公开(公告)号：US20170165632A1

公开(公告)日：2017-06-15

申请号：US15371835

申请日：2016-12-07

Applicant: Blacktrace Holdings Limited

Inventor： Philip Homewood ,  Mark Gilligan ,  Andrew Lovatt ,  Paul Crisp ,  Ben Taylor ,  Hannah Kenyon ,  Mike Hawes

IPC: B01J19/24 ,  B01J19/00

CPC classification number: B01J19/2415 ,  B01J19/0013 ,  B01J19/006 ,  B01J19/0093 ,  B01J19/242 ,  B01J19/243 ,  B01J2219/00063 ,  B01J2219/00085 ,  B01J2219/00094 ,  B01J2219/00772 ,  B01J2219/00792 ,  B01J2219/24

Abstract: A reactor device (100) for reaction fluid comprising a reaction vessel (102) comprising: an end cap (104) comprising at least one passage (112) for the reaction fluid; and at least one tube (116) which extends through the reaction vessel (102). The reaction vessel is operable to receive a control fluid outside the at least one tube (116) for controlling the temperature inside the at least one tube (116). A manifold (200) is connectable to the end cap (104) and comprises at least one channel (206) for reaction fluid. An outlet (208) from the manifold (200) is in fluid communication with the tube (116). The end cap (104) has a thermal conductivity of greater than 1 watt per square meter kelvin to provide a thermal coupling between the control fluid and the manifold (200).

公开(公告)号：US20170136438A1

公开(公告)日：2017-05-18

申请号：US15325605

申请日：2015-07-29

Applicant: NATIONAL UNIVERSITY CORPORATION SHINSHU UNIVERSITY ,  SHOWA DENKO K.K.

Inventor： Hisanao USAMI ,  Yasushi KURODA ,  Mitsuhiro IMAIZUMI

IPC: B01J19/12 ,  B01J35/00 ,  B01J21/06

CPC classification number: B01J19/122 ,  B01J19/0093 ,  B01J21/063 ,  B01J35/0013 ,  B01J35/004 ,  B01J2219/00792 ,  B01J2219/00797 ,  B01J2219/00824 ,  B01J2219/00826 ,  B01J2219/00831 ,  B01J2219/00835 ,  B01J2219/0086 ,  B01J2219/00934 ,  B01J2219/0892 ,  C02F1/325 ,  C02F1/725 ,  C02F2101/345 ,  C02F2101/36 ,  C02F2305/10 ,  Y02W10/37

Abstract: A fluid flow-through device and a photochemical reactor. The fluid flow-through device (1) includes an outer tube (2) having an outer surface (21) and an inner surface (22); and an inner tube (3) having an outer surface (31) and an inner surface (32), the inner tube being disposed inside the outer tube and forming a channel of a fluid by the inner surface of the outer tube and the outer surface, with a distance between the inner surface of the outer tube and the outer surface of the inner tube in a thickness direction of the outer tube being from 100 nm to 5 mm. The photochemical reactor includes the fluid flow-through device and a photocatalyst disposed on at least one surface of the inner surface of the outer tube and the outer surface of the inner tube.

公开(公告)号：US20170113938A1

公开(公告)日：2017-04-27

申请号：US15310725

申请日：2015-05-13

Applicant: LG CHEM, LTD.

Inventor： Yoo Seok KIM ,  Jeong Kyu KIM ,  JinHyoung YOO ,  JungWoo LEE ,  Eunsu JANG

IPC: C01B33/107 ,  B01J19/24 ,  B01J10/00

CPC classification number: C01B33/10763 ,  B01J8/008 ,  B01J8/085 ,  B01J10/00 ,  B01J19/0093 ,  B01J19/2415 ,  B01J2208/00176 ,  B01J2208/0053 ,  B01J2208/00787 ,  B01J2219/00792 ,  B01J2219/00822 ,  B01J2219/00855 ,  B01J2219/0086 ,  B01J2219/00867 ,  B01J2219/00869 ,  B01J2219/00873 ,  B01J2219/00889 ,  B01J2219/182 ,  C01B33/1071 ,  C01B33/10736

Abstract: The present invention relates to an apparatus for producing trichlorosilane from tetrachlorosilane in an efficient manner. The apparatus includes an inlet through which reaction raw materials including a metal silicon powder dispersed in liquid tetrachlorosilane enter, a hole through which a gaseous reaction raw material is fed, an outlet through which reaction products including trichlorosilane exit, a tubular reactor in which the reaction raw materials entering through the inlet react with each other during flow, and means for impeding the flow of the fluids to cause collision of the fluids during flow.

公开(公告)号：US09421536B2

公开(公告)日：2016-08-23

申请号：US14394929

申请日：2013-04-17

Applicant: DSM IP ASSETS B.V.

