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公开(公告)号：US08865271B2
公开(公告)日：2014-10-21
申请号：US10854019
申请日：2004-05-26
IPC分类号： C23C14/30 , C23C24/00 , C23C16/48 , G02B6/132 , C03B37/012 , C23C16/56 , C03B19/01 , C03B19/14 , C23C24/04 , C23C16/40 , C03B37/014 , G02B6/036
CPC分类号： G02B1/12 , B05D1/12 , B05D3/06 , C03B19/01 , C03B19/1415 , C03B37/0128 , C03B37/01294 , C03B37/01406 , C03B37/01413 , C03B37/0142 , C03B2201/10 , C03B2201/12 , C03B2201/28 , C03B2201/31 , C03B2207/34 , C23C16/401 , C23C16/482 , C23C16/483 , C23C16/56 , C23C24/00 , C23C24/04 , G02B6/036 , G02B6/132 , Y02P40/57
摘要： High rate deposition methods comprise depositing a powder coating from a product flow. The product flow results from a chemical reaction within the flow. Some of the powder coatings consolidate under appropriate conditions into an optical coating. The substrate can have a first optical coating onto which the powder coating is placed. The resulting optical coating following consolidation can have a large index-of-refraction difference with the underlying first optical coating, high thickness and index-of-refraction uniformity across the substrate and high thickness and index-of-refraction uniformity between coatings formed on different substrates under equivalent conditions. In some embodiments, the deposition can result in a powder coating of at least about 100 nm in no more than about 30 minutes with a substrate having a surface area of at least about 25 square centimeters.
摘要翻译： 高速沉积方法包括从产品流中沉积粉末涂层。 产物流由流动内的化学反应产生。 一些粉末涂料在合适的条件下固化成光学涂层。 基底可以具有第一光学涂层，其上放置粉末涂层。 固结后的所得光学涂层可以具有与基底的第一光学涂层，基底上的高厚度和折射率均匀性的较大的折射率差异，以及形成在不同的涂层之间的涂层之间的高厚度和折射率均匀性 在相同条件下的底物。 在一些实施方案中，沉积可导致至少约100nm的粉末涂层，其表面积至少约25平方厘米，其表面积至少约为25平方厘米。
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公开(公告)号：US07776406B2
公开(公告)日：2010-08-17
申请号：US11975613
申请日：2007-10-19
申请人： Craig R. Horne , Pierre J. DeMascarel , Christian C. Honeker , Benjamin Chaloner-Gill , Herman A. Lopez , Xiangxin Bi , Ronald J. Mosso , William E. McGovern , James T. Gardner , Sujeet Kumar , James A. Gilliam , Vince Pham , Eric Euvrard , Shivkumar Chiruvolu , Jesse Jur
发明人： Craig R. Horne , Pierre J. DeMascarel , Christian C. Honeker , Benjamin Chaloner-Gill , Herman A. Lopez , Xiangxin Bi , Ronald J. Mosso , William E. McGovern , James T. Gardner , Sujeet Kumar , James A. Gilliam , Vince Pham , Eric Euvrard , Shivkumar Chiruvolu , Jesse Jur
IPC分类号： C08J7/18
CPC分类号： B82Y30/00 , C01B13/20 , C01B19/004 , C01F17/0043 , C01G1/00 , C01G17/00 , C01G23/00 , C01P2002/02 , C01P2002/50 , C01P2004/50 , C01P2004/62 , C01P2004/64 , C01P2004/84 , C01P2006/60 , C01P2006/80 , C03B19/106 , C03B19/1415 , C03B2207/34 , C03C3/062 , C03C3/078 , C03C3/095 , C03C3/097 , C03C3/122 , C03C3/17 , C03C3/253 , C03C12/00 , C09K11/7706 , Y02P40/57 , Y10T428/25 , Y10T428/256 , Y10T428/2949 , Y10T428/2982 , Y10T428/2991 , Y10T428/31609
摘要： Nanoscale particles, particle coatings/particle arrays and corresponding consolidated materials are described based on an ability to vary the composition involving a wide range of metal and/or metalloid elements and corresponding compositions. In particular, metalloid oxides and metal-metalloid compositions are described in the form of improved nanoscale particles and coatings formed from the nanoscale particles. Compositions comprising rare earth metals and dopants/additives with rare earth metals are described. Complex compositions with a range of host compositions and dopants/additives can be formed using the approaches described herein. The particle coating can take the form of particle arrays that range from collections of disbursable primary particles to fused networks of primary particles forming channels that reflect the nanoscale of the primary particles. Suitable materials for optical applications are described along with some optical devices of interest.
