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21.发明授权Malononitrile-derivative anion salts, and their uses as ionic conducting materials 有权丙二腈衍生物阴离子盐及其用作离子导电材料公开(公告)号：US06576159B1
公开(公告)日：2003-06-10
申请号：US09638793
申请日：2000-08-09
IPC分类号： H01B112
CPC分类号： B01J31/0224 , B01J31/0215 , B01J31/0222 , B01J31/0225 , B01J31/0227 , B01J31/0235 , B01J31/0239 , B01J31/0247 , B01J31/0251 , B01J31/0252 , B01J31/0267 , B01J31/0271 , B01J31/0281 , B01J31/0288 , B01J31/0289 , B01J31/04 , B01J31/06 , B01J31/068 , B01J31/124 , B01J31/1815 , B01J31/2208 , B01J2231/122 , B01J2231/14 , B01J2231/326 , B01J2231/341 , B01J2231/348 , B01J2231/4205 , B01J2231/543 , B01J2531/35 , B01J2531/824 , C07B37/02 , C07B37/12 , C07C45/46 , C07C45/69 , C07C67/00 , C07C255/10 , C07C255/17 , C07C255/27 , C07C255/46 , C07C255/65 , C07C257/14 , C07C311/03 , C07C311/04 , C07C311/09 , C07C311/48 , C07C317/04 , C07C317/08 , C07C317/14 , C07C317/22 , C07C317/24 , C07C317/34 , C07C317/44 , C07C2601/10 , C07C2602/42 , C07D207/452 , C07D213/76 , C07D219/10 , C07D231/18 , C07D233/90 , C07D239/60 , C07D241/42 , C07D249/04 , C07D249/10 , C07D249/12 , C07D251/70 , C07D277/64 , C07D277/82 , C07D285/125 , C07D285/135 , C07D285/15 , C07D285/16 , C07D303/34 , C07D307/54 , C07D307/64 , C07D311/52 , C07D311/58 , C07D311/82 , C07D319/06 , C07D333/16 , C07D333/24 , C07D405/06 , C07D409/12 , C07D417/10 , C07D417/14 , C07F17/02 , C08F4/04 , C08G65/3344 , C09B69/00 , C09B69/02 , C09B69/10 , G02F1/1525 , G02F2001/151 , H01B1/122 , H01B1/128 , H01G9/022 , H01G9/038 , H01G11/02 , H01G11/62 , H01M4/00 , H01M4/02 , H01M4/131 , H01M4/133 , H01M4/134 , H01M4/382 , H01M4/405 , H01M4/48 , H01M4/485 , H01M4/505 , H01M4/525 , H01M4/5815 , H01M4/5825 , H01M4/60 , H01M4/625 , H01M4/661 , H01M6/00 , H01M6/04 , H01M6/164 , H01M6/166 , H01M6/168 , H01M6/181 , H01M6/183 , H01M10/052 , H01M10/0525 , H01M10/0565 , H01M10/0567 , H01M10/0568 , Y02E60/13 , Y10S430/127 , Y10T29/49108 , Y10T428/2918 , C07C49/84 , C07C49/553
摘要： The invention is related to ionic compounds, derivatives of malononitrile, in which the anionic load has been displaced. An ionic compound disclosed by the invention includes an anionic portion combined with at least one cationic portion M+m in sufficient number to ensure overall electronic neutrality; the compound is further comprised of M as a hydroxonium, a nitrosonium NO+, an ammonium —NH4+, a metallic cation with the valence m, an organic cation with the valence m, or an organometallic cation with the valence m. The anionic portion corresponds to one of the formulas RD—Y—C(C≡N)2− or Z—C(C≡N)2− in which Z is an electroattractive group, RD is an organic radical, and Y is a carbonyl, a thiocarbonyl, a sulfonyl, a sulfinyl, or a phosphonyl. The compounds can be used notably for ionic conducting materials, electronic conducting materials, colorants, and the catalysis of various chemical reactions.