Inventor： Werner Bonrath

IPC: B01J35/04 ,  B01J10/00 ,  B01J12/00 ,  B01J19/00 ,  B01J19/02 ,  B01J19/24 ,  B01J23/44 ,  B01J35/00 ,  C07C29/17 ,  C10G45/40 ,  B01J23/889 ,  B01J23/883 ,  B01J23/885 ,  B01J23/89 ,  B01J37/02 ,  C07C67/283 ,  C10G3/00 ,  B01J23/60 ,  B01J21/04 ,  B01J23/06

CPC classification number: B01J35/04 ,  B01J10/007 ,  B01J12/007 ,  B01J19/0093 ,  B01J19/02 ,  B01J19/2415 ,  B01J19/2485 ,  B01J21/04 ,  B01J23/06 ,  B01J23/44 ,  B01J23/60 ,  B01J23/883 ,  B01J23/885 ,  B01J23/8892 ,  B01J23/8993 ,  B01J35/006 ,  B01J37/0201 ,  B01J2219/00094 ,  B01J2219/00792 ,  B01J2219/00822 ,  B01J2219/00824 ,  B01J2219/00835 ,  B01J2219/0086 ,  B01J2219/00873 ,  B01J2219/0277 ,  B01J2219/2403 ,  B01J2219/2411 ,  B01J2219/2428 ,  B01J2219/2435 ,  B01J2219/2437 ,  B01J2219/2444 ,  C07C29/17 ,  C07C67/283 ,  C10G3/47 ,  C10G3/50 ,  C10G45/40 ,  Y02P30/20 ,  C07C33/03 ,  C07C33/02 ,  C07C69/145

Abstract: The present invention relates to a device for treatment of material transported through the device comprising at least one porous element consisting of specific solid metallic structure which allows cross-flow of the material through the porous element and wherein the porous element is coated by a non-acidic metal oxide which is impregnated by palladium (Pd).

Abstract translation: 本发明涉及一种用于处理通过该装置输送的材料的装置，包括至少一个由特定固体金属结构组成的多孔元件，该多孔元件允许材料跨过多孔元件的交叉流动，并且其中多孔元件被非金属结构涂覆， 用钯（Pd）浸渍的酸性金属氧化物。

公开(公告)号：US09370760B2

公开(公告)日：2016-06-21

申请号：US14114389

申请日：2011-05-13

Applicant: Yukako Asano ,  Shigenori Togashi

Inventor： Yukako Asano ,  Shigenori Togashi

IPC: B01J19/12 ,  B01J19/00

CPC classification number: B01J19/0093 ,  B01J19/122 ,  B01J2219/00792 ,  B01J2219/00806 ,  B01J2219/00808 ,  B01J2219/00819 ,  B01J2219/00831 ,  B01J2219/00867 ,  B01J2219/00873 ,  B01J2219/00934 ,  B01J2219/00943

Abstract: A microreactor for photoreactions includes a housing upper part, a lid plate made of a material that allows transmission of light, a flow path plate made of a material that suppresses light reflection and has a high thermal conductivity, and a housing lower part. Light is applied through a window of the housing upper part and the lid plate to a flow path of the flow path plate. The lid plate made of the material that allows transmission of light and the flow path plate made of the material that suppresses light reflection and has a high thermal conductivity are welded each other to form an integrated body.

Abstract translation: 用于光反应的微反应器包括壳体上部，由允许透光的材料制成的盖板，由抑制光反射并具有高导热性的材料制成的流路板和壳体下部。 通过壳体上部和盖板的窗口将光照射到流路板的流路。 由允许透光的材料制成的盖板和由抑制光反射并具有高导热性的材料制成的流路板彼此焊接以形成一体。

公开(公告)号：US20160122263A1

公开(公告)日：2016-05-05

申请号：US14891963

申请日：2014-05-29

Applicant: SAUDI BASIC INDUSTRIES CORPORATION

Inventor： Zeeshan H. Nawaz ,  Khaja Aliuddin Sharief ,  Faisal Baksh ,  Abdullah Al-Qahtani

