摘要:
Flame produced vapors for combustion chemical vapor deposition are redirected from the direction of the flame by differential atmospheric pressure, such as positive pressure provided by a blower or negative pressure provided by a vacuum. This allows, for example, lower surface temperatures of substrates being coated with flame-produced vapors and coating of interior surfaces.
摘要:
Tubular needles have a reduced inner diameter tip portion that increases back pressure behind the tip portion. This constricted tip portion promotes improved atomization, particularly when the liquid passes through the needle at near-supercritical conditions. A preferred method for constricting the inner diameter of a needle tip is to dip the dip of the needle in an electroless plating solution, such as an electroless nickel solution.
摘要:
The present invention is directed to the formation of unique carbonaceous materials and a new segregated manufacturing business of carbonaceous material. In particular, the invention is directed to using a flexible reactor (1) in which spray or vapor can be used to form carbonaceous materials (28) and also in combination with inorganic material (6) to enable performance enhancement of products made using these materials.
摘要:
A continuous feed coater for coating a length of substrate with vaporized or sprayed material, is disclosed. A specific example is a roll-to-roll coater which includes two lower supply rollers for supporting two webs of uncoated material, and two upper take-up rollers for supporting the webs after they are coated. A central web-support forms a plenum that acts as a deposition chimney or chamber by bringing the two webs into close proximity to each other to form two large walls of the plenum. The ends of the webs are sealed using side dams to form the chimney with a rectangular cross section such that the vapor cannot exit from the edges of the material. The vaporized coating constituents to be deposited on the rolled material are directed into the deposition plenum from a coating material supply source located at the bottom of the plenum, and are exhausted through the top of the plenum. By providing a plenum having two large surface area walls formed of the material to be coated, an extremely efficient coating system is provided. The top of the plenum includes an exhaust system with an orifice plate with a plurality of orifices spaced across the width of the deposition plenum. These orifices restrict gas exhaust to provide the gas and vapor residence time for the materials being used.
摘要:
A process is described for producing a powder batch comprises a plurality of particles, wherein the particles include (a) a first catalytically active component comprising at least one transition metal or a compound thereof; (b) a second component different from said first component and capable of removing oxygen from, or releasing oxygen to, an exhaust gas stream; and (c) a third component different from said first and second components and comprising a refractory support. The process comprises providing a precursor medium comprising a liquid vehicle and a precursor to al least one of said components (a) to (c) and heating droplets of said precursor medium carried in a gas stream to remove at least part of the liquid vehicle and chemically convert said precursor to said at least one component.
摘要:
A catalyst composition comprises a particulate support and catalyst nanoparticles on the particulate support. The catalyst nanoparticles comprise an alloy of platinum and palladium in an atomic ratio of from about 25:75 to about 75:25 and are present in a concentration of between about 3 and about 10 wt % weight percent of the catalyst composition. The catalyst composition has an X-ray diffraction pattern that is substantially free of the (311) diffraction peak assignable to PtxPd1-x, where 0.25≦x≦0.75.
摘要:
The present invention relates to colored reflective features, e.g., reflective security features or reflective decorative features, that optionally exhibit color shifting and to inks and processes for making such features. The features, as well as the inks optionally used to form the features, comprise nanoparticles and a colorant that preferably modifies a spectrum of light that is reflected by a reflective layer formed from the nanoparticles. The processes involve forming the features from one or more inks using a direct write printing process.
摘要:
A powder batch is described comprising single crystal metal-containing particles having a crystal size of less than 50 nm as measured by X-ray diffraction and having a weight average particle size of from about 10 nanometers to less than 100 nanometers as measured by transmission electron microscopy and including a continuous or non-continuous coating of a ceramic material. The powder batch is preferably produced by flame spraying.
摘要:
In one aspect, the process includes providing a precursor medium comprising a liquid vehicle and a precursor to a component, and flame spraying the precursor medium under conditions effective to form a population of nanoparticles, wherein the nanoparticles include the component. The population of nanoparticles, as formed, comprises less than about 5 percent by volume particles having a particle size greater than 1.0 μm. A size distribution of the population of nanoparticles may have a d50 value less than about 500 nm, and it may be unimodal. The size distribution may have a geometric standard deviation of less than about 2. The process may occur continuously for at least four hours or more. Greater than about 90 percent by weight of the precursor to the component in the precursor medium may be converted to the component in the nanoparticles. The process typically occurs in an enclosed flame spray reactor.