摘要翻译： 本发明涉及离子化合物，其中阴离子负载已被置换的丙二腈衍生物。 本发明公开的离子化合物包括与足够数量的至少一个阳离子部分M + m结合的阴离子部分以确保整体电子中性; 该化合物还包含作为氢氧化物的M，亚硝鎓NO +，铵NH4 +，价数m的金属阳离子，价数m的有机阳离子或价数m的有机金属阳离子。 阴离子部分对应于其中Z为电吸引基团的RD-YC（C = N）2-或ZC（C = N）2-）之一，RD为有机基团，Y为羰基，硫代羰基 ，磺酰基，亚磺酰基或膦酰基。 该化合物特别用于离子导电材料，电子导电材料，着色剂和各种化学反应的催化。
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22.发明授权Heterocyclic aromatic anion salts, and their uses as ionic conducting materials 有权杂环芳族阴离子盐及其作为离子导电材料的用途公开(公告)号：US06365068B1
公开(公告)日：2002-04-02
申请号：US09609362
申请日：2000-06-30
IPC分类号： H01B112
CPC分类号： B01J31/0224 , B01J31/0215 , B01J31/0222 , B01J31/0225 , B01J31/0227 , B01J31/0235 , B01J31/0239 , B01J31/0247 , B01J31/0251 , B01J31/0252 , B01J31/0267 , B01J31/0271 , B01J31/0281 , B01J31/0288 , B01J31/0289 , B01J31/04 , B01J31/06 , B01J31/068 , B01J31/124 , B01J31/1815 , B01J31/2208 , B01J2231/122 , B01J2231/14 , B01J2231/326 , B01J2231/341 , B01J2231/348 , B01J2231/4205 , B01J2231/543 , B01J2531/35 , B01J2531/824 , C07B37/02 , C07B37/12 , C07C45/46 , C07C45/69 , C07C67/00 , C07C255/10 , C07C255/17 , C07C255/27 , C07C255/46 , C07C255/65 , C07C257/14 , C07C311/03 , C07C311/04 , C07C311/09 , C07C311/48 , C07C317/04 , C07C317/08 , C07C317/14 , C07C317/22 , C07C317/24 , C07C317/34 , C07C317/44 , C07C2601/10 , C07C2602/42 , C07D207/452 , C07D213/76 , C07D219/10 , C07D231/18 , C07D233/90 , C07D239/60 , C07D241/42 , C07D249/04 , C07D249/10 , C07D249/12 , C07D251/70 , C07D277/64 , C07D277/82 , C07D285/125 , C07D285/135 , C07D285/15 , C07D285/16 , C07D303/34 , C07D307/54 , C07D307/64 , C07D311/52 , C07D311/58 , C07D311/82 , C07D319/06 , C07D333/16 , C07D333/24 , C07D405/06 , C07D409/12 , C07D417/10 , C07D417/14 , C07F17/02 , C08F4/04 , C08G65/3344 , C09B69/00 , C09B69/02 , C09B69/10 , G02F1/1525 , G02F2001/151 , H01B1/122 , H01B1/128 , H01G9/022 , H01G9/038 , H01G11/02 , H01G11/62 , H01M4/00 , H01M4/02 , H01M4/131 , H01M4/133 , H01M4/134 , H01M4/382 , H01M4/405 , H01M4/48 , H01M4/485 , H01M4/505 , H01M4/525 , H01M4/5815 , H01M4/5825 , H01M4/60 , H01M4/625 , H01M4/661 , H01M6/00 , H01M6/04 , H01M6/164 , H01M6/166 , H01M6/168 , H01M6/181 , H01M6/183 , H01M10/052 , H01M10/0525 , H01M10/0565 , H01M10/0567 , H01M10/0568 , Y02E60/13 , Y10S430/127 , Y10T29/49108 , Y10T428/2918 , C07C49/84 , C07C49/553
摘要： The invention relates to ionic compounds in which the anionic load has been displaced, and the uses of these compounds. A compound disclosed by the invention comprises an anionic portion combined with at least one cationic portion M+m in sufficient numbers to ensure overall electronic neutrality. The anionic portion is comprised of one of the groups (A) and (B): wherein Y1, Y2, Y3, Y4 and Y5 represent a carbonyl group, a sulfonyl group, a thiocarbonyl group, a thionyl group, a —C(═NCN)— or a —C(═C(CN)2)— group; Z represents an electroattractive radical; each of the substituents, RA, RB, RC and RD represents independently of one another a monovalent or divalent organic radical or is part of a polymer chain, with at least one of the substituents RC and RD being a perfluorinated radical. The compounds can be used especially for ionic conducting materials, electronic conducting materials, colorants, and the catalysis of various chemical reactions.