摘要翻译： 基于改变涉及宽范围的金属和/或准金属元素和相应组合物的组合物的能力来描述纳米颗粒，颗粒涂层/颗粒阵列和相应的固结材料。 特别地，准金属氧化物和金属 - 准金属组合物以改进的纳米级颗粒和由纳米级颗粒形成的涂层的形式描述。 描述了包含稀土金属和稀土金属的掺杂剂/添加剂的组合物。 可以使用本文所述的方法形成具有一系列主体组合物和掺杂剂/添加剂的复合组合物。 颗粒涂层可以采用粒子阵列的形式，其范围从可分离的初级粒子的集合到形成反映初级粒子的纳米尺度的通道的初级粒子的融合网络。 适用于光学应用的材料与一些感兴趣的光学装置一起被描述。
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公开(公告)号：US07306845B2
公开(公告)日：2007-12-11
申请号：US10977608
申请日：2004-10-29
申请人： Craig R. Horne , Pierre J. DeMascarel , Christian C. Honeker , Benjamin Chaloner-Gill , Herman A. Lopez , Xiangxin Bi , Ronald J. Mosso , William E. McGovern , James T. Gardner , Sujeet Kumar , James A. Gilliam , Vince Pham , Eric Euvrard , Shivkumar Chiruvolu , Jesse Jur
发明人： Craig R. Horne , Pierre J. DeMascarel , Christian C. Honeker , Benjamin Chaloner-Gill , Herman A. Lopez , Xiangxin Bi , Ronald J. Mosso , William E. McGovern , James T. Gardner , Sujeet Kumar , James A. Gilliam , Vince Pham , Eric Euvrard , Shivkumar Chiruvolu , Jesse Jur
IPC分类号： B32B5/16
CPC分类号： B82Y30/00 , C01B13/20 , C01B19/004 , C01F17/0043 , C01G1/00 , C01G17/00 , C01G23/00 , C01P2002/02 , C01P2002/50 , C01P2004/50 , C01P2004/62 , C01P2004/64 , C01P2004/84 , C01P2006/60 , C01P2006/80 , C03B19/106 , C03B19/1415 , C03B2207/34 , C03C3/062 , C03C3/078 , C03C3/095 , C03C3/097 , C03C3/122 , C03C3/17 , C03C3/253 , C03C12/00 , C09K11/7706 , Y02P40/57 , Y10T428/25 , Y10T428/256 , Y10T428/2949 , Y10T428/2982 , Y10T428/2991 , Y10T428/31609
摘要： Nanoscale particles, particle coatings/particle arrays and corresponding consolidated materials are described based on an ability to vary the composition involving a wide range of metal and/or metalloid elements and corresponding compositions. In particular, metalloid oxides and metal-metalloid compositions are described in the form of improved nanoscale particles and coatings formed from the nanoscale particles. Compositions comprising rare earth metals and dopants/additives with rare earth metals are described. Complex compositions with a range of host compositions and dopants/additives can be formed using the approaches described herein. The particle coating can take the form of particle arrays that range from collections of disbursable primary particles to fused networks of primary particles forming channels that reflect the nanoscale of the primary particles. Suitable materials for optical applications are described along with some optical devices of interest.
