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    Synthetic mesoporous material with radially assembled nanotubes
    42.
    发明授权
    Synthetic mesoporous material with radially assembled nanotubes 有权
    具有径向组装的纳米管的合成介孔材料

    公开(公告)号：US07005118B2

    公开(公告)日：2006-02-28

    申请号：US10620770

    申请日：2003-07-17

    Applicant: Eduardo Terres Rojas ,  Jose Manuel Dominguez Esquivel

    Inventor： Eduardo Terres Rojas ,  Jose Manuel Dominguez Esquivel

    IPC: C01B33/12 ,  C01B33/20 ,  C01B33/26

    CPC classification number: B82Y30/00 ,  B01J20/103 ,  B01J20/28019 ,  B01J20/28057 ,  B01J20/28083 ,  B01J21/08 ,  B01J29/0308 ,  B01J29/041 ,  B01J35/1023 ,  B01J35/1028 ,  B01J35/1042 ,  B01J35/1061 ,  B01J35/1085 ,  C01B37/005 ,  C01B37/02 ,  Y10S977/778

    Abstract: This invention relates to a new composition of high surface area materials suitable for adsorption of both organic and inorganic species and as a component of catalysts useful for the transformation of hydrocarbons into a variety of products. These materials are composed by mesoporous spherical particles that have large sorption capacity, as demonstrated by the uptake of nitrogen at 78 K having a diameter of 0.1 to 1.0 microns, a mean pore diameter of 2.0 nm to 4.0 nm, a surface area of 750 to 1050 m2/g and a mean pore volume of 0.75 to 1.0 ml/g. The typical inner structure is composed of nanotubes having diameters around 3.5 nm aligned along the radius of the spherical particles, with surface areas around 1,000 m2/g, depending on the surfactant (C16H33N(CH3)3Br) to co-solvent (CnH2n+1OH, where n=2,3, or CH3COCH3) molar ratio. Elliptical particles are also obtained with cylindrical pores running along or across the major axis of the particles having very high surface areas of up to 1561 m2/g and a mean pore diameter of 2.0 to 4.0 nm. The walls of the nanotubes are pure silica or a composition of silica with M(III)Ox where M is a trivalent metal such as Al, Ga, or lanthanide.

    Abstract translation: 本发明涉及适于吸附有机和无机物质的高表面积材料的新组合物，以及用于将烃转化为多种产物的催化剂组分。 这些材料由具有大吸附能力的介孔球形颗粒组成，如通过在78K下吸收直径为0.1至1.0微米的氮气，平均孔径为2.0nm至4.0nm，表面积为750至 1050m 2 / g，平均孔体积为0.75〜1.0ml / g。 典型的内部结构由沿着球形颗粒的半径排列的直径约3.5nm的纳米管组成，其表面积约为1000m 2 / g，这取决于表面活性剂（C 16 C 16） N（CH 3）3 Br）与共溶剂（C n H n H 3） 其中n = 2,3或CH 3 COCH 3 3摩尔比。 也可以获得椭圆形颗粒，其圆柱形孔沿着或横过具有高达1561m 2 / g的非常高的表面积和2.0至4.0nm的平均孔径的颗粒的长轴。 纳米管的壁是纯二氧化硅或具有M（III）O x x的二氧化硅组合物，其中M是三价金属如Al，Ga或镧系元素。

    Synthetic mesoporous material with radially assembled nanotubes
    46.
    发明申请
    Synthetic mesoporous material with radially assembled nanotubes 有权
    具有径向组装的纳米管的合成介孔材料

