Operation method for dezincification plant

    公开(公告)号:US09751035B2

    公开(公告)日:2017-09-05

    申请号:US14760066

    申请日:2013-12-10

    CPC classification number: B01D37/04 C01G9/08 C22B1/00 C22B23/043 C22B23/0461

    Abstract: At the beginning of a dezincification plant used in a dezincification step in a hydrometallurgical method for nickel, a decrease throughout the dezincification plant is controlled to prevent a decrease in production volume and a cake layer is formed on a filter cloth provided to a filter device inside the dezincification plant. At the beginning of dezincification plant, a slurry containing a formed zinc sulfide is supplied to a filter for filtration and separation, an adjustment is performed in which the flow rate of the slurry is increased to reach a target flow rate in a time T2 which satisfies the following relational expression 3×T1≦T2≦5×T1, where T1 represents the time between starting a slurry supply and attaining the target flow rate in the case of transferring the slurry at the maximum liquid transfer capacity of a pump configured to transfer the slurry.

    POLYCRYSTALLINE CHALCOGENIDE CERAMIC MATERIAL
    77.
    发明申请
    POLYCRYSTALLINE CHALCOGENIDE CERAMIC MATERIAL 审中-公开
    多晶氯化铝陶瓷材料

    公开(公告)号:US20130271610A1

    公开(公告)日:2013-10-17

    申请号:US13447921

    申请日:2012-04-16

    Abstract: The invention relates to a polycrystalline IR transparent material produced by sintering chalcogenide powder, e.g., ZnS powder, using hot uniaxial pressing followed by hot isostatic pressing. The microstructure of the material described in this disclosure is much finer than that found in material produced using the state of the art process. By using a powder with a particle size fine enough to improve sintering behavior but coarse enough to prevent a lowering of the wurtzite-sphalerite transition temperature, a highly transparent material with improved strength is created without degrading the optical properties. A high degree of transparency is achieved during hot pressing by applying pressure after the part has reached a desired temperature. This allows some degree of plastic deformation and prevents rapid grain growth which can entrap porosity. The crystallographic twins created during this process further inhibit grain growth during hot isostatic pressing.

    Abstract translation: 本发明涉及一种多晶IR透明材料,其通过使用热单轴压制,然后通过热等静压来烧结硫族化物粉末,例如ZnS粉末而制备。 在本公开中描述的材料的微观结构比使用现有技术方法生产的材料中的微观结构更精细。 通过使用粒度足够细的粉末来改善烧结行为,但是足够粗的以防止纤锌矿 - 闪锌矿转变温度的降低,产生具有改善的强度的高度透明的材料,而不降低光学性能。 在部件达到期望温度之后通过施加压力在热压期间实现高度的透明度。 这允许一定程度的塑性变形并且防止能够截留多孔性的快速晶粒生长。 在该过程中产生的晶体双胞胎在热等静压过程中进一步抑制晶粒生长。

    Hydrometallurgical process for a nickel oxide ore
    78.
    发明授权
    Hydrometallurgical process for a nickel oxide ore 有权
    氧化镍矿石的湿法冶金工艺

    公开(公告)号:US08343447B2

    公开(公告)日:2013-01-01

    申请号:US12458677

    申请日:2009-07-20

    CPC classification number: C22B23/043 C22B23/0461

    Abstract: A hydrometallurgical process for a nickel oxide ore comprising obtaining an aqueous solution of crude nickel sulfate by high pressure acid leaching of a nickel oxide ore; obtaining a zinc free final solution by sulfurization of the solution; obtaining a waste solution; and scrubbing hydrogen sulfide gas from an exhaust gas. The process is characterized by at least one of the following operations: Adjusting the total volume (m3) of a sulfurization reactor to a ratio of 0.2-0.9 (m3/kg/h) relative to the input mass (kg/h) of the nickel to be introduced to the reactor; and/or subjecting the waste solution and the exhaust gas to countercurrent contact, then introducing the exhaust gas back to the scrubber and charging the waste solution from the scrubber into the sulfurization reactor.

    Abstract translation: 一种用于镍氧化物矿石的湿法冶金方法,包括通过高压酸洗镍氧化物矿石获得粗硫酸镍水溶液; 通过溶液硫化获得无锌的最终溶液; 获得废液; 并从废气中洗涤硫化氢气体。 该方法的特征在于以下操作中的至少一个:将硫化反应器的总体积(m3)相对于输入质量(kg / h)的比例调整为0.2-0.9(m3 / kg / h) 将镍引入反应器; 和/或使废溶液和废气进行逆流接触,然后将废气引回到洗涤器中,并将废液从洗涤器装入硫化反应器中。

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