摘要翻译： 基于改变涉及宽范围的金属和/或准金属元素和相应组合物的组合物的能力来描述纳米颗粒，颗粒涂层/颗粒阵列和相应的固结材料。 特别地，准金属氧化物和金属 - 准金属组合物以改进的纳米级颗粒和由纳米级颗粒形成的涂层的形式描述。 描述了包含稀土金属和稀土金属的掺杂剂/添加剂的组合物。 可以使用本文所述的方法形成具有一系列主体组合物和掺杂剂/添加剂的复合组合物。 颗粒涂层可以采用粒子阵列的形式，其范围从可分离的初级粒子的集合到形成反映初级粒子的纳米尺度的通道的初级粒子的融合网络。 适用于光学应用的材料与一些感兴趣的光学装置一起被描述。
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公开(公告)号：US06849334B2
公开(公告)日：2005-02-01
申请号：US10099597
申请日：2002-03-15
申请人： Craig R. Horne , Pierre J. DeMascarel , Christian C. Honeker , Benjamin Chaloner-Gill , Herman A. Lopez , Xiangxin Bi , Ronald J. Mosso , William E. McGovern , James T. Gardner , Sujeet Kumar , James A. Gilliam , Vince Pham , Eric Euvrard , Shivkumar Chiruvolu , Jesse Jur
发明人： Craig R. Horne , Pierre J. DeMascarel , Christian C. Honeker , Benjamin Chaloner-Gill , Herman A. Lopez , Xiangxin Bi , Ronald J. Mosso , William E. McGovern , James T. Gardner , Sujeet Kumar , James A. Gilliam , Vince Pham , Eric Euvrard , Shivkumar Chiruvolu , Jesse Jur
IPC分类号： G02B6/12 , C01B13/20 , C01B19/00 , C01F17/00 , C01G1/00 , C01G17/00 , C01G23/00 , C03B8/00 , C03B19/10 , C03B19/14 , C03C3/068 , C03C3/095 , C03C3/15 , C03C4/12 , C03C12/00 , C23C16/42 , G02B1/00 , B32B5/16
CPC分类号： B82Y30/00 , C01B13/20 , C01B19/004 , C01F17/0043 , C01G1/00 , C01G17/00 , C01G23/00 , C01P2002/02 , C01P2002/50 , C01P2004/50 , C01P2004/62 , C01P2004/64 , C01P2004/84 , C01P2006/60 , C01P2006/80 , C03B19/106 , C03B19/1415 , C03B2207/34 , C03C3/062 , C03C3/078 , C03C3/095 , C03C3/097 , C03C3/122 , C03C3/17 , C03C3/253 , C03C12/00 , C09K11/7706 , Y02P40/57 , Y10T428/25 , Y10T428/256 , Y10T428/2949 , Y10T428/2982 , Y10T428/2991 , Y10T428/31609
摘要： Nanoscale particles, particle coatings/particle arrays and corresponding consolidated materials are described based on an ability to vary the composition involving a wide range of metal and/or metalloid elements and corresponding compositions. In particular, metalloid oxides and metal-metalloid compositions are described in the form of improved nanoscale particles and coatings formed from the nanoscale particles. Compositions comprising rare earth metals and dopants/additives with rare earth metals are described. Complex compositions with a range of host compositions and dopants/additives can be formed using the approaches described herein. The particle coating can take the form of particle arrays that range from collections of disbursable primary particles to fused networks of primary particles forming channels that reflect the nanoscale of the primary particles. Suitable materials for optical applications are described along with some optical devices of interest.