    公开(公告)号：US20040052714A1

    公开(公告)日：2004-03-18

    申请号：US10620770

    申请日：2003-07-17

    Applicant: Instituto Mexicano del Petroleo

    Inventor： Eduardo Terres Rojas ,  Jose Manuel Dominguez Esquivel

    IPC: C01B033/26 ,  C01B033/18

    CPC classification number: B82Y30/00 ,  B01J20/103 ,  B01J20/28019 ,  B01J20/28057 ,  B01J20/28083 ,  B01J21/08 ,  B01J29/0308 ,  B01J29/041 ,  B01J35/1023 ,  B01J35/1028 ,  B01J35/1042 ,  B01J35/1061 ,  B01J35/1085 ,  C01B37/005 ,  C01B37/02 ,  Y10S977/778

    Abstract: This invention relates to a new composition of high surface area materials suitable for adsorption of both organic and inorganic species and as a component of catalysts useful for the transformation of hydrocarbons into a variety of products. These materials are composed by mesoporous spherical particles that have large sorption capacity, as demonstrated by the uptake of nitrogen at 78 K having a diameter of 0.1 to 1.0 microns, a mean pore diameter of 2.0 nm to 4.0 nm, a surface area of 750 to 1050 m2/g and a mean pore volume of 0.75 to 1.0 ml/g. The typical inner structure is composed of nanotubes having diameters around 3.5 nm aligned along the radius of the spherical particles, with surface areas around 1,000 m2/g, depending on the surfactant (C16H33N(CH3)3 Br) to co-solvent (CnH2nnull1OH, where nnull2,3, or CH3COCH3) molar ratio. Elliptical particles are also obtained with cylindrical pores running along or across the major axis of the particles having very high surface areas of up to 1561 m2/g and a mean pore diameter of 2.0 to 4.0 nm. The walls of the nanotubes are pure silica or a composition of silica with M(III)Ox where M is a trivalent metal such as Al, Ga, or lanthanide.

    Abstract translation: 本发明涉及适于吸附有机和无机物质的高表面积材料的新组合物，以及用于将烃转化为多种产物的催化剂组分。 这些材料由具有大吸附能力的介孔球形颗粒组成，如通过在78K下吸收直径为0.1至1.0微米的氮气，平均孔径为2.0nm至4.0nm，表面积为750至 1050m 2 / g，平均孔体积为0.75〜1.0ml / g。 典型的内部结构由直径约3.5nm的纳米管组成，沿着球形颗粒的半径排列，其表面积约为1000m 2 / g，取决于表面活性剂（C16H33N（CH3）3 Br））与共溶剂 （C n H 2n + 1OH，其中n = 2,3或CH 3 COCH 3）摩尔比。 还可以获得椭圆形颗粒，其圆柱形孔沿着或横过具有高达1561m 2 / g的非常高的表面积的颗粒的长轴或者平均孔径为2.0至4.0nm。 纳米管的壁是纯二氧化硅或具有M（III）Ox的二氧化硅的组合物，其中M是三价金属如Al，Ga或镧系元素。

    Palladium catalyst and process for producing ether
    47.
    发明授权
    Palladium catalyst and process for producing ether 失效
    钯催化剂及其制备方法

    公开(公告)号：US06657089B1

    公开(公告)日：2003-12-02

    申请号：US10111920

    申请日：2002-05-01

    Applicant: Atsushi Nagasawa ,  Munehisa Okutsu ,  Tomohito Kitsuki

    Inventor： Atsushi Nagasawa ,  Munehisa Okutsu ,  Tomohito Kitsuki

    IPC: C07C4101

    CPC classification number: B01J29/043 ,  B01J29/041 ,  C07C41/28 ,  C07C43/13

    Abstract: This invention relates to a palladium catalyst comprising a mesoporous aluminosilicate which has been treated with ammonia or a salt thereof, and palladium supported on said mesoporous aluminosilicate; and also to a process for producing an ether, which comprises reacting a cyclic acetal and hydrogen in the presence of the palladium catalyst.

    Abstract translation: 本发明涉及包含用氨或其盐处理的介孔硅铝酸盐和负载在所述介孔硅铝酸盐上的钯的钯催化剂; 并且还涉及一种制备醚的方法，其包括在钯催化剂存在下使环缩醛和氢反应。

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