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公开(公告)号：US5130192A
公开(公告)日：1992-07-14
申请号：US613062
申请日：1990-11-15
IPC分类号： B32B15/088 , B32B7/04 , B32B15/08 , B32B38/00 , B32B43/00 , C08G73/10 , C09D179/08 , C23C14/20 , C23C28/02 , H05K1/03 , H05K3/38
CPC分类号： H05K3/388 , C08G73/1007 , C08G73/1032 , C08G73/1067 , C23C14/20 , H05K3/389 , H05K2201/0154 , Y10T428/26 , Y10T428/31681
摘要： A process for preparing a metallized polyimide film, comprising the steps of: forming a solidified film containing 100 parts by weight of an aromatic polyamic acid in the form of a solution obtained by polymerizing approximately equal moles of an aromatic tetracarboxylic acid component and an aromatic diamine component and 5 to 150 parts by weight of an organic polar solvent; applying a surface treatment solution containing a heat-resistant surface treating agent to the surface of the solidified film; heating the solidified film to a high temperature to imidize the polyamic acid, while drying the film to prepare a polyimide film; forming a thin metal vapor-deposited layer by a vapor deposition of a metal on the treated surface of the polyimide film with the heat-resistant surface treatment agent; and applying metal plating onto the metal vapor deposited layer to form a metal plated layer thereon.
摘要翻译： 一种制备金属化聚酰亚胺膜的方法，包括以下步骤：形成含有100重量份芳族聚酰胺酸的固化膜，所述芳族聚酰胺酸以通过聚合近似相等摩尔的芳族四羧酸组分和芳族二胺获得的溶液形式 组分和5至150重量份的有机极性溶剂; 将含有耐热表面处理剂的表面处理溶液涂布在固化膜的表面上; 将固化膜加热到高温以酰亚胺化聚酰胺酸，同时干燥该膜以制备聚酰亚胺膜; 通过利用耐热表面处理剂在聚酰亚胺膜的处理表面上气相沉积金属来形成薄金属气相沉积层; 并在金属蒸镀层上涂敷金属镀层，在其上形成金属镀层。
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公开(公告)号：US5262227A
公开(公告)日：1993-11-16
申请号：US707570
申请日：1991-05-30
CPC分类号： H05K3/386 , B32B15/08 , H05K1/0346 , H05K1/036 , H05K1/0393 , H05K2201/0154 , H05K2201/0195 , H05K2201/0355 , H05K2203/1545 , Y10T428/24967 , Y10T428/24975 , Y10T428/31681 , Y10T428/31721
摘要： An aromatic polyimide film directly laminated with a metal foil and an aromatic polyimide film directly laminated on both sides with a metal foil wherein the polyimide film (substrate) comprises an aromatic polyimide layer-A of 6-200 .mu.m thick whose polyimide is derived from a biphenyltetracarboxylic acid or its derivative and a phenylenediamine and an aromatic polyimide layer-B of 0.2-15 .mu.m thick whose polyimide is derived from an aromatic tetracarboxylic acid or its derivative and an aromatic diamine having plural benzene rings, and the polyimide layer-A has a thickness of not less than 55% of the total thickness of the aromatic polyimide substrate film, the polyimide layer-B is fixed to the polyimide layer-A under the condition that the layer-B cannot be peeled from the layer-A along the interface between these layers-A and -B and the metal foil is directly fixed on the surface of the polyimide layer-B via no adhesive.
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3.发明授权公开(公告)号：US09115250B2
公开(公告)日：2015-08-25
申请号：US12514793
申请日：2007-11-12
IPC分类号： C08G73/10
CPC分类号： C08G73/1028 , C08G73/1007
摘要： In a first step, a diamine is reacted with a molar excess of a tetracarboxylic dianhydride in a solvent containing more than ⅓ mole of water per mole of the tetracarboxylic dianhydride, whereby preparing a polyamic acid solution. Subsequently, in a second step, a diamine and/or a tetracarboxylic dianhydride are added to the polyamic acid solution obtained in the first step so that the molar amount of the diamine component is substantially equal to the molar amount of the tetracarboxylic acid component, and then the diamine and the tetracarboxylic dianhydride are reacted, whereby preparing a polyamic acid solution. By this process, a polyamic acid solution having a high concentration and a low viscosity may be reproducibly and reliably produced, while controlling the molecular weight of the polyamic acid to a predetermined low level.