摘要翻译： 基于改变涉及宽范围的金属和/或准金属元素和相应组合物的组合物的能力来描述纳米颗粒，颗粒涂层/颗粒阵列和相应的固结材料。 特别地，准金属氧化物和金属 - 准金属组合物以改进的纳米级颗粒和由纳米级颗粒形成的涂层的形式描述。 描述了包含稀土金属和稀土金属的掺杂剂/添加剂的组合物。 可以使用本文所述的方法形成具有一系列主体组合物和掺杂剂/添加剂的复合组合物。 颗粒涂层可以采用粒子阵列的形式，其范围从可分离的初级粒子的集合到形成反映初级粒子的纳米尺度的通道的初级粒子的融合网络。 适用于光学应用的材料与一些感兴趣的光学装置一起被描述。
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公开(公告)号：US08673407B2
公开(公告)日：2014-03-18
申请号：US11192159
申请日：2005-07-28
申请人： Xiangxin Bi , Elizabeth Anne Nevis , Ronald J. Mosso , Michael Edward Chapin , Shivkumar Chiruvolu , Sardar Hyat Khan , Sujeet Kumar , Herman Adrian Lopez , Nguyen Tran The Huy , Craig Richard Horne , Michael A. Bryan , Eric Euvrard
发明人： Xiangxin Bi , Elizabeth Anne Nevis , Ronald J. Mosso , Michael Edward Chapin , Shivkumar Chiruvolu , Sardar Hyat Khan , Sujeet Kumar , Herman Adrian Lopez , Nguyen Tran The Huy , Craig Richard Horne , Michael A. Bryan , Eric Euvrard
IPC分类号： C23C16/04 , C23C16/22 , C23C16/40 , C23C16/455 , C23C16/48
CPC分类号： H01S3/0632 , H01S3/0635 , H01S3/0637 , H01S3/0941 , H01S3/176 , H01S3/2308
摘要： Three dimensional optical structures are described that can have various integrations between optical devices within and between layers of the optical structure. Optical turning elements can provide optical pathways between layers of optical devices. Methods are described that provide for great versatility on contouring optical materials throughout the optical structure. Various new optical devices are enabled by the improved optical processing approaches.
摘要翻译： 描述了三维光学结构，其可以在光学结构的层内和层之间的光学器件之间具有各种集成。 光学旋转元件可以提供光学装置的层之间的光学路径。 描述了在整个光学结构中轮廓化光学材料方面具有很大通用性的方法。 通过改进的光学处理方法可以实现各种新的光学器件。
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公开(公告)号：US06952504B2
公开(公告)日：2005-10-04
申请号：US10027906
申请日：2001-12-21
申请人： Xiangxin Bi , Elizabeth Anne Nevis , Ronald J. Mosso , Michael Edward Chapin , Shivkumar Chiruvolu , Sardar Hyat Khan , Sujeet Kumar , Herman Adrian Lopez , Nguyen Tran The Huy , Craig Richard Horne , Michael A. Bryan , Eric Euvrard
发明人： Xiangxin Bi , Elizabeth Anne Nevis , Ronald J. Mosso , Michael Edward Chapin , Shivkumar Chiruvolu , Sardar Hyat Khan , Sujeet Kumar , Herman Adrian Lopez , Nguyen Tran The Huy , Craig Richard Horne , Michael A. Bryan , Eric Euvrard
IPC分类号： H01S3/063 , H01S3/0941 , H01S3/17 , H01S3/00 , G02F1/295
CPC分类号： H01S3/0632 , H01S3/0635 , H01S3/0637 , H01S3/0941 , H01S3/176 , H01S3/2308
摘要： Three dimensional optical structures are described that can have various integrations between optical devices within and between layers of the optical structure. Optical turning elements can provide optical pathways between layers of optical devices. Methods are described that provide for great versatility on contouring optical materials throughout the optical structure. Various new optical devices are enabled by the improved optical processing approaches.
