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    Method for forming guanidine group on carbon nanotube, method for attaching carbon nanotube having guanidine group formed thereon to substrate and carbon nanotube and substrate formed thereby
    4.
    发明专利
    Method for forming guanidine group on carbon nanotube, method for attaching carbon nanotube having guanidine group formed thereon to substrate and carbon nanotube and substrate formed thereby 有权
    形成碳纳米管组合物的方法，连接其形成的基团的碳纳米管的碳纳米管和碳纳米管和形成的基体的方法

    公开(公告)号：JP2006206568A

    公开(公告)日：2006-08-10

    申请号：JP2005142928

    申请日：2005-05-16

    申请人： Samsung Electro-Mechanics Co Ltd ,  サムソン エレクトロ−メカニックス カンパニーリミテッド.

    发明人： LEE HAI SUNG

    IPC分类号： C07C277/08 ,  B82B3/00 ,  C01B31/02 ,  C07C279/24

    CPC分类号： B82Y30/00 ,  D01F11/12 ,  D01F11/14 ,  Y10S977/745 ,  Y10S977/746 ,  Y10S977/847

    摘要： PROBLEM TO BE SOLVED: To provide a method for forming guanidine groups not chelate-reacting with metal cations existing in solutions on a carbon nanotube, and to provide a method for forming guanidine groups on a carbon nanotube as a method for more increasing the dispersibility of carbon nanotube. SOLUTION: A method for attaching carbon nanotubes having guanidine groups formed thereon to a substrate comprises a step for coating the substrate with a crown ether-having polymer, a step for drying the crown ether-having polymer layer coated on the substrate in a semi-dry state, and a step for coating the semi-dry polymer layer with a solution containing the carbon nanotubes having the guanidine groups formed thereon. The carbon nanotubes having the guanidine groups formed thereon and produced by the method are uniformly dispersed in solutions by the hydrogen bond of the guanidine groups to the hydrogen bond-formable solvent molecules. The guanidine groups are selectively bound to the crown ether, and the property is utilized to vertically arrange the carbon nanotubes having the guanidine groups formed thereon on the substrate at a constant distance. COPYRIGHT: (C)2006,JPO&NCIPI

    摘要翻译： 待解决的问题：提供形成与碳纳米管上溶液中存在的金属阳离子不螯合反应的胍基的方法，并提供在碳纳米管上形成胍基的方法，作为更多增加的方法 碳纳米管的分散性。 解决方案：将其上形成有胍基的碳纳米管连接到基底上的方法包括用具有冠醚的聚合物涂覆基底的步骤，用于干燥涂覆在基底上的冠醚聚合物层的步骤 半干态，以及用含有形成有胍基的碳纳米管的溶液涂布半干聚合物层的步骤。 通过该方法制造的具有胍基的碳纳米管通过胍基的氢键均匀地分散在溶液中，形成氢键形成的溶剂分子。 胍基选择性地结合到冠醚上，并且利用这种性质将其上形成有胍基的碳纳米管在恒定距离上垂直排列在基底上。 版权所有（C）2006，JPO＆NCIPI

    ORGANIC BASE PRODUCING AGENT
    10.
    发明专利
    ORGANIC BASE PRODUCING AGENT 失效

    公开(公告)号：JPH11269138A

    公开(公告)日：1999-10-05

    申请号：JP7191598

    申请日：1998-03-20

    申请人： MITSUBISHI PAPER MILLS LTD

    发明人： HIZADATE YOSHIHARU ,  KUBOTA KIYOKO

    IPC分类号： C07C271/12 ,  B41M5/26 ,  B41M5/337 ,  C07C255/13 ,  C07C271/20 ,  C07C271/28 ,  C07C279/18 ,  C07C279/24 ,  C07C317/18 ,  C09K3/00

    摘要： PROBLEM TO BE SOLVED: To obtain a new compound useful as an organic base precursor having the rapidity of producing a base at the time of heating compatible with the stability during the preservation. SOLUTION: This compound is represented by formula I [R to R are each H, an alkyl, an alkenyl, an aralkyl or an aryl; Z is a substituent group having a value of σ of >=0 when defined by the Hammett's equation; [(i)+(j)] is 3 and (i) is 1 or 2] or formula II (R to R are each same as R to R ), e.g. a compound represented by formula III. The compound represented by formula I is obtained by charging stearylamine, triethylamine and chloroform into a flask equipped with a stirrer, dropping 1.5 g of 1-chloro-2-methyl-2-propyl chloroformate thereinto under cooling with ice, continuing the stirring for 2 hr, then diluting the reactional solution with chloroform, washing the diluted reactional solution with water, dehydrating the washed solution, subsequently distilling off the chloroform under a reduced pressure and recrystallizing the prepared colorless powder from a mixed solvent of an ether with n-hexane.