Method of synthesizing metal doped diamond-like carbon films
    3.
    发明授权
    Method of synthesizing metal doped diamond-like carbon films 失效
    合成金刚石类金刚石碳膜的方法

    公开(公告)号:US06669996B2

    公开(公告)日:2003-12-30

    申请号:US09900439

    申请日:2001-07-06

    IPC分类号: H05H110

    CPC分类号: C23C16/26 C23C16/30

    摘要: A method of synthesizing metal doped carbon films by placing a substrate in a chamber with a selected amount of a metalorganic compound. An electron cyclotron resonance is applied to the chamber in order to vaporize the metalorganic compound. The resonance is applied to the chamber until a metal doped carbon film is formed. The metalorganic compound is preferably selected from the group consisting of an organic salt of ruthenium, palladium, gold or platinum.

    摘要翻译: 一种通过将基板放置在具有选定量的金属有机化合物的室中来合成金属掺杂碳膜的方法。 将电子回旋加速器共振施加到室以便蒸发金属有机化合物。 将谐振施加到室,直到形成金属掺杂碳膜。 金属有机化合物优选选自钌,钯,金或铂的有机盐。

    Methods for producing fused silica glass
    4.
    发明授权
    Methods for producing fused silica glass 失效
    石英玻璃生产方法

    公开(公告)号:US06532767B1

    公开(公告)日:2003-03-18

    申请号:US09659880

    申请日:2000-09-12

    IPC分类号: C03B1906

    摘要: Methods for producing high purity fused silica (HPFS) glass having desired levels of dissolved hydrogen are provided. The methods involve measuring the level of hydrogen in the cavity of the furnace used to produce the glass and controlling the pressure within the furnace and/or gas flows to the furnace's burners so that the measured concentration has a desired value. In this way, the level of dissolved hydrogen in the glass can be controlled since, as shown in FIG. 3, there is a direct correlation between the hydrogen concentration in the cavity atmosphere and level of dissolved hydrogen in the glass.

    摘要翻译: 提供了具有所需水溶液的高纯度熔融石英(HPFS)玻璃的方法。 这些方法包括测量用于制造玻璃的炉的空腔中的氢的水平,并且控制炉内的压力和/或气体流入炉的燃烧器,使得测量的浓度具有期望的值。 以这种方式,可以控制玻璃中溶解的氢的水平,因为如图1所示。 如图3所示,在空腔气氛中的氢浓度和玻璃中溶解氢的水平之间存在直接的相关性。

    Mutual solvents comprising 2,2,4-trimethyl-1,3-pentanediol mono-or di-isobutyrate and stable emulsions thereof
    5.
    发明授权
    Mutual solvents comprising 2,2,4-trimethyl-1,3-pentanediol mono-or di-isobutyrate and stable emulsions thereof 失效
    包含2,2,4-三甲基-1,3-戊二醇单或二异丁酸酯的相互溶剂及其稳定的乳液

    公开(公告)号:US06242388B1

    公开(公告)日:2001-06-05

    申请号:US09197494

    申请日:1998-11-23

    IPC分类号: C09K300

    CPC分类号: B01F17/0064 C09K8/524

    摘要: A mutual solvent for use in oil and gas well operations comprising 2,2,4-trimethyl-1,3-pentanediol monoisobutyrate and/or 2,2,4-trimethyl-1,3-pentanediol diisobutyrate, a coupling solvent, and an acid stable surfactant. The coupling solvent is selected from ethylene glycol monobutyl ether; diethylene glycol monobutyl ether; propylene glycol monomethyl ether acetate; propylene glycol monomethyl ether; C1-C5 alkyl alcohol; and mixtures thereof. The invention also relates to an emulsion for use in oil and gas well operations comprising an aqueous acid or acid-salt brine solution and the mutual solvent as described above. An emulsion according to the invention is stable, non-toxic, and effectively removes asphaltenic and paraffinic hydrocarbons from drilling equipment and oil and gas wells.

    摘要翻译: 用于油气井操作的相互溶剂,包括2,2,4-三甲基-1,3-戊二醇单异丁酸酯和/或2,2,4-三甲基-1,3-戊二醇二异丁酸酯,偶联溶剂和 酸稳定的表面活性剂。 偶联溶剂选自乙二醇单丁醚; 二甘醇单丁醚; 丙二醇单甲醚乙酸酯; 丙二醇单甲醚; C1-C5烷基醇; 及其混合物。 本发明还涉及用于油气井操作的乳液,其包含如上所述的酸或盐酸盐水溶液和互溶剂。 根据本发明的乳液是稳定的,无毒的,并有效地从钻井设备和油气井中除去沥青和石蜡烃。

    REACTOR AND METHOD FOR PRODUCTION OF NANOSTRUCTURES
    7.
    发明申请
    REACTOR AND METHOD FOR PRODUCTION OF NANOSTRUCTURES 审中-公开
    用于生产纳米结构的反应器和方法