摘要翻译： 描述了三维光学结构，其可以在光学结构的层内和层之间的光学器件之间具有各种集成。 光学旋转元件可以提供光学装置的层之间的光学路径。 描述了在整个光学结构中轮廓化光学材料方面具有很大通用性的方法。 通过改进的光学处理方法可以实现各种新的光学器件。
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公开(公告)号：US20050019504A1
公开(公告)日：2005-01-27
申请号：US10854019
申请日：2004-05-26
申请人： Xiangxin Bi , Herman Lopez , Prasad Narasimha , Eric Euvrard , Ronald Mosso
发明人： Xiangxin Bi , Herman Lopez , Prasad Narasimha , Eric Euvrard , Ronald Mosso
IPC分类号： B05D3/02 , B05D7/00 , B32B20060101 , C03B37/018 , C23C16/40 , C23C16/452 , C23C16/453 , C23C24/00 , C23C24/04 , G02B6/10
CPC分类号： G02B1/12 , B05D1/12 , B05D3/06 , C03B19/01 , C03B19/1415 , C03B37/0128 , C03B37/01294 , C03B37/01406 , C03B37/01413 , C03B37/0142 , C03B2201/10 , C03B2201/12 , C03B2201/28 , C03B2201/31 , C03B2207/34 , C23C16/401 , C23C16/482 , C23C16/483 , C23C16/56 , C23C24/00 , C23C24/04 , G02B6/036 , G02B6/132 , Y02P40/57
摘要： High rate deposition methods comprise depositing a powder coating from a product flow. The product flow results from a chemical reaction within the flow. Some of the powder coatings consolidate under appropriate conditions into an optical coating. The substrate can have a first optical coating onto which the powder coating is placed. The resulting optical coating following consolidation can have a large index-of-refraction difference with the underlying first optical coating, high thickness and index-of-refraction uniformity across the substrate and high thickness and index-of-refraction uniformity between coatings formed on different substrates under equivalent conditions. In some embodiments, the deposition can result in a powder coating of at least about 100 nm in no more than about 30 minutes with a substrate having a surface area of at least about 25 square centimeters.
摘要翻译： 高速沉积方法包括从产品流中沉积粉末涂层。 产物流由流动内的化学反应产生。 一些粉末涂料在合适的条件下固化成光学涂层。 基底可以具有第一光学涂层，其上放置粉末涂层。 固结后的所得光学涂层可以具有与基底的第一光学涂层，基底上的高厚度和折射率均匀性的较大的折射率差异，以及形成在不同的涂层之间的涂层之间的高厚度和折射率均匀性 在相同条件下的底物。 在一些实施方案中，沉积可导致至少约100nm的粉末涂层，其表面积至少为约25平方厘米，而不超过约30分钟。
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公开(公告)号：US20120012032A1
公开(公告)日：2012-01-19
申请号：US13240785
申请日：2011-09-22
申请人： Xiangxin Bi , Nobuyuki Kambe , Craig R. Horne , James T. Gardner , Ronald J. Mosso , Shivkumar Chiruvolu , Sujeet Kumar , William E. McGovern , Pierre J. DeMascarel , Robert B. Lynch
发明人： Xiangxin Bi , Nobuyuki Kambe , Craig R. Horne , James T. Gardner , Ronald J. Mosso , Shivkumar Chiruvolu , Sujeet Kumar , William E. McGovern , Pierre J. DeMascarel , Robert B. Lynch
CPC分类号： B22F1/0018 , B22F9/24 , B82Y30/00 , C01B21/068 , C01B25/45 , C01B32/956 , C01B33/182 , C01F7/302 , C01F7/308 , C01F7/44 , C01F17/0043 , C01G9/02 , C01G19/02 , C01G23/005 , C01G31/00 , C01G31/02 , C01G45/02 , C01G45/1242 , C01G51/42 , C01G53/42 , C01P2002/02 , C01P2002/32 , C01P2002/54 , C01P2002/72 , C01P2004/04 , C01P2004/51 , C01P2004/64 , C01P2004/80 , C01P2006/12 , C04B35/44 , C04B2235/3215 , C04B2235/3224 , C04B2235/3262 , C04B2235/5454 , Y10T428/2982
摘要： Methods are described that have the capability of producing submicron/nanoscale particles, in some embodiments dispersible, at high production rates. In some embodiments, the methods result in the production of particles with an average diameter less than about 75 nanometers that are produced at a rate of at least about 35 grams per hour. In other embodiments, the particles are highly uniform. These methods can be used to form particle collections and/or powder coatings. Powder coatings and corresponding methods are described based on the deposition of highly uniform submicron/nanoscale particles.
