the plating liquid collected in the container; and an electrode inserted from the opening to contact the plating liquid.

摘要翻译： 一种制造导电颗粒的方法，其有效地允许在每个颗粒上形成均匀厚度的镀层，而不会使电镀液体中的颗粒聚集。 该装置包括：固定到垂直驱动轴的顶部的盘形底板; 多孔体，其布置在所述底板的外周的上表面上，并且仅允许所述电镀液体通过; 接触环，布置在所述多孔体的上表面上以导电; 一个中空的盖子，它包括一个在其上部中心部分具有一个开口的截锥形盖子，以及一个中空圆柱体，该中空圆柱体的直径与安装在截头锥形盖子上端的开口直径相同，中空圆柱体的上端部分被折叠 回到其内壁侧; 可旋转处理室，其形成为将多孔体和接触环保持在中空盖的外周与底板之间; 供给管，用于将电镀液体从开口供给到处理室中; 容纳从多孔体的孔隙散布的镀液的容器; 排出管，用于排出收集在容器中的电镀液; 以及从开口插入以接触电镀液体的电极。

公开(公告)号：US06432292B1

公开(公告)日：2002-08-13

申请号：US09573438

申请日：2000-05-16

申请人： Martin Pinto ,  Stuart Smedley ,  Jeffrey A. Colborn ,  James W. Evans

发明人： Martin Pinto ,  Stuart Smedley ,  Jeffrey A. Colborn ,  James W. Evans

IPC分类号： C25D700

CPC分类号： C25C7/002 ,  C25D7/00

摘要： The present invention relates to a device and method for electrolytic deposition of metals on conducting particles. The conducting particles are completely immersed in a liquid and allowed to flow across a particle contacting surface of a cathode support. The particles flow across the surface and into a reservoir. Electrical contact is made between the negative pole of a DC power supply and the conducting particles. An anode mesh is placed above and parallel to the top face of the particle bed such that the mesh does not touch the particle bed but remains a controlled distance from it. The anode mesh is connected to the positive terminal of the DC power supply. A significant aspect of the present invention is that the device does not require a separator between the particle bed and the anode.

摘要翻译： 本发明涉及金属在导电粒子上电解沉积的装置和方法。 导电颗粒完全浸入液体中并允许流过阴极载体的颗粒接触表面。 颗粒流过表面并进入储层。 在直流电源的负极与导电粒子之间进行电接触。 将阳极网放置在颗粒床的顶面上并平行于颗粒床的顶面，使得网不接触颗粒床，但保持与其的受控距离。 阳极网连接到直流电源的正极。 本发明的重要方面是该装置不需要在颗粒床和阳极之间的分离器。

公开(公告)号：US06537430B1

公开(公告)日：2003-03-25

申请号：US09363037

申请日：1999-07-29

申请人： La Gala Francesco

发明人： La Gala Francesco

IPC分类号： C25D700

CPC分类号： B65G49/0454 ,  C25D17/20

摘要： In at least one bath of the system, tumbling barrels containing pieces to be treated are arranged with their respective longitudinal axes set parallel to or coinciding with the longitudinal axis of the bath and are free to move longitudinally along the bath, supported by idle wheels resting on the edges of the bath. At least one pusher in each bath is free to move for a length longitudinally and engages a frame of a barrel at a trailing position to push the said barrel and possible barrels in front of it in an advance direction. The system may comprise a spray wash in sequential stages.

摘要翻译： 在系统的至少一个浴中，包含要处理的块的滚筒被布置成其各自的纵轴设置成与浴的纵向轴线平行或重合，并且沿着浴自由地纵向移动，由空转轮支撑 在浴缸的边缘。 每个浴缸中的至少一个推动器可自由地纵向移动一段长度并且在拖尾位置处接合桶的框架，以将其推向前方推动所述桶和可能的桶。 该系统可以包括顺序阶段的喷雾洗涤。

公开(公告)号：US06432284B1

公开(公告)日：2002-08-13

申请号：US09684027

申请日：2000-10-06

申请人： Sekharipuram R. Narayanan ,  William Chun ,  Barbara Jeffries-Nakamura ,  Thomas I. Valdez