    公开(公告)号:US20120027955A1

    公开(公告)日:2012-02-02

    申请号:US12248731

    申请日:2008-10-09

    IPC分类号: H05H1/46 C23C16/455

    摘要: A reactor and method for production of nanostructures produces, for example, metal oxide nanowires or nanoparticles. The reactor includes a metal powder delivery system wherein the metal powder delivery system includes a funnel in communication with a dielectric tube; a plasma-forming gas inlet, whereby a plasma-forming gas is delivered substantially longitudinally into the dielectric tube; a sheath gas inlet, whereby a sheath gas is delivered into the dielectric tube; and a microwave energy generator coupled to the dielectric tube, whereby microwave energy is delivered into a plasma-forming gas. The method for producing nanostructures includes delivering a plasma-forming gas substantially longitudinally into a dielectric tube; delivering a sheath gas into the tube; forming a plasma from the plasma-forming gas by applying microwave energy to the plasma-forming gas; delivering a metal powder into the dielectric tube; and reacting the metal powder within the plasma to form metal oxide nanostructures.

    摘要翻译: 用于生产纳米结构的反应器和方法产生例如金属氧化物纳米线或纳米颗粒。 反应器包括金属粉末输送系统,其中金属粉末输送系统包括与电介质管连通的漏斗; 等离子体形成气体入口,其中等离子体形成气体基本纵向地输送到电介质管中; 护套气体入口,其中护套气体被输送到电介质管中; 以及耦合到电介质管的微波能量发生器,由此将微波能量输送到等离子体形成气体中。 生产纳米结构的方法包括将等离子体形成气体基本纵向地输送到电介质管中; 将鞘气输送到管中; 通过向等离子体形成气体施加微波能量从等离子体形成气体形成等离子体; 将金属粉末输送到介质管中; 并使等离子体内的金属粉末反应形成金属氧化物纳米结构体。

    Bulk synthesis of metal and metal based dielectric nanowires
    9.
    发明授权
    Bulk synthesis of metal and metal based dielectric nanowires 失效
    金属和金属基介电纳米线的大量合成

    公开(公告)号:US07771689B2

    公开(公告)日:2010-08-10

    申请号:US10705687

    申请日:2003-11-10

    IPC分类号: C01B21/06

    摘要: A process of synthesizing metal and metal nitride nanowires, the steps comprising of: forming a catalytic metal (such as gallium, and indium) on a substrate (such as fused silica quartz, pyrolytic boron nitride, alumina, and sapphire), heating the combination in a pressure chamber, adding gaseous reactant and/or solid metal source, applying sufficient microwave energy (or current in hot filament reactor) to activate the metal of interest (such as gold, copper, tungsten, and bismuth) and continuing the process until nanowires of the desired length are formed. The substrate may be fused silica quartz, the catalytic metal a gallium or indium metal, the gaseous reactant is nitrogen and/or hydrogen and the nanowires are tungsten nitride and/or tungsten.

    摘要翻译: 合成金属和金属氮化物纳米线的方法,其步骤包括:在基底(如熔融石英石英,热解氮化硼,氧化铝和蓝宝石)上形成催化金属(如镓和铟),加热组合 在压力室中加入气体反应物和/或固体金属源,施加足够的微波能量(或热丝反应器中的电流)以激活感兴趣的金属(例如金,铜,钨和铋)并继续该过程直到 形成所需长度的纳米线。 衬底可以是熔融石英石英,催化金属是镓或铟金属,气体反应物是氮和/或氢,并且纳米线是氮化钨和/或钨。

    Synthesis of fibers of inorganic materials using low-melting metals
    10.
    发明授权
    Synthesis of fibers of inorganic materials using low-melting metals 有权
    使用低熔点金属合成无机材料的纤维

    公开(公告)号:US07713352B2

    公开(公告)日:2010-05-11

    申请号:US11521084

    申请日:2006-09-14

    IPC分类号: C30B17/00 C30B23/00

    摘要: A process is provided to produce bulk quantities of nanowires in a variety of semiconductor materials. Thin films and droplets of low-melting metals such as gallium, indium, bismuth, and aluminum are used to dissolve and to produce nanowires. The dissolution of solutes can be achieved by using a solid source of solute and low-melting metal, or using a vapor phase source of solute and low-melting metal. The resulting nanowires range in size from 1 nanometer up to 1 micron in diameter and lengths ranging from 1 nanometer to several hundred nanometers or microns. This process does not require the use of metals such as gold and iron in the form of clusters whose size determines the resulting nanowire size. In addition, the process allows for a lower growth temperature, better control over size and size distribution, and better control over the composition and purity of the nanowire produced therefrom.

    摘要翻译: 提供了一种在各种半导体材料中产生大量纳米线的方法。 使用低熔点金属如镓,铟,铋和铝的薄膜和液滴来溶解和产生纳米线。 溶质的溶解可以通过使用溶质和低熔点金属的固体源,或使用溶质和低熔点金属的气相源来实现。 所得的纳米线的尺寸范围从1纳米直到1微米的直径和长度范围从1纳米到几百纳米或微米。 该方法不需要以尺寸决定所得纳米线尺寸的簇的形式使用诸如金和铁的金属。 此外,该方法允许较低的生长温度,更好地控制尺寸和尺寸分布,以及更好地控制由其制备的纳米线的组成和纯度。