IPC: C07C5/333 ,  B01J23/42 ,  B01J23/26 ,  B01J21/04 ,  B01J23/14

CPC classification number: C07C5/3332 ,  B01J8/0025 ,  B01J8/0055 ,  B01J8/0207 ,  B01J8/0242 ,  B01J8/0415 ,  B01J8/0442 ,  B01J8/0492 ,  B01J8/26 ,  B01J19/0093 ,  B01J21/04 ,  B01J23/14 ,  B01J23/26 ,  B01J23/42 ,  B01J2208/00513 ,  B01J2208/0053 ,  B01J2219/00792 ,  B01J2219/00835 ,  B01J2219/0086 ,  B01J2219/00873 ,  C07C5/3337 ,  C07C2521/04 ,  C07C2521/08 ,  C07C2521/12 ,  C07C2523/14 ,  C07C2523/26 ,  C07C2523/42 ,  C10G49/007 ,  C10G49/04 ,  C10G49/06 ,  C10G49/16 ,  C10G2300/1081 ,  C10G2300/42 ,  C10G2400/20 ,  Y02P20/132 ,  Y02P20/142 ,  Y02P20/52 ,  C07C11/02 ,  C07C11/06 ,  C07C11/08

Abstract: Disclosed herein are methods for dehydrogenation of alkanes to olefins by co-injecting the alkane feed with hydrogen. The present methods provide the improved feed conversion, desired product selectivity, total olefins in product stream, and lower catalyst deactivation rate.

Abstract translation: 本文公开了通过用氢气共同注入烷烃进料将烷烃脱氢成烯烃的方法。 本方法提供改进的进料转化率，所需产物选择性，产物流中的总烯烃和较低的催化剂失活速率。

公开(公告)号：US20160045843A1

公开(公告)日：2016-02-18

申请号：US14829259

申请日：2015-08-18

Applicant: Howard A. STONE ,  Jiang LI ,  Haosheng CHEN

Inventor： Howard A. STONE ,  Jiang LI ,  Haosheng CHEN

IPC: B01D17/04 ,  C03C17/30 ,  C03C17/00 ,  B01J19/24 ,  B01L3/00

CPC classification number: B01D17/04 ,  B01F5/0647 ,  B01F13/0071 ,  B01J19/0093 ,  B01J2219/00783 ,  B01J2219/00792 ,  B01J2219/00828 ,  B01J2219/00831 ,  B01J2219/00833 ,  B01J2219/0084 ,  B01J2219/0086 ,  B01J2219/00889 ,  B01J2219/00903 ,  B01J2219/00907 ,  B01L3/502707 ,  B01L3/502769 ,  B01L2200/0673 ,  B01L2300/0838 ,  B01L2300/0864 ,  B01L2300/161 ,  B01L2400/0487 ,  C03C17/004 ,  C03C17/30 ,  C03C2217/76

Abstract: Emulsion breaking and phase separation is achieved by droplet adhesion. An emulsion breaking device includes a channel having distinct adjacent zones with distinctly different surface wettability characteristics, namely, solvophilic and solvophobic surfaces. The device is positioned such that the upstream portion of the device is configured to be wetted by the continuous phase of the emulsion, and the downstream portion of the device is configured to be wetted by the dispersed phase of the emulsion. As the emulsion flows from the upstream zone to the downstream zone, the change in surface wettability characteristics promotes adhesion of the dispersed phase as the dispersed phase wets the surface of the downstream portion of the channel, which results in breaking of the emulsion. Subsequent collection of the broken emulsion in a collection vessel results in separation of the disparate phases to facilitate their recapture and recycling.

Abstract translation: 乳液破碎和相分离通过液滴粘附实现。 乳液破碎装置包括具有不同相邻区域的通道，其具有明显不同的表面润湿特性，即溶剂性和疏油性表面。 该装置被定位成使得装置的上游部分构造成被乳液的连续相润湿，并且装置的下游部分被构造成被乳液的分散相润湿。 当乳液从上游区流向下游区时，表面润湿特性的变化促进分散相的粘附，因为分散相润湿通道下游部分的表面，导致乳液破裂。 随后在收集容器中收集破碎的乳液，导致不同相的分离，以促进它们的再捕获和再循环。

公开(公告)号：US20160016141A1

公开(公告)日：2016-01-21

申请号：US14870786

申请日：2015-09-30

Applicant: HITACHI, LTD.

Inventor： Yukako ASANO ,  Shigenori TOGASHI

IPC: B01J19/00 ,  B01J19/12

CPC classification number: B01J19/0093 ,  B01J19/122 ,  B01J2219/00792 ,  B01J2219/00806 ,  B01J2219/00808 ,  B01J2219/00819 ,  B01J2219/00831 ,  B01J2219/00867 ,  B01J2219/00873 ,  B01J2219/00934 ,  B01J2219/00943

Abstract: A microreactor for photoreactions includes a housing upper part, a lid plate made of a material that allows transmission of light, a flow path plate made of a material that suppresses light reflection and has a high thermal conductivity, and a housing lower part. Light is applied through a window of the housing upper part and the lid plate to a flow path of the flow path plate. The lid plate made of the material that allows transmission of light and the flow path plate made of the material that suppresses light reflection and has a high thermal conductivity are welded each other to form an integrated body.