摘要翻译： 本发明涉及其中阴离子负载已被置换的离子化合物，以及这些化合物的用途。 本发明公开的化合物包含与足够数量的至少一个阳离子部分M + m结合的阴离子部分以确保整体电子中性。 阴离子部分由（A）和（B）中的一个组成：其中Y1，Y2，Y3，Y4和Y5表示羰基，磺酰基，硫代羰基，亚硫酰基，-C（= NCN） - 或-C（= C（CN）2） - 基团; Z表示电吸引基团; 每个取代基RA，RB，RC和RD彼此独立地表示一价或二价有机基团或者是聚合物链的一部分，其中至少一个取代基RC和RD是全氟化基团。 该化合物可以特别用于离子导电材料，电子导电材料，着色剂和各种化学反应的催化。
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公开(公告)号：US5916475A
公开(公告)日：1999-06-29
申请号：US537944
申请日：1995-11-21
IPC分类号： C01B21/093 , C07C307/00 , C07C311/48 , C07C317/04 , C07C317/24 , C07F9/36 , C07F9/53 , H01B1/12 , H01B1/20 , H01G9/02 , H01G9/025 , H01G11/02 , H01G11/20 , H01G11/54 , H01G11/56 , H01G11/60 , H01G11/62 , H01M4/66 , H01M6/16 , H01M6/18 , H01M10/05 , H01M10/052 , H01M10/0525 , H01M10/0565 , H01M10/0567 , H01M10/0568 , H01M10/0569 , H01M10/36 , C08L7/02
CPC分类号： H01G9/038 , C01B21/0935 , C07C307/00 , H01B1/122 , H01G11/20 , H01G11/56 , H01M10/052 , H01M10/0565 , H01M10/0567 , H01M10/0568 , H01M10/0569 , H01M6/181 , H01M10/0525 , Y02E60/13
摘要： An ionically conductive material which contains at least one ionic compound in solution in an aprotic solvent, wherein the ionic compound is selected from the group consisting of compounds of the formulae (1/mM).sup.61 ((ZY)2N).sup..crclbar., (1/mM).sup..sym. ((ZY).sub.3 C).sup..crclbar., or (1/mM).sup..sym. ((ZY).sub.2 CQ).sup..crclbar., wherein M, Z, Y and Q are as defined herein.
摘要翻译： PCT No.PCT / FR95 / 00343 Sec。 371日期：1995年11月21日 102（e）1995年11月21日日期PCT 1995年3月21日PCT PCT。 公开号WO95 / 26056 日期1995年9月28日在非质子溶剂中含有溶液中的至少一种离子化合物的离子导电材料，其中离子化合物选自式（1 / mM）61（（ZY）2 N）化合物， （ - ），（1）/（+）（（ZY）3C）（ - ）或（1 / mM）（+）（（ZY）2CQ）（ - ），其中M，Z，Y和Q为 如本文所定义。
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24.发明授权Li4Ti5O12, Li(4-α)ZαTi5O12or Li4ZβTi(5-β)O12 particles, processes for obtaining same and their use in electrochemical generators 有权Li4Ti5O12，Li（4-α）ZαTi5O12或Li4Z＆bgr; Ti（5-＆bgr）O12颗粒，其获得方法及其在电化学发生器中的应用公开(公告)号：US09077031B2
公开(公告)日：2015-07-07
申请号：US13360173
申请日：2012-01-27
申请人： Karim Zaghib , Michel Gauthier , Fernand Brochu , Abdelbast Guerfi , Monique Masse , Michel Armand
发明人： Karim Zaghib , Michel Gauthier , Fernand Brochu , Abdelbast Guerfi , Monique Masse , Michel Armand
IPC分类号： B05D5/12 , H01M4/485 , B82Y30/00 , C01G23/00 , H01G9/00 , H01M4/04 , H01M4/131 , H01M4/136 , H01M4/36 , H01M4/58 , H01M4/62 , H01M4/74 , H01M10/0525 , H01M4/02 , H01M4/505 , H01M4/525 , H01M4/66 , H01M10/0562 , H01M10/0565
