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    Production of phenol
    23.
    发明授权
    Production of phenol 失效
    生产苯酚

    公开(公告)号：US06441251B1

    公开(公告)日：2002-08-27

    申请号：US09946711

    申请日：2001-09-04

    Applicant: Doron Levin ,  Jose G. Santiesteban ,  Lei Zhang

    Inventor： Doron Levin ,  Jose G. Santiesteban ,  Lei Zhang

    IPC: C07C3708

    CPC classification number: C07C37/08 ,  B01J29/0308 ,  B01J37/0209 ,  B01J2229/12 ,  B01J2229/14 ,  B01J2229/34 ,  C07C45/53 ,  Y02P20/52 ,  Y02P20/588 ,  C07C49/08 ,  C07C39/04

    Abstract: A process for producing phenol and acetone from cumene hydroperoxide is described in which the cumene hydroperoxide is contacted with a solid-acid catalyst comprising an inorganic, porous, crystalline material, designated as M41S, exhibiting, after calcination, an x-ray diffraction pattern with at least one peak at a d-spacing greater than about 18 Angstrom Units with a relative intensity of 100 and a benzene adsorption capacity of greater than 15 grams of benzene per 100 grams of said material at 50 torr and 25° C., wherein said material comprises sulfonate functionality.

    Abstract translation: 描述了由氢过氧化枯烯生产苯酚和丙酮的方法，其中氢过氧化枯烯与包含称为M41S的无机多孔结晶材料的固体酸催化剂接触，在焙烧后表现出x射线衍射图与 在50托和25℃下，相对强度为100的d间距的至少一个峰值大于约18埃，相对强度为100，苯吸附能力大于15克苯/ 100克所述材料，其中所述 材料包括磺酸盐官能团。

    Olefin epoxidation catalysts
    24.
    发明授权
    Olefin epoxidation catalysts 有权
    烯烃环氧化催化剂

    公开(公告)号：US6114551A

    公开(公告)日：2000-09-05

    申请号：US412773

    申请日：1999-10-04

    Applicant: Doron Levin ,  Clarence D. Chang ,  Shifang Luo ,  Jose G. Santiesteban ,  James C. Vartuli

    Inventor： Doron Levin ,  Clarence D. Chang ,  Shifang Luo ,  Jose G. Santiesteban ,  James C. Vartuli

    IPC: B01J29/89 ,  C01B39/06 ,  C07D301/19 ,  C07D303/04 ,  C07D305/00

    CPC classification number: C07D301/19 ,  B01J29/89 ,  B01J2229/16 ,  B01J2229/183 ,  B01J2229/32 ,  B01J29/7038

    Abstract: A method of synthesizing an olefin epoxidation catalyst comprises the step of treating a porous crystalline aluminosilicate material having an X-ray diffraction pattern including d-spacing maxima at 12.4.+-.0.25, 6.9.+-.0.15, 3.57.+-.0.07 and 3.42.+-.0.07 Angstrom, such as MCM-22, with a dealuminating agent under conditions effective to remove framework aluminium from the material and produce a dealuminated product. The dealuminated product is then treated with a titanium-containing material under conditions effective to insert titanium into the dealuminated product and produce a titanium-containing, dealuminated catalyst composition.The resultant catalyst is useful in the epoxidation of olefins, such as propylene and cyclohexene, with hydrogen peroxide and organic hydroperoxides.

    Abstract translation: 合成烯烃环氧化催化剂的方法包括以下步骤：处理多晶结晶硅铝酸盐材料，该多晶结晶硅铝酸盐材料具有包含d间距最大值的X射线衍射图，为12.4 +/- 0.25,6.9 +/- 0.15,3.57 +/- 0.07和3.42 +/- 0.07埃，例如MCM-22，在有效从材料中除去骨架铝并产生脱铝产品的条件下用脱铝剂。 然后在有效地将钛插入脱铝产品中并且生产含钛脱铝催化剂组合物的条件下，用含钛材料处理脱铝产品。 得到的催化剂可用于烯烃如丙烯和环己烯与过氧化氢和有机氢过氧化物的环氧化。

    Transalkylation of heavy aromatic hydrocarbon feedstocks
    27.
    发明授权
    Transalkylation of heavy aromatic hydrocarbon feedstocks 有权
    重芳香烃原料的烷基转移

    公开(公告)号：US08183424B2

    公开(公告)日：2012-05-22

    申请号：US12973358

    申请日：2010-12-20

    Applicant: Doron Levin ,  April D. Ross ,  James H. Beech, Jr.