摘要翻译： 在第一步中，二胺与摩尔过量的四羧酸二酐在每摩尔四羧酸二酐中含有超过1/3摩尔水的溶剂中反应，由此制备聚酰胺酸溶液。 接着，在第二工序中，在第一工序得到的聚酰胺酸溶液中添加二胺和/或四羧酸二酐，使二胺成分的摩尔量基本上等于四羧酸成分的摩尔量， 然后使二胺和四羧酸二酐反应，由此制备聚酰胺酸溶液。 通过该方法，可以可重复地且可靠地制造高浓度和低粘度的聚酰胺酸溶液，同时将聚酰胺酸的分子量控制在预定的低水平。
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公开(公告)号：US5180627A
公开(公告)日：1993-01-19
申请号：US801686
申请日：1991-12-02
IPC分类号： B32B7/12 , C09J163/00 , C09J179/08 , C09J183/10 , H05K1/00 , H05K3/38
CPC分类号： H05K3/386 , B32B7/12 , C09J163/00 , C09J179/08 , C09J183/10 , H05K1/0393 , H05K2201/0154 , H05K2201/0162 , H05K2201/0355 , Y10T428/24959 , Y10T428/31522 , Y10T428/31721
摘要： The disclosed heat resistant adhesive composition comprises a polyimidesiloxane obtained from a biphenyltetracarboxylic acid or its derivative and a diamine composition comprising a diaminopolysiloxane and an aromatic diamine, an epoxy compound having an epoxy group, and an epoxy compound-hardening agent. An adhesive film and a composite sheet utilizing the heat resistant resinous composition are also disclosed.
摘要翻译： 所公开的耐热粘合剂组合物包含由联苯四羧酸或其衍生物获得的聚酰亚胺硅氧烷和包含二氨基聚硅氧烷和芳族二胺的二胺组合物，具有环氧基的环氧化合物和环氧化合物硬化剂。 还公开了一种使用耐热树脂组合物的粘合膜和复合片。
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5.发明申请BINDER RESIN COMPOSITION FOR ELECTRODE, ELECTRODE MIXTURE PASTE, AND ELECTRODE 有权电极，电极混合胶和电极的粘结剂树脂组合物公开(公告)号：US20120168688A1
公开(公告)日：2012-07-05
申请号：US13394815
申请日：2010-09-22
IPC分类号： H01B1/12 , H01B1/24 , H01B1/22 , C08K5/3415
CPC分类号： H01B1/22 , H01G11/28 , H01G11/30 , H01G11/38 , H01M4/133 , H01M4/134 , H01M4/1393 , H01M4/1395 , H01M4/622 , H01M10/0525 , Y02E60/122 , Y02E60/13
摘要： The present invention relates to a binder resin composition for an electrode, including a polyamic acid and a solvent, wherein the polyamic acid is (i) a polyamic acid which includes a tetracarboxylic acid component including 10 to 100 mol % of 4,4′-oxydiphthalic acid and 90 to 0 mol % of 3,3′,4,4′-biphenyltetracarboxylic acid and/or pyromellitic acid and a diamine component including an aromatic diamine having 1 to 4 aromatic rings, (ii) a polyamic acid which includes a tetracarboxylic acid component including 3,3′,4,4′-biphenyltetracarboxylic acid dianhydride and a diamine component including 10 to 90 mol % of p-phenylene diamine and 90 to 10 mol % of 4,4′-diaminodiphenyl ether, or (iii) a polyamic acid which includes a tetracarboxylic acid component including 3,3′,4,4′-biphenyltetracarboxylic acid dianhydride and a diamine component including 40 mol % or more of a bis[4-(4-aminophenoxy)phenyl] compound.