发明人： Sekharipuram R. Narayanan ,  William Chun ,  Barbara Jeffries-Nakamura ,  Thomas I. Valdez

IPC分类号： C25D700

CPC分类号： C25B1/02 ,  C25B9/10 ,  H01M8/0656 ,  Y02P20/134

摘要： A device for electrolysis of an aqueous solution of an organic fuel. The electrolyte is a solid-state polymer membrane with anode and cathode catalysts on both surfaces for electro-oxidization and electro-reduction. A low-cost and portable hydrogen generator can be made based on the device with organic fuels such as methanol.

公开(公告)号：US06299744B1

公开(公告)日：2001-10-09

申请号：US09123957

申请日：1998-07-28

申请人： Sekharipuram R. Narayanan ,  William Chun ,  Barbara Jeffries-Nakamura ,  Thomas I. Valdez

发明人： Sekharipuram R. Narayanan ,  William Chun ,  Barbara Jeffries-Nakamura ,  Thomas I. Valdez

IPC分类号： C25D700

CPC分类号： C25B1/02 ,  C25B9/10 ,  H01M8/0656 ,  Y02P20/134

摘要： A device for electrolysis of an aqueous solution of an organic fuel. The electrolyte is a solid-state polymer membrane with anode and cathode catalysts on both surfaces for electro-oxidization and electro-reduction. A low-cost and portable hydrogen generator can be made based on the device with organic fuels such as methanol.

摘要翻译： 一种电解有机燃料水溶液的装置。 电解质是一种固态聚合物膜，在两面用阳极和阴极催化剂进行电氧化和电还原。 可以使用具有有机燃料如甲醇的装置制造低成本且便携式的氢发生器。

公开(公告)号：US06332967B1

公开(公告)日：2001-12-25

申请号：US09448612

申请日：1999-11-23

申请人： Raghu N. Bhattacharya

发明人： Raghu N. Bhattacharya

IPC分类号： C25D700

CPC分类号： H01L39/2451 ,  C04B35/4512 ,  C04B35/6264 ,  C04B35/62645 ,  C04B2235/3208 ,  C04B2235/3213 ,  C04B2235/3215 ,  C04B2235/3241 ,  C04B2235/3298 ,  C04B2235/443 ,  C04B2235/96 ,  C23C28/322 ,  C23C28/345 ,  C23C28/3455 ,  C23C28/42 ,  C25D5/10 ,  C25D5/50 ,  C25D9/08

摘要： Methods for preparing high quality superconducting oxide precursors which are well suited for further oxidation and annealing to form superconducting oxide films. The method comprises forming a multilayered superconducting precursor on a substrate by providing an electrodeposition bath comprising an electrolyte medium and a substrate electrode, and providing to the bath a plurality of precursor metal salts which are capable of exhibiting superconducting properties upon subsequent treatment. The superconducting precursor is then formed by electrodepositing a first electrodeposited (ED) layer onto the substrate electrode, followed by depositing a layer of silver onto the first electrodeposited (ED) layer, and then electrodepositing a second electrodeposited (ED) layer onto the Ag layer. The multilayered superconducting precursor is suitable for oxidation at a sufficient annealing temperature in air or an oxygen-containing atmosphere to form a crystalline superconducting oxide film.

摘要翻译： 制备高质量超导氧化物前体的方法，其非常适于进一步氧化和退火以形成超导氧化物膜。 该方法包括通过提供包含电解质介质和底物电极的电沉积浴在基底上形成多层超导前体，并向浴中提供多种能够在后续处理时显示超导性质的前体金属盐。 然后通过将第一电沉积（ED）层电沉积到衬底电极上，然后在第一电沉积（ED）层上沉积银层，然后将第二电沉积（ED）层电沉积到Ag层上而形成超导前体 。 多层超导前体适合于在空气或含氧气氛中以足够的退火温度进行氧化以形成结晶超导氧化物膜。