    Inventor： Doron Levin ,  April D. Ross ,  James H. Beech, Jr.

    IPC: C07C6/12

    CPC classification number: B01J8/04 ,  B01J29/064 ,  B01J29/072 ,  B01J29/076 ,  B01J29/44 ,  B01J29/46 ,  B01J29/7034 ,  B01J29/7669 ,  B01J35/0006 ,  B01J35/023 ,  B01J37/0009 ,  B01J37/20 ,  B01J2229/42 ,  C07C6/12 ,  C07C2529/42 ,  Y02P20/52 ,  C07C15/08

    Abstract: In a process for producing xylene by transalkylation of a C9+ aromatic hydrocarbon feedstock with a C6 and/or C7 aromatic hydrocarbon, the C9+ aromatic hydrocarbon feedstock, at least one C6 and/or C7 aromatic hydrocarbon and hydrogen are contacted with a first catalyst comprising (i) a first molecular sieve having a Constraint Index in the range of about 3 to about 12 and (ii) at least first and second different metals or compounds thereof of Groups 6 to 12 of the Periodic Table of the Elements. Contacting with the first catalyst is conducted under conditions effective to dealkylate aromatic hydrocarbons in the feedstock containing C2+ alkyl groups and to saturate C2+ olefins formed so as to produce a first effluent. At least a portion of the first effluent is then contacted with a second catalyst comprising a second molecular sieve having a Constraint Index less than 3 under conditions effective to transalkylate C9+ aromatic hydrocarbons with said at least one C6-C7 aromatic hydrocarbon to form a second effluent comprising xylene.

    Abstract translation: 在通过C 9 +芳族烃原料与C 6和/或C 7芳烃的烷基转移生产二甲苯的方法中，C 9 +芳烃原料，至少一种C 6和/或C 7芳烃和氢与第一催化剂接触，所述第一催化剂包含（ i）具有在约3至约12范围内的约束指数的第一分子筛和（ii）至少元素周期表第6至12族的第一和第二不同金属或其化合物。 与第一催化剂接触在有效地使含有C 2 +烷基的原料中芳族烃脱烷基化并使形成的C 2 +烯烃饱和以产生第一流出物的条件下进行。 然后至少一部分第一流出物与包含第二分子筛的第二催化剂接触，该第二催化剂在有效使C 9+芳族烃与所述至少一种C 6 -C 7芳族烃烷基转移的条件下具有小于3的约束指数，以形成第二流出物 包括二甲苯。

    Transalkylation of Heavy Aromatic Hydrocarbon Feedstocks
    28.
    发明申请
    Transalkylation of Heavy Aromatic Hydrocarbon Feedstocks 有权
    重芳香烃原料的烷基转移

    公开(公告)号：US20110190556A1

    公开(公告)日：2011-08-04

    申请号：US12973358

    申请日：2010-12-20

    Applicant: Doron Levin ,  April D. Ross ,  James H. Beech, JR.

    Inventor： Doron Levin ,  April D. Ross ,  James H. Beech, JR.

    IPC: C07C2/00 ,  B01J35/02

    CPC classification number: B01J8/04 ,  B01J29/064 ,  B01J29/072 ,  B01J29/076 ,  B01J29/44 ,  B01J29/46 ,  B01J29/7034 ,  B01J29/7669 ,  B01J35/0006 ,  B01J35/023 ,  B01J37/0009 ,  B01J37/20 ,  B01J2229/42 ,  C07C6/12 ,  C07C2529/42 ,  Y02P20/52 ,  C07C15/08