CPC分类号： H01M4/485 , B82Y30/00 , C01G23/003 , C01G23/005 , C01P2002/77 , C01P2002/88 , C01P2004/03 , C01P2004/64 , C01P2006/40 , H01G9/155 , H01G11/04 , H01G11/46 , H01M4/02 , H01M4/0471 , H01M4/131 , H01M4/136 , H01M4/366 , H01M4/505 , H01M4/525 , H01M4/5825 , H01M4/623 , H01M4/625 , H01M4/661 , H01M4/745 , H01M10/0525 , H01M10/0562 , H01M10/0565 , H01M2300/004 , H01M2300/0082 , H01M2300/0085 , Y02E60/122 , Y02E60/13 , Y02P70/54 , Y10T428/2982
摘要： Synthesis process for new particles of Li4Ti5O12, Li(4-α)ZαTi5O12 or Li4ZβTi(5-β)O12, wherein β is >0 and ≦0.5, α is a number >0 and ≦0.33, Z is a source of at least one metal, preferably chosen from the group made up of Mg, Nb, Al, Zr, Ni, Co. These particles coated with a layer of carbon notably exhibit electrochemical properties that are particularly interesting as components of anodes and/or cathodes in electrochemical generators. The process may involve the steps of a) preparing a dispersion of a mixture of TiOx—LizY-carbon, wherein x is a number between 1 and 2, z is 1 or 2, and Y is a radical chosen among CO3, OH, O and TiO3 or a mixture thereof; and 2) heating of the dispersion, preferably to a temperature of between about 400° C. and about 1000° C.
摘要翻译： Li4Ti5O12，Li（4-α）ZαTi5O12或Li4Z＆bgr; Ti（5-＆bgr）O12的新颗粒的合成工艺，其中＆bgr; 是> 0和＆nlE; 0.5，α是数> 0和＆nlE; 0.33，Z是至少一种金属的源，优选选自由Mg，Nb，Al，Zr，Ni，Co组成的组。 涂覆有碳层的颗粒特别表现出电化学特性，其特别令人感兴趣的是作为电化学发生器中阳极和/或阴极的组分。 该方法可以包括以下步骤：a）制备TiOx-LizY-碳的混合物的分散体，其中x是1和2之间的数，z是1或2，Y是选自CO 3，OH，O 和TiO 3或其混合物; 和2）分散体的加热，优选至约400℃至约1000℃的温度
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25.发明授权Polymers obtained from monomers allowing a sequential polymerization, and their use for preparing ionic conductors 有权从允许顺序聚合的单体获得的聚合物及其用于制备离子导体的用途公开(公告)号：US08512899B2
公开(公告)日：2013-08-20
申请号：US12118483
申请日：2008-05-09
CPC分类号： C08F226/06 , C07C43/15 , C08G65/14 , C08G65/16 , C08G65/20 , C08G65/22 , C08G65/337 , H01B1/122 , H01M4/131 , H01M4/133 , H01M4/136 , H01M4/1393 , H01M4/1397 , H01M4/485 , H01M4/505 , H01M4/525 , H01M4/5815 , H01M4/5825 , H01M6/164 , H01M10/052 , H01M10/0525 , H01M10/0565 , Y10S525/901 , Y10S525/919
摘要： The present invention concerns polymers obtained by anionic initiation and bearing functions that can be activated by cationic initiations that are not reactive in the presence of anionic polymerization initiators. The presence of such cationic initiation functions allow an efficient cross-linking of the polymer after molding, particularly in the form of a thin film. It is thus possible to obtain polymers with well-defined properties in terms of molecular weight and cross-linking density. The polymers of the present invention are capable of dissolving ionic compounds inducing a conductivity for the preparation of solid electrolytes.