摘要翻译： 本发明涉及包含聚酰胺酸和溶剂的电极用粘合剂树脂组合物，其中聚酰胺酸为（ⅰ）聚酰胺酸，其包含含有10〜100摩尔％的4,4'-二羧酸的四羧酸成分， 氧联二邻苯二甲酸和90至0mol％的3,3'，4,4'-联苯四羧酸和/或均苯四酸和包含具有1-4个芳环的芳族二胺的二胺组分，（ii）聚酰胺酸，其包括 或包含3,3'，4,4'-联苯四羧酸二酐的四羧酸组分和包含10-90mol％对苯二胺和90-10mol％的4,4'-二氨基二苯醚的二胺组分，或（iii ）聚酰胺酸，其包括包含3,3'，4,4'-联苯四羧酸二酐的四羧酸组分和包含40mol％或更多的双[4-（4-氨基苯氧基）苯基]化合物的二胺组分。
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公开(公告)号：US07491427B2
公开(公告)日：2009-02-17
申请号：US10589982
申请日：2005-02-21
IPC分类号： B05D3/02
CPC分类号： C08L83/10 , C08G18/61 , C08K3/36 , C08L79/08 , C09D183/10 , H01L21/563 , H01L23/49894 , H01L2924/0002 , H05K3/285 , C08L83/00 , H01L2924/00
摘要： [PROBLEMS] To provide a polyimidesiloxane solution composition that is excellent in defoaming ability and that can maintain the wettability of an outer lead bonded portion on a wiring board at a high level, even when it is applied on the surface of the wiring board and then cured, to form an insulating cured film.[MEANS FOR SOLVING PROBLEMS] A polyimidesiloxane solution composition which comprises an organic solvent, polyimidesiloxane soluble in the organic solvent, a curable components such as an epoxy compound and a polyvalent isocyanate compound, and a silicone defoamer, wherein the silicone defoaming agent comprises dimethylpolysiloxane, a polysiloxane compound having a hydrophilic group in a side chain or a terminal moiety, and a micro-powder silica.
摘要翻译： [问题]为了提供消泡能力优异且能够将布线基板上的外引线接合部的润湿性保持在高水平的聚酰亚胺硅溶液组合物，即使将其施加在布线板的表面上， 固化，形成绝缘固化膜。 解决问题的手段聚硅氧烷溶液组合物，其包含有机溶剂，可溶于有机溶剂的聚酰亚胺硅氧烷，可固化组分如环氧化合物和多价异氰酸酯化合物，以及硅氧烷消泡剂，其中所述硅氧烷消泡剂包括二甲基聚硅氧烷， 在侧链或末端部分具有亲水基团的聚硅氧烷化合物和微粉末二氧化硅。
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7.发明授权Process for producing pigment-containing curable resin solution composition, pigment dispersed liquid, and pigment-containing curable resin solution composition 有权用于制备含颜料的可固化树脂溶液组合物，颜料分散液和含颜料的可固化树脂溶液组合物的方法公开(公告)号：US08735467B2
公开(公告)日：2014-05-27
申请号：US12492807
申请日：2009-06-26
CPC分类号： H05K3/285 , C08G77/455 , H05K1/0269 , H05K2203/161
摘要： A process for producing a pigment-containing curable resin solution composition which comprises a pigment and a modified polysiloxane is disclosed. The process comprises the steps of: (a) preparing a pigment-dispersed liquid, wherein a pigment is dispersed in an organic solvent in the presence of a first modified polysiloxane; and (b) mixing the pigment-dispersed liquid with a resin solution which comprises at least a second modified polysiloxane. This process provides a pigment-containing curable resin solution composition with excellent dispersion stability of pigment.
摘要翻译： 公开了一种含有颜料和改性聚硅氧烷的含颜料的可固化树脂溶液组合物的制备方法。 该方法包括以下步骤：（a）制备颜料分散液体，其中在第一改性聚硅氧烷存在下将颜料分散在有机溶剂中; 和（b）将分散颜料的液体与至少包含第二改性聚硅氧烷的树脂溶液混合。 该方法提供了颜料的分散稳定性优异的含颜料的可固化树脂溶液组合物。
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公开(公告)号：US20100305295A1
公开(公告)日：2010-12-02
申请号：US12745217
申请日：2008-12-01
IPC分类号： C08G73/10
CPC分类号： C08G73/1032 , C08G73/1007 , C08G73/1028 , C08G73/1042 , C08G73/1046 , C08G73/105 , C08G73/1067 , C08G73/1071
摘要： Disclosed is a process for producing a polyamic acid solution by reacting a diamine component consisting essentially of 20 mol % to 80 mol % of p-phenylenediamine and 80 mol % to 20 mol % of diaminodiphenyl ether with a tetracarboxylic acid component consisting essentially of 10 mol % to 60 mol % of 2,3,3′,4′-biphenyltetracarboxylic dianhydride and 90 mol % to 40 mol % of 3,3′,4,4′-biphenyltetracarboxylic dianhydride in a solvent, comprising:a first step in which a diamine component is reacted with a molar excess of a tetracarboxylic acid component in a solvent containing more than ⅓ mole of water per mole of the tetracarboxylic acid component, whereby preparing a polyamic acid solution; anda second step in which a diamine component, or a diamine component and a tetracarboxylic acid component are added to the polyamic acid solution obtained in the first step so that the molar amount of the diamine component is substantially equal to the molar amount of the tetracarboxylic acid component, and then the diamine component and the tetracarboxylic acid component are reacted.