    Abstract: In a process for producing xylene by transalkylation of a C9+ aromatic hydrocarbon feedstock with a C6 and/or C7 aromatic hydrocarbon, the C9+ aromatic hydrocarbon feedstock, at least one C6 and/or C7 aromatic hydrocarbon and hydrogen are contacted with a first catalyst comprising (i) a first molecular sieve having a Constraint Index in the range of about 3 to about 12 and (ii) at least first and second different metals or compounds thereof of Groups 6 to 12 of the Periodic Table of the Elements. Contacting with the first catalyst is conducted under conditions effective to dealkylate aromatic hydrocarbons in the feedstock containing C2+ alkyl groups and to saturate C2+ olefins formed so as to produce a first effluent. At least a portion of the first effluent is then contacted with a second catalyst comprising a second molecular sieve having a Constraint Index less than 3 under conditions effective to transalkylate C9+ aromatic hydrocarbons with said at least one C6-C7 aromatic hydrocarbon to form a second effluent comprising xylene.

    Abstract translation: 在通过C 9 +芳族烃原料与C 6和/或C 7芳烃的烷基转移生产二甲苯的方法中，C 9 +芳烃原料，至少一种C 6和/或C 7芳烃和氢与第一催化剂接触，所述第一催化剂包含（ i）具有在约3至约12范围内的约束指数的第一分子筛和（ii）至少元素周期表第6至12族的第一和第二不同金属或其化合物。 与第一催化剂接触在有效地使含有C 2 +烷基的原料中芳族烃脱烷基化并使形成的C 2 +烯烃饱和以产生第一流出物的条件下进行。 然后至少一部分第一流出物与包含第二分子筛的第二催化剂接触，该第二催化剂在有效使C 9+芳族烃与所述至少一种C 6 -C 7芳族烃烷基转移的条件下具有小于3的约束指数，以形成第二流出物 包括二甲苯。

    Heavy Aromatics Processing Catalyst and Process of Using the Same
    30.
    发明申请
    Heavy Aromatics Processing Catalyst and Process of Using the Same 有权
    重芳烃加工催化剂及其使用方法

    公开(公告)号：US20090112034A1

    公开(公告)日：2009-04-30

    申请号：US12249279

    申请日：2008-10-10

    Applicant: Doron Levin

    Inventor： Doron Levin

    IPC: C07C5/52

    CPC classification number: C07C6/126 ,  B01J29/44 ,  B01J29/48 ,  B01J29/7469 ,  B01J29/80 ,  B01J35/0006 ,  B01J35/026 ,  B01J37/18 ,  B01J2229/186 ,  B01J2229/42 ,  C07C2529/44 ,  C07C2529/74 ,  Y02P20/52 ,  C07C15/08

    Abstract: This disclosure relates to a catalyst system adapted for transalkylation a C9+ aromatic feedstock with a C6-C7 aromatic feedstock, comprising: (a) a first catalyst comprising a first molecular sieve having a Constraint Index in the range of 3-12 and 0.01 to 5 wt. % of at least one source of a first metal element of Groups 6-10; and (b) a second catalyst comprising a second molecular sieve having a Constraint Index less than 3 and 0 to 5 wt. % of at least one source of a second metal element of Groups 6-10, wherein the weight ratio of the first catalyst over the second catalyst is in the range of 5:95 to 75:25 and wherein the first catalyst is located in front of the second catalyst when they are brought into contacting with the C9+ aromatic feedstock and the C6-C7 aromatic feedstock in the present of hydrogen.

    Abstract translation: 本公开涉及一种适于使C 9+芳族原料与C 6 -C 7芳族原料进行烷基转移的催化剂体系，其包含：（a）第一催化剂，其包含第一分子筛，其约束指数为3-12和0.01至5 重量 至少一个第6-10族第一金属元素源的％; 和（b）包含第二分子筛的第二催化剂，所述第二分子筛具有小于3和0-5重量％的约束指数。 至少一种第6-10族第二金属元素源的％，其中第一催化剂与第二催化剂的重量比在5:95至75:25的范围内，其中第一催化剂位于前面 的第二催化剂当它们与C9 +芳族原料和当前氢气中的C6-C7芳族原料接触时。

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