摘要翻译： 描述了在高生产率下具有产生亚微米/纳米级颗粒的能力的方法，在一些实施方案中可分散。 在一些实施方案中，该方法导致以至少约35克/小时的速率生产平均直径小于约75纳米的颗粒。 在其它实施方案中，颗粒是高度均匀的。 这些方法可用于形成颗粒收集和/或粉末涂料。 基于高度均匀的亚微米/纳米级颗粒的沉积来描述粉末涂料和相应的方法。
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公开(公告)号：US08568684B2
公开(公告)日：2013-10-29
申请号：US12686803
申请日：2010-01-13
申请人： Xiangxin Bi , Nobuyuki Kambe , James T. Gardner , Ronald J. Mosso , Shivkumar Chiruvolu , Sujeet Kumar , William E. McGovern
发明人： Xiangxin Bi , Nobuyuki Kambe , James T. Gardner , Ronald J. Mosso , Shivkumar Chiruvolu , Sujeet Kumar , William E. McGovern
IPC分类号： C01B33/02
CPC分类号： C09D5/031 , B22F1/0018 , B22F9/24 , B82Y30/00 , C01B21/068 , C01B25/45 , C01B32/956 , C01B33/182 , C01F7/302 , C01F7/308 , C01F7/44 , C01F17/0043 , C01G9/02 , C01G19/02 , C01G23/005 , C01G31/00 , C01G31/02 , C01G45/02 , C01G45/1242 , C01G51/42 , C01G53/42 , C01P2002/02 , C01P2002/32 , C01P2002/54 , C01P2002/72 , C01P2004/04 , C01P2004/51 , C01P2004/64 , C01P2004/80 , C01P2006/12 , C04B35/44 , C04B2235/3215 , C04B2235/3224 , C04B2235/3262 , C04B2235/5454 , Y10T428/2982
摘要： Methods are described that have the capability of producing submicron/nanoscale particles, in some embodiments dispersible, at high production rates. In some embodiments, the methods result in the production of particles with an average diameter less than about 75 nanometers that are produced at a rate of at least about 35 grams per hour. In other embodiments, the particles are highly uniform. These methods can be used to form particle collections and/or powder coatings. Powder coatings and corresponding methods are described based on the deposition of highly uniform submicron/nanoscale particles.
摘要翻译： 描述了在高生产率下具有产生亚微米/纳米级颗粒的能力的方法，在一些实施方案中可分散。 在一些实施方案中，该方法导致以至少约35克/小时的速率生产平均直径小于约75纳米的颗粒。 在其它实施方案中，颗粒是高度均匀的。 这些方法可用于形成颗粒收集和/或粉末涂料。 基于高度均匀的亚微米/纳米级颗粒的沉积来描述粉末涂料和相应的方法。
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公开(公告)号：US07507382B2
公开(公告)日：2009-03-24
申请号：US09970279
申请日：2001-10-03
申请人： Hariklia Dris Reitz , Sujeet Kumar , Xiangxin Bi , Nobuyuki Kambe , Ronald J. Mosso , James T. Gardner
发明人： Hariklia Dris Reitz , Sujeet Kumar , Xiangxin Bi , Nobuyuki Kambe , Ronald J. Mosso , James T. Gardner
IPC分类号： B01J19/08
CPC分类号： C01G9/03 , B82Y30/00 , C01P2002/72 , C01P2004/04 , C01P2004/62 , C01P2004/64 , C09C1/043 , C09K11/54 , H01C7/112
摘要： A collection of zinc oxide nanoparticles have been produced by laser pyrolysis. The zinc oxide nanoparticles have average particle diameters of less than about 95 nm and a very narrow particle size distribution. The laser pyrolysis process is characterized by the production of a reactant stream within the reaction chamber, where the reactant stream includes a zinc precursor and other reactants. The zinc precursor can be delivered as an aerosol.
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