Abstract translation: 用于光反应的微反应器包括壳体上部，由允许透光的材料制成的盖板，由抑制光反射并具有高导热性的材料制成的流路板和壳体下部。 通过壳体上部和盖板的窗口将光照射到流路板的流路。 由允许透光的材料制成的盖板和由抑制光反射并具有高导热性的材料制成的流路板彼此焊接以形成一体。

公开(公告)号：US20150376111A1

公开(公告)日：2015-12-31

申请号：US14768391

申请日：2014-04-25

Applicant: BASF SE

Inventor： Ralf BOEHLING ,  Michael HAYER ,  Alwin REHFINGER ,  Michael SCHELPER ,  Johann-Peter MELDER ,  Martin ERNST ,  Joaquim Henrique TELES

IPC: C07C201/08

CPC classification number: C07C201/08 ,  B01J19/0093 ,  B01J2219/00792 ,  B01J2219/00795 ,  B01J2219/00824 ,  B01J2219/00826 ,  B01J2219/00831 ,  B01J2219/00835 ,  B01J2219/00842 ,  B01J2219/0086 ,  B01J2219/00867 ,  B01J2219/00873 ,  B01J2219/00889 ,  B01J2219/00891 ,  Y02P20/582 ,  C07C205/02

Abstract: The invention relates to a process for preparing nitroalkanes by reaction of at least one alkane with at least one nitrating agent in the gas phase, wherein the nitration is carried out in a microstructured reaction zone having parallel channels having hydraulic diameters of less than 2.5 mm and a total specific internal surface area of more than 1600 m2/m3 and the alkane and the nitrating agent are conveyed under a pressure of from 1 bar to 20 bar through the reaction zone and reacted at a temperature of from 150° C. to 650° C. and the reaction products are cooled downstream of the reaction zone and discharged and the at least one nitrating agent is introduced over from two to ten introduction points along the reaction zone.

Abstract translation: 本发明涉及通过在气相中至少一种烷烃与至少一种硝化剂反应来制备硝基烷烃的方法，其中硝化在具有水力直径小于2.5mm的平行通道的微结构反应区中进行，以及 超过1600m 2 / m 3的总比表面积和烷烃和硝化剂在1巴-20巴的压力下通过反应区输送，并在150℃至650℃的温度下反应 并且反应产物在反应区的下游冷却并排出，并且将至少一种硝化剂沿着反应区引入二至十个引入点。

公开(公告)号：US20150375209A1

公开(公告)日：2015-12-31

申请号：US14749441

申请日：2015-06-24

Applicant: UNIVERSITY OF WYOMING

Inventor： Maohong FAN ,  Tiberiu POPA

IPC: B01J23/72 ,  B01J8/02 ,  B01J37/03 ,  B01J37/08 ,  C07C29/149 ,  B01J37/04

CPC classification number: B01J23/72 ,  B01J19/0093 ,  B01J29/064 ,  B01J29/14 ,  B01J29/46 ,  B01J35/023 ,  B01J37/035 ,  B01J37/036 ,  B01J37/08 ,  B01J2208/02 ,  B01J2219/00792 ,  B01J2219/00835 ,  B01J2219/00873 ,  B01J2219/00909 ,  B01J2219/00916 ,  B01J2219/00961 ,  B01J2219/00963 ,  B01J2219/00986 ,  B01J2523/00 ,  C07C29/149 ,  Y02P20/52 ,  C07C31/202 ,  B01J2523/17 ,  B01J2523/41

Abstract: Embodiments described herein generally relate to hydrogenation catalysts, syntheses of hydrogenation catalysts, and apparatus and methods for hydrogenation. Methods for forming a hydrogenation catalyst may include mixing a silica generating precursor with a copper precursor and adding an ammonium salt to an end pH of between about 5 to about 9. Methods for hydrogenating an oxalate may include forming a reaction mixture by flowing a hydrogenation catalyst to a reactor, flowing a hydrogen source to the reactor, and flowing an oxalate to the reactor, wherein the hydrogenation catalyst has a particle size between about 10 nm to about 40 nm. Methods may further include reacting the oxalate to form ethylene glycol.

Abstract translation: 本文所述的实施方案通常涉及氢化催化剂，氢化催化剂的合成，以及用于氢化的装置和方法。 形成氢化催化剂的方法可以包括将二氧化硅生成前体与铜前体混合并加入铵盐至约5至约9的终止pH。用于氢化草酸盐的方法可包括通过使氢化催化剂 到一个反应器中，将氢源流到反应器中，并使草酸盐流到反应器中，其中氢化催化剂的粒度在约10nm到约40nm之间。 方法还可包括使草酸酯反应形成乙二醇。