摘要翻译： 本发明涉及通过阴离子引发而获得的聚合物，并且可通过在阴离子聚合引发剂存在下不具有反应性的阳离子引发而活化。 这种阳离子引发功能的存在允许聚合物在模制之后，特别是薄膜形式的有效交联。 因此，可以获得在分子量和交联密度方面具有明确特性的聚合物。 本发明的聚合物能够溶解诱导用于制备固体电解质的导电性的离子化合物。
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26.发明授权Process for preparing electroactive insertion compounds and electrode materials obtained therefrom 有权制备电活性插入化合物的方法和由其获得的电极材料公开(公告)号：US08273481B2
公开(公告)日：2012-09-25
申请号：US13217719
申请日：2011-08-25
CPC分类号： C01B25/45 , C01B25/37 , H01M4/136 , H01M4/1397 , H01M4/366 , H01M4/525 , H01M4/5825 , H01M4/625 , H01M10/052 , H01M2004/028
摘要： A process for preparing an at least partially lithiated transition metal oxyanion-based lithium-ion reversible electrode material, which includes providing a precursor of said lithium-ion reversible electrode material, heating said precursor, melting same at a temperature sufficient to produce a melt including an oxyanion containing liquid phase, cooling said melt under conditions to induce solidification thereof and obtain a solid electrode that is capable of reversible lithium ion deinsertion/insertion cycles for use in a lithium battery. Also, lithiated or partially lithiated oxyanion-based-lithium-ion reversible electrode materials obtained by the aforesaid process.
摘要翻译： 一种制备至少部分锂化的过渡金属氧阴离子的锂离子可逆电极材料的方法，其包括提供所述锂离子可逆电极材料的前体，加热所述前体，在足以产生熔体的温度下熔化，包括 含有氧阴离子的液相，在条件下冷却所述熔体以诱导其固化，并获得能够在锂电池中使用的可逆锂离子去插入/插入循环的固体电极。 而且，通过上述方法获得的锂化或部分锂化的氧阴离子 - 锂离子可逆电极材料。
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27.发明申请公开(公告)号：US20120028121A1
公开(公告)日：2012-02-02
申请号：US13217719
申请日：2011-08-25
CPC分类号： C01B25/45 , C01B25/37 , H01M4/136 , H01M4/1397 , H01M4/366 , H01M4/525 , H01M4/5825 , H01M4/625 , H01M10/052 , H01M2004/028
摘要： A process for preparing an at least partially lithiated transition metal oxyanion-based lithium-ion reversible electrode material, which includes providing a precursor of said lithium-ion reversible electrode material, heating said precursor, melting same at a temperature sufficient to produce a melt including an oxyanion containing liquid phase, cooling said melt under conditions to induce solidification thereof and obtain a solid electrode that is capable of reversible lithium ion deinsertion/insertion cycles for use in a lithium battery. Also, lithiated or partially lithiated oxyanion-based-lithium-ion reversible electrode materials obtained by the aforesaid process.
摘要翻译： 一种制备至少部分锂化的过渡金属氧阴离子的锂离子可逆电极材料的方法，其包括提供所述锂离子可逆电极材料的前体，加热所述前体，在足以产生熔体的温度下熔化，包括 含有氧阴离子的液相，在条件下冷却所述熔体以诱导其固化，并获得能够在锂电池中使用的可逆锂离子去插入/插入循环的固体电极。 而且，通过上述方法获得的锂化或部分锂化的氧阴离子 - 锂离子可逆电极材料。
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28.发明申请公开(公告)号：US20110062380A1
公开(公告)日：2011-03-17
申请号：US12953077
申请日：2010-11-23
CPC分类号： C01B25/45 , C01B25/37 , H01M4/136 , H01M4/1397 , H01M4/366 , H01M4/525 , H01M4/5825 , H01M4/625 , H01M10/052 , H01M2004/028
摘要： A process for preparing an at least partially lithiated transition metal oxyanion-based lithium−ion reversible electrode material, which includes providing a precursor of said lithium−ion reversible electrode material, heating said precursor, melting same at a temperature sufficient to produce a melt including an oxyanion containing liquid phase, cooling said melt under conditions to induce solidification thereof and obtain a solid electrode that is capable of reversible lithium ion deinsertion/insertion cycles for use in a lithium battery. Also, lithiated or partially lithiated oxyanion-based-lithium−ion reversible electrode materials obtained by the aforesaid process.