摘要翻译： 公开了一种通过使基本上由20摩尔％至80摩尔％的对苯二胺和80摩尔％至20摩尔％的二氨基二苯醚组成的二胺组分与基本上由10摩尔组成的四羧酸组分反应制备聚酰胺酸溶液的方法 在溶剂中的2,3,3'，4'-联苯四羧酸二酐和90摩尔％至40摩尔％的3,3'，4,4'-联苯四羧酸二酐的％至60摩尔％，包括：第一步，其中 二胺成分与摩尔过量的四羧酸成分在每摩尔四羧酸成分含有超过1/3摩尔水的溶剂中反应，由此制备聚酰胺酸溶液; 第二步是将二胺成分或二胺成分和四羧酸成分添加到第一工序得到的聚酰胺酸溶液中，使二胺成分的摩尔量基本上等于四羧酸的摩尔量 酸组分，然后二胺组分和四羧酸组分反应。
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9.发明授权Shaped electroconductive aromatic imide polymer article and process for producing 失效形状导电芳香族酰亚胺聚合物制品及其制备方法
公开(公告)号：US4810419A
公开(公告)日：1989-03-07
申请号：US117431
申请日：1987-11-02
CPC分类号： H01B1/24 , C08K7/06 , Y10T428/249941 , Y10T428/31721
摘要： A shaped electroconductive aromatic imide polymer article comprising an aromatic imide polymer matrix and 10% to 40% by weight of short cut carbon fibers 1 to 30 .mu.m thick and 0.05 to 3.0 mm long dispersed in the matrix, is produced by admixing a slurry of the short cut carbon fibers having a limited moisture content of 1.0% or less in a polymerization medium, with a polymerization mixture containing an aromatic tetracarboxylic acid component and an aromatic diamine component, by subjecting the resultant admixture to a polymerization procedure to prepare a dope comprising a resultant polymerization product, the carbon fibers and the polymerization medium, and by subjecting the dope to shaped article-producing procedures in which the dope is shaped into a desired form and the shaped dope is solidified by removing the polymerization medium to provide a desired shaped article.
摘要翻译： 包含芳族酰亚胺聚合物基质和10％至40％重量的分散在基质中1至30μm厚和0.05至3.0mm长的短切碳纤维的成形导电芳族酰亚胺聚合物制品是通过将 在聚合介质中具有有限水分含量为1.0％以下的短切碳纤维，含有芳香族四羧酸成分和芳香族二胺成分的聚合混合物通过对所得到的混合物进行聚合过程来制备涂料，包括 所得到的聚合产物，碳纤维和聚合介质，以及通过将掺杂物制成制品的方法，其中将涂料成型为所需形状，并且通过除去聚合介质来固化成型的涂料以提供所需的成型 文章。
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公开(公告)号：US4729771A
公开(公告)日：1988-03-08
申请号：US910946
申请日：1986-09-24
CPC分类号： B24D11/00 , B24D3/344 , C09K3/1409 , C09K3/1445
摘要： An abrasive sheet having an excellent flexibility, mechanical strength and heat resistance comprises an aromatic imide polymer matrix and abrasive particles having an average size of 0.1 to 50 .mu.m and is prepared by evenly dispersing the abrasive particles in an organic polar solvent, mixing the resultant dispersion with a polymerization mixture consisting of an acid component comprising, as a major acid ingredient, a biphenyltetracarboxylic acid or an dianhydride thereof with a diamine component comprising an aromatic diamine, while polymerizing the acid and diamine components at 0.degree. C. to 80.degree. C. into an aromatic polyamic acid, forming the resultant dope dispersion into a thin layer and solidifying the thin layer while imidizing the aromatic polyamic acid into a corresponding aromatic imide polymer.
摘要翻译： 具有优异的柔韧性，机械强度和耐热性的研磨片包括芳族酰亚胺聚合物基质和平均粒度为0.1-50μm的研磨颗粒，并通过将磨料颗粒均匀分散在有机极性溶剂中，将所得的 在含有酸组分的聚合混合物中分散，该酸组分包含作为主要酸成分的联苯四羧酸或其二酐与包含芳族二胺的二胺组分，同时在0℃至80℃下聚合酸和二胺组分 形成芳族聚酰胺酸，将所得的涂料分散体形成薄层并固化薄层，同时将芳族聚酰胺酸酰亚胺化成相应的芳族酰亚胺聚合物。
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