摘要翻译： 一种制备至少部分锂化的过渡金属氧阴离子的锂离子可逆电极材料的方法，其包括提供所述锂离子可逆电极材料的前体，加热所述前体，在足以产生熔体的温度下熔化，包括 含有氧阴离子的液相，在条件下冷却所述熔体以诱导其固化，并获得能够在锂电池中使用的可逆锂离子去插入/插入循环的固体电极。 而且，通过上述方法获得的锂化或部分锂化的氧阴离子 - 锂离子可逆电极材料。
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29.发明申请Polymers Obtained From Monomers Allowing A Sequential Polymerization, And Their Use For Preparing Ionic Conductors 有权从单体获得的聚合物允许顺序聚合，以及它们用于制备离子导体的用途公开(公告)号：US20080213661A1
公开(公告)日：2008-09-04
申请号：US12118483
申请日：2008-05-09
CPC分类号： C08F226/06 , C07C43/15 , C08G65/14 , C08G65/16 , C08G65/20 , C08G65/22 , C08G65/337 , H01B1/122 , H01M4/131 , H01M4/133 , H01M4/136 , H01M4/1393 , H01M4/1397 , H01M4/485 , H01M4/505 , H01M4/525 , H01M4/5815 , H01M4/5825 , H01M6/164 , H01M10/052 , H01M10/0525 , H01M10/0565 , Y10S525/901 , Y10S525/919
摘要： The present invention concerns polymers obtained by anionic initiation and bearing functions that can be activated by cationic initiations that are not reactive in the presence of anionic polymerization initiators. The presence of such cationic initiation functions allow an efficient cross-linking of the polymer after moulding, particularly in the form of a thin film. It is thus possible to obtain polymers with well-defined properties in terms of molecular weight and cross-linking density. The polymers of the present invention are capable of dissolving ionic compounds inducing a conductivity for the preparation of solid electrolytes.
摘要翻译： 本发明涉及通过阴离子引发而获得的聚合物，并且可通过在阴离子聚合引发剂存在下不具有反应性的阳离子引发而活化。 这种阳离子引发功能的存在允许聚合物在模制之后，特别是薄膜形式的有效交联。 因此，可以获得在分子量和交联密度方面具有明确特性的聚合物。 本发明的聚合物能够溶解诱导用于制备固体电解质的导电性的离子化合物。
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30.发明申请公开(公告)号：US20070194158A1
公开(公告)日：2007-08-23
申请号：US11790020
申请日：2007-04-23
申请人： Karim Zaghib , Michel Gauthier , Gabrielle Nadeau , Abdelbast Guerfi , Monique Masse , Fernand Brochu , Michel Armand
发明人： Karim Zaghib , Michel Gauthier , Gabrielle Nadeau , Abdelbast Guerfi , Monique Masse , Fernand Brochu , Michel Armand
CPC分类号： H01M4/583 , C01B32/215 , H01M4/133 , H01M10/0525
摘要： The present invention relates to the physical or chemical specific purification of natural mineral graphite. This purification is preferably applied to the surface of natural graphite in order to allow the formation of a passivation film during the first electrical discharge or the insertion of lithium in the graphite when the latter is used in a lithium-ion cell. The grinding to a small size before purification allows the optimization of the distribution of the particles, resulting in a more uniform electrode. This grinding is carried out in the presence of the natural impurities of the graphite that play the role of a micro-abrasive and result in a hardness of the graphite that increases its mechanical properties.
摘要翻译： 本发明涉及天然矿物石墨的物理或化学特异性纯化。 优选将该纯化施加到天然石墨的表面，以便在锂离子电池中使用时，在石墨中的第一次放电或锂的插入期间允许形成钝化膜。 在纯化之前研磨至小尺寸允许优化颗粒的分布，导致更均匀的电极。 这种研磨是在发生微磨料作用的石墨的天然杂质的存在下进行的，并导致石墨的硬度增加其机械性能。
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